共沉淀法合成纳米填料增强普通玻璃离子水泥的表面粗糙度和颜色稳定性。

IF 4.5 Q3 MATERIALS SCIENCE, BIOMATERIALS
International Journal of Biomaterials Pub Date : 2026-04-30 eCollection Date: 2026-01-01 DOI:10.1155/ijbm/4952239
Neven S Aref
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引用次数: 0

摘要

目的:利用纳米填料对常规玻璃离子水门合剂(GIC)进行改性是提高其临床性能的一种很有前途的方法。以70:30羟基磷灰石/壳聚糖(HA/CTS)纳米复合材料改性后的常规GIC为材料,考察其表面粗糙度和颜色稳定性。材料与方法:合成了一种70:30的羟基磷灰石/壳聚糖纳米复合材料,并以1、3、5 wt.%的比例加入到GIC粉末中。设4组:第一组(对照组),第二组(1只)。% HA/CTS),第三组(3 wt。% HA/CTS), IV组(5 wt。% HA / CTS)。共制作80个标本(每组10个)。使用轮廓仪测量表面粗糙度(Ra),使用分光光度计评估颜色稳定性(ΔE)。数据分析采用单因素方差分析和Tukey事后检验(α = 0.05)。结果:用3 wt修饰GIC。% HA/CTS纳米复合材料具有最低的表面粗糙度和临床可接受的颜色变化(ΔE≤3.3)(p < 0.05)。更高的纳米复合材料负载(5 wt.%)导致表面粗糙度显著增加和临床可感知的颜色改变。结论:合并3wt。% 70:30 HA/CTS纳米复合材料在常规GIC中产生了更光滑的表面和可接受的美观结果,表明有希望改善临床性能的配方。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Surface Roughness and Color Stability of Conventional Glass Ionomer Cement Reinforced With a Nanofiller Synthesized by the Coprecipitation Method.

Aim: Modification of conventional glass ionomer cement (GIC) using nanofillers is a promising approach to enhance its clinical performance. This study aimed to evaluate the surface roughness and color stability of conventional GIC after modification with a synthesized 70:30 hydroxyapatite/chitosan (HA/CTS) nanocomposite.

Materials and methods: A 70:30 hydroxyapatite/chitosan nanocomposite was synthesized and incorporated into GIC powder at 1, 3, and 5 wt.%. Four groups were prepared: Group I (control), Group II (1 wt.% HA/CTS), Group III (3 wt.% HA/CTS), and Group IV (5 wt.% HA/CTS). A total of 80 specimens were fabricated (n = 10 per group for each test). Surface roughness (Ra) was measured using a profilometer, while color stability (ΔE) was assessed using a spectrophotometer. Data were analyzed using one-way ANOVA followed by Tukey's post hoc test (α = 0.05).

Results: GIC modified with the 3 wt.% HA/CTS nanocomposite exhibited the lowest surface roughness and demonstrated clinically acceptable color change (ΔE ≤ 3.3) (p < 0.05). Higher nanocomposite loading (5 wt.%) resulted in significantly increased surface roughness and clinically perceptible color alteration.

Conclusions: Incorporation of the 3 wt.% 70:30 HA/CTS nanocomposite into conventional GIC produced a smoother surface and acceptable esthetic outcome, suggesting a promising formulation for improved clinical performance.

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来源期刊
International Journal of Biomaterials
International Journal of Biomaterials MATERIALS SCIENCE, BIOMATERIALS-
CiteScore
4.30
自引率
3.20%
发文量
50
审稿时长
21 weeks
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