{"title":"一锅微波辅助合成棒状和六边形板状AgNP@Ni-BTC复合材料的潜在唾液葡萄糖传感器","authors":"Faesal Amri, Wandi Kasim, Achmad Rochliadi, Aep Patah","doi":"10.1016/j.snr.2023.100141","DOIUrl":null,"url":null,"abstract":"<div><p>Diabetes is a serious disease with a huge number of patients worldwide. Glucose levels in people with diabetes are above 6.6 mM in blood samples and 200 μM in saliva samples. Metal-organic frameworks (MOFs) have outstanding properties for glucose sensors, such as a large surface area and being rich in active sites. In this research, a silver nanoparticle@Ni-BTC (AgNP@Ni-BTC) composite was synthesized through one-pot synthesis using a microwave at 130 °C for 1 hour at 200 W. The results showed that the 4%AgNP@Ni-BTC-modified carbon paste electrode obtained better sensor performance than Ni-BTC with a limit of detection (LoD) of 14.73 μM, a sensitivity of 6584.89 μA mM<sup>−1</sup> cm<sup>−2</sup>, and a linear range of 10–1250 μM. The 4%AgNP@Ni-BTC-modified carbon paste electrode also had better stability than Ni-BTC and had good reproducibility. Glucose detection tests on salivary samples showed that the 4%AgNP@Ni-BTC-modified carbon paste electrode could be used to measure glucose levels in salivary samples.</p></div>","PeriodicalId":426,"journal":{"name":"Sensors and Actuators Reports","volume":null,"pages":null},"PeriodicalIF":6.5000,"publicationDate":"2023-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"4","resultStr":"{\"title\":\"Facile one-pot microwave-assisted synthesis of rod-like and hexagonal plate-like AgNP@Ni-BTC composites for a potential salivary glucose sensor\",\"authors\":\"Faesal Amri, Wandi Kasim, Achmad Rochliadi, Aep Patah\",\"doi\":\"10.1016/j.snr.2023.100141\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p>Diabetes is a serious disease with a huge number of patients worldwide. Glucose levels in people with diabetes are above 6.6 mM in blood samples and 200 μM in saliva samples. Metal-organic frameworks (MOFs) have outstanding properties for glucose sensors, such as a large surface area and being rich in active sites. In this research, a silver nanoparticle@Ni-BTC (AgNP@Ni-BTC) composite was synthesized through one-pot synthesis using a microwave at 130 °C for 1 hour at 200 W. The results showed that the 4%AgNP@Ni-BTC-modified carbon paste electrode obtained better sensor performance than Ni-BTC with a limit of detection (LoD) of 14.73 μM, a sensitivity of 6584.89 μA mM<sup>−1</sup> cm<sup>−2</sup>, and a linear range of 10–1250 μM. The 4%AgNP@Ni-BTC-modified carbon paste electrode also had better stability than Ni-BTC and had good reproducibility. Glucose detection tests on salivary samples showed that the 4%AgNP@Ni-BTC-modified carbon paste electrode could be used to measure glucose levels in salivary samples.</p></div>\",\"PeriodicalId\":426,\"journal\":{\"name\":\"Sensors and Actuators Reports\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":6.5000,\"publicationDate\":\"2023-06-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"4\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Sensors and Actuators Reports\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S2666053923000048\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"BIOTECHNOLOGY & APPLIED MICROBIOLOGY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Sensors and Actuators Reports","FirstCategoryId":"1085","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S2666053923000048","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"BIOTECHNOLOGY & APPLIED MICROBIOLOGY","Score":null,"Total":0}
Facile one-pot microwave-assisted synthesis of rod-like and hexagonal plate-like AgNP@Ni-BTC composites for a potential salivary glucose sensor
Diabetes is a serious disease with a huge number of patients worldwide. Glucose levels in people with diabetes are above 6.6 mM in blood samples and 200 μM in saliva samples. Metal-organic frameworks (MOFs) have outstanding properties for glucose sensors, such as a large surface area and being rich in active sites. In this research, a silver nanoparticle@Ni-BTC (AgNP@Ni-BTC) composite was synthesized through one-pot synthesis using a microwave at 130 °C for 1 hour at 200 W. The results showed that the 4%AgNP@Ni-BTC-modified carbon paste electrode obtained better sensor performance than Ni-BTC with a limit of detection (LoD) of 14.73 μM, a sensitivity of 6584.89 μA mM−1 cm−2, and a linear range of 10–1250 μM. The 4%AgNP@Ni-BTC-modified carbon paste electrode also had better stability than Ni-BTC and had good reproducibility. Glucose detection tests on salivary samples showed that the 4%AgNP@Ni-BTC-modified carbon paste electrode could be used to measure glucose levels in salivary samples.
期刊介绍：
Sensors and Actuators Reports is a peer-reviewed open access journal launched out from the Sensors and Actuators journal family. Sensors and Actuators Reports is dedicated to publishing new and original works in the field of all type of sensors and actuators, including bio-, chemical-, physical-, and nano- sensors and actuators, which demonstrates significant progress beyond the current state of the art. The journal regularly publishes original research papers, reviews, and short communications.
For research papers and short communications, the journal aims to publish the new and original work supported by experimental results and as such purely theoretical works are not accepted.
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