聚烷氧基取代的亚硝基二苯乙烯在合成薄片蛋白类似物中的应用。薄层素H的形式合成

IF 1.7 4区化学 Q3 CHEMISTRY, MULTIDISCIPLINARY

Russian Chemical Bulletin Pub Date : 2023-09-26 DOI:10.1007/s11172-023-4003-y

E. A. Silyanova, A. S. Maksimenko, M. D. Brunner, I. A. Koblov, V. P. Kislyi, A. V. Samet, V. V. Semenov

引用次数: 0

摘要

通过6,7-二甲氧基异喹啉叶立德与五甲氧基取代的亚硝基二苯乙烯的1,3-偶极环加成，然后在中间体环加成物中闭合内酯环，制备了片状D三甲基醚。这种方法允许正式合成薄片蛋白H。

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Polyalkoxy-substituted nitrostilbenes in the synthesis of lamellarin analogs. Formal synthesis of lamellarin H

Lamellarin D trimethyl ether was prepared by 1,3-dipolar cycloaddition of 6,7-dimethoxyisoquinolinium ylide to pentamethoxy-substituted nitrostilbene followed by a lactone ring closure in the intermediate cycloadduct. This approach allowed a formal synthesis of lamellarin H.

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来源期刊

Russian Chemical Bulletin 化学-化学综合

CiteScore

2.70

自引率

47.10%

发文量

257

审稿时长

3-8 weeks

期刊介绍： Publishing nearly 500 original articles a year, by leading Scientists from Russia and throughout the world, Russian Chemical Bulletin is a prominent international journal. The coverage of the journal spans practically all areas of fundamental chemical research and is presented in five sections: General and Inorganic Chemistry; Physical Chemistry; Organic Chemistry; Organometallic Chemistry; Chemistry of Natural Compounds and Bioorganic Chemistry.