{"title":"硬质合金表面宏观和微观性能的微观组织和涂层制备工艺策略研究","authors":"Pei Han , Shucai Yang , Zekang Ren","doi":"10.1016/j.ijrmhm.2025.107503","DOIUrl":null,"url":null,"abstract":"<div><div>Surface coating and micro-texture technologies can act synergistically to enhance the performance of cutting tools. However, the strengthening mechanisms and the influence of composite processes on the surface properties of tool materials still require comprehensive investigation from a microstructural perspective. In this study, X-ray diffraction (XRD), energy-dispersive spectroscopy (EDS), Vickers microhardness testing, friction and wear test, and nanoindentation techniques are employed to elucidate the regulation mechanisms of macro- and micro-scale surface properties of cemented carbide induced by the combined preparation process of micro-texture and coating. The findings indicate that when micro-texture is performed prior to coating deposition, the samples exhibit notable advantages in surface morphology, grain refinement, coating resistance to plastic deformation, microhardness, and tribological performance. Compared with non-textured coated sample, the grain size, coating resistance to plastic deformation, coating microhardness, friction force, and wear rate improved by 24 %, 20 %, 14 %, 13 %, and 36 %, respectively. Adhesive wear is identified as the dominant wear mechanism, and it is further demonstrated that the fractal dimension of wear surface images provides a quantitative metric for characterizing the extent of surface damage.</div></div>","PeriodicalId":14216,"journal":{"name":"International Journal of Refractory Metals & Hard Materials","volume":"135 ","pages":"Article 107503"},"PeriodicalIF":4.6000,"publicationDate":"2025-10-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Research on micro-texture and coating preparation process strategy for macro and micro properties of cemented carbide surface\",\"authors\":\"Pei Han , Shucai Yang , Zekang Ren\",\"doi\":\"10.1016/j.ijrmhm.2025.107503\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>Surface coating and micro-texture technologies can act synergistically to enhance the performance of cutting tools. However, the strengthening mechanisms and the influence of composite processes on the surface properties of tool materials still require comprehensive investigation from a microstructural perspective. In this study, X-ray diffraction (XRD), energy-dispersive spectroscopy (EDS), Vickers microhardness testing, friction and wear test, and nanoindentation techniques are employed to elucidate the regulation mechanisms of macro- and micro-scale surface properties of cemented carbide induced by the combined preparation process of micro-texture and coating. The findings indicate that when micro-texture is performed prior to coating deposition, the samples exhibit notable advantages in surface morphology, grain refinement, coating resistance to plastic deformation, microhardness, and tribological performance. Compared with non-textured coated sample, the grain size, coating resistance to plastic deformation, coating microhardness, friction force, and wear rate improved by 24 %, 20 %, 14 %, 13 %, and 36 %, respectively. Adhesive wear is identified as the dominant wear mechanism, and it is further demonstrated that the fractal dimension of wear surface images provides a quantitative metric for characterizing the extent of surface damage.</div></div>\",\"PeriodicalId\":14216,\"journal\":{\"name\":\"International Journal of Refractory Metals & Hard Materials\",\"volume\":\"135 \",\"pages\":\"Article 107503\"},\"PeriodicalIF\":4.6000,\"publicationDate\":\"2025-10-20\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"International Journal of Refractory Metals & Hard Materials\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S0263436825004688\",\"RegionNum\":2,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"MATERIALS SCIENCE, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"International Journal of Refractory Metals & Hard Materials","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0263436825004688","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
Research on micro-texture and coating preparation process strategy for macro and micro properties of cemented carbide surface
Surface coating and micro-texture technologies can act synergistically to enhance the performance of cutting tools. However, the strengthening mechanisms and the influence of composite processes on the surface properties of tool materials still require comprehensive investigation from a microstructural perspective. In this study, X-ray diffraction (XRD), energy-dispersive spectroscopy (EDS), Vickers microhardness testing, friction and wear test, and nanoindentation techniques are employed to elucidate the regulation mechanisms of macro- and micro-scale surface properties of cemented carbide induced by the combined preparation process of micro-texture and coating. The findings indicate that when micro-texture is performed prior to coating deposition, the samples exhibit notable advantages in surface morphology, grain refinement, coating resistance to plastic deformation, microhardness, and tribological performance. Compared with non-textured coated sample, the grain size, coating resistance to plastic deformation, coating microhardness, friction force, and wear rate improved by 24 %, 20 %, 14 %, 13 %, and 36 %, respectively. Adhesive wear is identified as the dominant wear mechanism, and it is further demonstrated that the fractal dimension of wear surface images provides a quantitative metric for characterizing the extent of surface damage.
期刊介绍:
The International Journal of Refractory Metals and Hard Materials (IJRMHM) publishes original research articles concerned with all aspects of refractory metals and hard materials. Refractory metals are defined as metals with melting points higher than 1800 °C. These are tungsten, molybdenum, chromium, tantalum, niobium, hafnium, and rhenium, as well as many compounds and alloys based thereupon. Hard materials that are included in the scope of this journal are defined as materials with hardness values higher than 1000 kg/mm2, primarily intended for applications as manufacturing tools or wear resistant components in mechanical systems. Thus they encompass carbides, nitrides and borides of metals, and related compounds. A special focus of this journal is put on the family of hardmetals, which is also known as cemented tungsten carbide, and cermets which are based on titanium carbide and carbonitrides with or without a metal binder. Ceramics and superhard materials including diamond and cubic boron nitride may also be accepted provided the subject material is presented as hard materials as defined above.