天然果汁中抗坏血酸现场检测的纳米功能化纸上光学传感平台设计。

IF 3.3 4区 生物学 Q3 BIOCHEMISTRY & MOLECULAR BIOLOGY
Hussana Chaman, Seham J F Alanazi, Muhammad Umer Farooq, Muhammad Nasir, Silvana Andreescu, Akhtar Hayat
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引用次数: 0

摘要

采用一种快速、简单的传感器方法,将二硫化钼和银基多金属氧酸盐(MoS2-Ag-POM)吸附在纤维素纳米纸上,进行了抗坏血酸的光学检测。这种分析抗坏血酸的检测方法不需要任何产生信号的染料。采用水热法制备了MoS2和Ag-POM。采用傅里叶变换红外(FT-IR)光谱分析、动态光散射(DLS)、场发射扫描电镜(FE-SEM)、紫外吸收光谱和x射线衍射(XRD)对材料和改性纳米纸表面进行了表征。将MoS2-Ag-POM复合材料通过溶胶-凝胶的方式嵌入到纤维素纳米纸传感器上。当暴露在抗坏血酸中时,改性的纤维素纳米纸传感器会变成天蓝色。基于这些改性纤维素纳米纸传感器的分析定量是通过使用一个Capsure Pantone比色阅读器进行的。纤维素纳米纸传感器的光反射率值(LRV)与被分析物浓度在0.19 ~ 780µM范围内呈较强的线性相关,检出限为0.097µM。所设计的纤维素纳米纸传感器价格合理,快速,目标选择性强,可用于果汁样品等食品中的抗坏血酸分析。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Design of a Nano-Functionalized Lab-on-Paper Optical Sensing Platform for On-Site Detection of Ascorbic Acid in Natural Fruit Juices.

The optical detection of ascorbic acid was carried out using a quick and simple sensor-based approach designed by adsorbing molybdenum disulfide and silver-based polyoxometalates (MoS2-Ag-POM) on cellulose nanopaper strips. This detection method for the analysis of ascorbic acid does not require any signal-generating dye. MoS2 and Ag-POM were prepared by a hydrothermal procedure. The material and modified nanopaper surface were characterized by Fourier transform infrared (FT-IR) spectroscopy analysis, dynamic light scattering (DLS), field emission scanning electron microscopy (FE-SEM), UV absorption spectra, and X-ray diffraction (XRD). The MoS2-Ag-POM composite was embedded on the cellulose nano-enabled paper sensors by incorporating silica sol-gel. The modified cellulose nano-enabled paper sensors turned sky blue when exposed to ascorbic acid. The analytical quantification based on these modified cellulose nano-enabled paper sensors was performed by using a Capsure Pantone colorimetric reader. The cellulose nano-enabled paper sensor showed a strong linear correlation between light reflectance values (LRV) and the level of analyte ranging from 0.19 to 780 µM and presented a detection limit of 0.097 µM. The designed cellulose nano-enabled paper sensor was affordable, quick, and target-selective for ascorbic acid analysis in food products like fruit juice samples.

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来源期刊
Applied Biochemistry and Biotechnology
Applied Biochemistry and Biotechnology 工程技术-生化与分子生物学
CiteScore
5.70
自引率
6.70%
发文量
460
审稿时长
5.3 months
期刊介绍: This journal is devoted to publishing the highest quality innovative papers in the fields of biochemistry and biotechnology. The typical focus of the journal is to report applications of novel scientific and technological breakthroughs, as well as technological subjects that are still in the proof-of-concept stage. Applied Biochemistry and Biotechnology provides a forum for case studies and practical concepts of biotechnology, utilization, including controls, statistical data analysis, problem descriptions unique to a particular application, and bioprocess economic analyses. The journal publishes reviews deemed of interest to readers, as well as book reviews, meeting and symposia notices, and news items relating to biotechnology in both the industrial and academic communities. In addition, Applied Biochemistry and Biotechnology often publishes lists of patents and publications of special interest to readers.
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