Vinayak V. Rao, Pradipkumar Dixit, R. Hari Krishna, K. Ramakrishna Murthy
{"title":"纳米Al2O3填充硅橡胶试样用于室外绝缘的实验研究","authors":"Vinayak V. Rao, Pradipkumar Dixit, R. Hari Krishna, K. Ramakrishna Murthy","doi":"10.3103/S1068375523040154","DOIUrl":null,"url":null,"abstract":"<p>Composite insulators are popular choice in contemporary power industry due to their numerous advantages. When these insulators are subject to various stresses, their performance gets affected due to the material degradation. One of the methods to improve the material property is to incorporate inorganic nanofillers. In this work, aluminum oxide nanofillers, synthesized in the laboratory using a solution combustion process were used and studied. The nano range was ascertained with X-ray diffraction. Those fillers were mixed in the silicone rubber specimens in 0, 1, 3, and 5 wt % concentrations. They were more rapidly aged under UV radiation, temperature, humidity and electric stresses. Dry and wet flashover tests were carried out on both virgin and aged samples, and the results showed that the concentration of 3 wt % offered a better breakdown voltage. Fourier transform infrared spectroscopy revealed percentage variations in the properties of the aged specimens, the aging resistance, degradation resistance, hydrophobicity, oxidation resistance, and erosion resistance were significantly better in 3 wt % Al<sub>2</sub>O<sub>3</sub> filled samples. Scanning electron microscopy with energy dispersive X-ray spectroscopy images showed that at 3 wt % concentration there was a fairly uniform distribution of nanofillers in the silicone base and there was the least ingress of water at same weight percentage of specimens. Their improvements in the insulation property is primarily attributed to the fair distribution of nano Al<sub>2</sub>O<sub>3</sub> fillers into the silicone base, a good Si–CH<sub>3</sub> bond structure, a low carbon cross linking and good percolation, which makes them the best candidates for outdoor insulation of power systems.</p>","PeriodicalId":782,"journal":{"name":"Surface Engineering and Applied Electrochemistry","volume":null,"pages":null},"PeriodicalIF":0.9000,"publicationDate":"2023-09-04","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Experimental Investigation of Nano Al2O3 Filled Silicone Rubber Specimen Used in Outdoor Insulation\",\"authors\":\"Vinayak V. Rao, Pradipkumar Dixit, R. Hari Krishna, K. Ramakrishna Murthy\",\"doi\":\"10.3103/S1068375523040154\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p>Composite insulators are popular choice in contemporary power industry due to their numerous advantages. When these insulators are subject to various stresses, their performance gets affected due to the material degradation. One of the methods to improve the material property is to incorporate inorganic nanofillers. In this work, aluminum oxide nanofillers, synthesized in the laboratory using a solution combustion process were used and studied. The nano range was ascertained with X-ray diffraction. Those fillers were mixed in the silicone rubber specimens in 0, 1, 3, and 5 wt % concentrations. They were more rapidly aged under UV radiation, temperature, humidity and electric stresses. Dry and wet flashover tests were carried out on both virgin and aged samples, and the results showed that the concentration of 3 wt % offered a better breakdown voltage. Fourier transform infrared spectroscopy revealed percentage variations in the properties of the aged specimens, the aging resistance, degradation resistance, hydrophobicity, oxidation resistance, and erosion resistance were significantly better in 3 wt % Al<sub>2</sub>O<sub>3</sub> filled samples. Scanning electron microscopy with energy dispersive X-ray spectroscopy images showed that at 3 wt % concentration there was a fairly uniform distribution of nanofillers in the silicone base and there was the least ingress of water at same weight percentage of specimens. Their improvements in the insulation property is primarily attributed to the fair distribution of nano Al<sub>2</sub>O<sub>3</sub> fillers into the silicone base, a good Si–CH<sub>3</sub> bond structure, a low carbon cross linking and good percolation, which makes them the best candidates for outdoor insulation of power systems.</p>\",\"PeriodicalId\":782,\"journal\":{\"name\":\"Surface Engineering and Applied Electrochemistry\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.9000,\"publicationDate\":\"2023-09-04\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Surface Engineering and Applied Electrochemistry\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://link.springer.com/article/10.3103/S1068375523040154\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q3\",\"JCRName\":\"Engineering\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Surface Engineering and Applied Electrochemistry","FirstCategoryId":"1085","ListUrlMain":"https://link.springer.com/article/10.3103/S1068375523040154","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"Engineering","Score":null,"Total":0}
Experimental Investigation of Nano Al2O3 Filled Silicone Rubber Specimen Used in Outdoor Insulation
Composite insulators are popular choice in contemporary power industry due to their numerous advantages. When these insulators are subject to various stresses, their performance gets affected due to the material degradation. One of the methods to improve the material property is to incorporate inorganic nanofillers. In this work, aluminum oxide nanofillers, synthesized in the laboratory using a solution combustion process were used and studied. The nano range was ascertained with X-ray diffraction. Those fillers were mixed in the silicone rubber specimens in 0, 1, 3, and 5 wt % concentrations. They were more rapidly aged under UV radiation, temperature, humidity and electric stresses. Dry and wet flashover tests were carried out on both virgin and aged samples, and the results showed that the concentration of 3 wt % offered a better breakdown voltage. Fourier transform infrared spectroscopy revealed percentage variations in the properties of the aged specimens, the aging resistance, degradation resistance, hydrophobicity, oxidation resistance, and erosion resistance were significantly better in 3 wt % Al2O3 filled samples. Scanning electron microscopy with energy dispersive X-ray spectroscopy images showed that at 3 wt % concentration there was a fairly uniform distribution of nanofillers in the silicone base and there was the least ingress of water at same weight percentage of specimens. Their improvements in the insulation property is primarily attributed to the fair distribution of nano Al2O3 fillers into the silicone base, a good Si–CH3 bond structure, a low carbon cross linking and good percolation, which makes them the best candidates for outdoor insulation of power systems.
期刊介绍:
Surface Engineering and Applied Electrochemistry is a journal that publishes original and review articles on theory and applications of electroerosion and electrochemical methods for the treatment of materials; physical and chemical methods for the preparation of macro-, micro-, and nanomaterials and their properties; electrical processes in engineering, chemistry, and methods for the processing of biological products and food; and application electromagnetic fields in biological systems.