Celiane Mc Tapety, Yvina Kp Carneiro, Yarina M Chagas, Lidiane C Souza, Nayara de O Souza, Lidia Ar Valadas
{"title":"具有先进聚合体系的商业复合材料的转化率和机械性能。","authors":"Celiane Mc Tapety, Yvina Kp Carneiro, Yarina M Chagas, Lidiane C Souza, Nayara de O Souza, Lidia Ar Valadas","doi":"10.54589/aol.36/2/112","DOIUrl":null,"url":null,"abstract":"<p><p>Advanced Polymerization System (APS) technology in a commercial composite resin enables reduction of the concentration of camphorquinone without altering composite physicochemical properties.</p><p><strong>Aim: </strong>The aim of this study was to evaluate the degree of conversion and mechanical properties of a commercial composite with an advanced polymerization system (APS) and compare it to other composites that do not use this system.</p><p><strong>Materials and method: </strong>Five groups were analyzed. Group 1 (VT: Vittra APS - FGM); G2 (AU: Aura - SDI); G3 (ES: Quick Sigma Stelite - TOKOYAMA); G4 (FZ: Filtek Z350 XT - 3M ESPE); G5 (OP: Opallis -FGM). Degree of conversion (DC, n=3) was analyzed immediately and after 24h by analysis with FTIR spectroscopy. For Knoop hardness (KHN, n=3), 5 indentations were made at the top and bottom of specimens 2 mm thick. Flexural strength (FS, n=10) was determined by the three-point method in a universal testing machine. Polymerization stress (PS) was determined by light-curing the material (1.0 mm high) between polymethylmethacrylate rods in a universal testing machine. Light curing was performed with a Valo Cordless LED (1,000 mW/cm2 x 20 s: 20J). The results were analyzed using ANOVA and complemented by Tukey's test (α=0.05).</p><p><strong>Results: </strong>The highest DC values (immediate and 24h after) were observed for VT and OP resins, followed by FZ, AU and ES. FZ (top and bottom) had the highest KHN values, similar to VT top. AU, ES, OP and VT had statistically different KHN between their top and bottom surfaces. The highest RF values were observed for FZ, followed by OP/VT, ES and AU. The highest TP values were observed for FZ, OP and VT.</p><p><strong>Conclusion: </strong>The Vittra APS resin with a new polymerization system presents satisfactory performance for the parameters evaluated.</p>","PeriodicalId":93853,"journal":{"name":"Acta odontologica latinoamericana : AOL","volume":"36 2","pages":"112-119"},"PeriodicalIF":0.0000,"publicationDate":"2023-08-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://ftp.ncbi.nlm.nih.gov/pub/pmc/oa_pdf/0a/eb/1852-4834-36-2-112.PMC10557085.pdf","citationCount":"1","resultStr":"{\"title\":\"Degree of Conversion and Mechanical Properties of a Commercial Composite with an Advanced Polymerization System.\",\"authors\":\"Celiane Mc Tapety, Yvina Kp Carneiro, Yarina M Chagas, Lidiane C Souza, Nayara de O Souza, Lidia Ar Valadas\",\"doi\":\"10.54589/aol.36/2/112\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p><p>Advanced Polymerization System (APS) technology in a commercial composite resin enables reduction of the concentration of camphorquinone without altering composite physicochemical properties.</p><p><strong>Aim: </strong>The aim of this study was to evaluate the degree of conversion and mechanical properties of a commercial composite with an advanced polymerization system (APS) and compare it to other composites that do not use this system.</p><p><strong>Materials and method: </strong>Five groups were analyzed. Group 1 (VT: Vittra APS - FGM); G2 (AU: Aura - SDI); G3 (ES: Quick Sigma Stelite - TOKOYAMA); G4 (FZ: Filtek Z350 XT - 3M ESPE); G5 (OP: Opallis -FGM). Degree of conversion (DC, n=3) was analyzed immediately and after 24h by analysis with FTIR spectroscopy. For Knoop hardness (KHN, n=3), 5 indentations were made at the top and bottom of specimens 2 mm thick. Flexural strength (FS, n=10) was determined by the three-point method in a universal testing machine. Polymerization stress (PS) was determined by light-curing the material (1.0 mm high) between polymethylmethacrylate rods in a universal testing machine. Light curing was performed with a Valo Cordless LED (1,000 mW/cm2 x 20 s: 20J). The results were analyzed using ANOVA and complemented by Tukey's test (α=0.05).</p><p><strong>Results: </strong>The highest DC values (immediate and 24h after) were observed for VT and OP resins, followed by FZ, AU and ES. FZ (top and bottom) had the highest KHN values, similar to VT top. AU, ES, OP and VT had statistically different KHN between their top and bottom surfaces. The highest RF values were observed for FZ, followed by OP/VT, ES and AU. The highest TP values were observed for FZ, OP and VT.</p><p><strong>Conclusion: </strong>The Vittra APS resin with a new polymerization system presents satisfactory performance for the parameters evaluated.</p>\",\"PeriodicalId\":93853,\"journal\":{\"name\":\"Acta odontologica latinoamericana : AOL\",\"volume\":\"36 2\",\"pages\":\"112-119\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2023-08-31\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://ftp.ncbi.nlm.nih.gov/pub/pmc/oa_pdf/0a/eb/1852-4834-36-2-112.PMC10557085.pdf\",\"citationCount\":\"1\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Acta odontologica latinoamericana : AOL\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.54589/aol.36/2/112\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Acta odontologica latinoamericana : AOL","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.54589/aol.36/2/112","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 1
摘要
商业复合树脂中的先进聚合系统(APS)技术能够在不改变复合物物理化学性质的情况下降低樟脑醌的浓度。目的:本研究的目的是评估具有先进聚合体系(APS)的商业复合材料的转化率和机械性能,并将其与其他不使用该体系的复合材料进行比较。材料与方法:对5组患者进行分析。第1组(VT:Vittra APS-FGM);G2(AU:Aura-SDI);G3(ES:Quick Sigma钨铬钴合金-东京);G4(FZ:Filtek Z350 XT-3M ESPE);G5(OP:蛋白石-女性生殖器切割)。立即和24小时后通过FTIR光谱分析来分析转化度(DC,n=3)。对于努氏硬度(KHN,n=3),在2mm厚的试样的顶部和底部形成5个压痕。弯曲强度(FS,n=10)在通用试验机中通过三点法测定。聚合应力(PS)是通过在通用试验机中使聚甲基丙烯酸甲酯棒之间的材料(1.0mm高)光固化来测定的。使用Valo无绳LED(1000mW/cm2 x 20s:20J)进行光固化。结果:VT和OP树脂的DC值最高(立即和24小时后),其次是FZ、AU和ES。FZ(顶部和底部)的KHN值最高,与VT顶部相似。AU、ES、OP和VT在其顶面和底面之间具有统计学上不同的KHN。FZ的RF值最高,其次是OP/VT、ES和AU。FZ、OP和VT的TP值最高。
Degree of Conversion and Mechanical Properties of a Commercial Composite with an Advanced Polymerization System.
Advanced Polymerization System (APS) technology in a commercial composite resin enables reduction of the concentration of camphorquinone without altering composite physicochemical properties.
Aim: The aim of this study was to evaluate the degree of conversion and mechanical properties of a commercial composite with an advanced polymerization system (APS) and compare it to other composites that do not use this system.
Materials and method: Five groups were analyzed. Group 1 (VT: Vittra APS - FGM); G2 (AU: Aura - SDI); G3 (ES: Quick Sigma Stelite - TOKOYAMA); G4 (FZ: Filtek Z350 XT - 3M ESPE); G5 (OP: Opallis -FGM). Degree of conversion (DC, n=3) was analyzed immediately and after 24h by analysis with FTIR spectroscopy. For Knoop hardness (KHN, n=3), 5 indentations were made at the top and bottom of specimens 2 mm thick. Flexural strength (FS, n=10) was determined by the three-point method in a universal testing machine. Polymerization stress (PS) was determined by light-curing the material (1.0 mm high) between polymethylmethacrylate rods in a universal testing machine. Light curing was performed with a Valo Cordless LED (1,000 mW/cm2 x 20 s: 20J). The results were analyzed using ANOVA and complemented by Tukey's test (α=0.05).
Results: The highest DC values (immediate and 24h after) were observed for VT and OP resins, followed by FZ, AU and ES. FZ (top and bottom) had the highest KHN values, similar to VT top. AU, ES, OP and VT had statistically different KHN between their top and bottom surfaces. The highest RF values were observed for FZ, followed by OP/VT, ES and AU. The highest TP values were observed for FZ, OP and VT.
Conclusion: The Vittra APS resin with a new polymerization system presents satisfactory performance for the parameters evaluated.