Shiyuan Xu , Jing Xu , Bo Guan , Xuan Luo , Dikai Guan , Xuejian Li , Huihui Yu , Jiahao Wang , Qiang Hu , Yunchang Xin
{"title":"挤压温度和速度对Mg-Zn-Gd合金织构演变的影响及其与力学性能的关系","authors":"Shiyuan Xu , Jing Xu , Bo Guan , Xuan Luo , Dikai Guan , Xuejian Li , Huihui Yu , Jiahao Wang , Qiang Hu , Yunchang Xin","doi":"10.1016/j.msea.2025.149183","DOIUrl":null,"url":null,"abstract":"<div><div>It is generally believed that the addition of rare earth (RE) elements can modify the texture distribution to form a distinct RE texture, which is typically weaker and more dispersed than conventional textures. In this study, we systematically investigated the influence of extrusion temperature and speed synergy on grain boundary segregation and texture evolution in Mg-2Zn-1Gd (wt.%) alloy. Further investigation using Electron Backscattered Diffraction (EBSD) and Energy Dispersive Spectroscopy (EDS) in Scanning transmission electron microscopy mode (STEM-EDS) revealed that rare earth magnesium alloys (Mg-RE alloys) do not invariably result in the formation of RE textures, that is under low-temperature and low-speed conditions, Zn/Gd co-segregation dominates RE texture formation by increasing the critical strain for dynamic recrystallization and promoting the nucleation of twins and shear bands. Under high-temperature and high-speed conditions, an imbalance in segregation kinetics (grain boundary migration rate > solute diffusion rate) activates basal slip. This basal slip is activated within recrystallized grains to accommodate imposed strain, contributing to the development of a strong basal texture. In addition, the effect of microstructure evolution with extrusion parameters on mechanical properties of Mg-2Zn-1Gd rods are also systematically investigated, and a numerical calculation are conducted to determine the mechanism on the effect of texture evolution on mechanical properties.</div></div>","PeriodicalId":385,"journal":{"name":"Materials Science and Engineering: A","volume":"947 ","pages":"Article 149183"},"PeriodicalIF":7.0000,"publicationDate":"2025-09-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Effect of extrusion temperature and speed on texture evolution in Mg-Zn-Gd alloy and their correlation with mechanical properties\",\"authors\":\"Shiyuan Xu , Jing Xu , Bo Guan , Xuan Luo , Dikai Guan , Xuejian Li , Huihui Yu , Jiahao Wang , Qiang Hu , Yunchang Xin\",\"doi\":\"10.1016/j.msea.2025.149183\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>It is generally believed that the addition of rare earth (RE) elements can modify the texture distribution to form a distinct RE texture, which is typically weaker and more dispersed than conventional textures. In this study, we systematically investigated the influence of extrusion temperature and speed synergy on grain boundary segregation and texture evolution in Mg-2Zn-1Gd (wt.%) alloy. Further investigation using Electron Backscattered Diffraction (EBSD) and Energy Dispersive Spectroscopy (EDS) in Scanning transmission electron microscopy mode (STEM-EDS) revealed that rare earth magnesium alloys (Mg-RE alloys) do not invariably result in the formation of RE textures, that is under low-temperature and low-speed conditions, Zn/Gd co-segregation dominates RE texture formation by increasing the critical strain for dynamic recrystallization and promoting the nucleation of twins and shear bands. Under high-temperature and high-speed conditions, an imbalance in segregation kinetics (grain boundary migration rate > solute diffusion rate) activates basal slip. This basal slip is activated within recrystallized grains to accommodate imposed strain, contributing to the development of a strong basal texture. In addition, the effect of microstructure evolution with extrusion parameters on mechanical properties of Mg-2Zn-1Gd rods are also systematically investigated, and a numerical calculation are conducted to determine the mechanism on the effect of texture evolution on mechanical properties.</div></div>\",\"PeriodicalId\":385,\"journal\":{\"name\":\"Materials Science and Engineering: A\",\"volume\":\"947 \",\"pages\":\"Article 149183\"},\"PeriodicalIF\":7.0000,\"publicationDate\":\"2025-09-30\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Materials Science and Engineering: A\",\"FirstCategoryId\":\"5\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S0921509325014078\",\"RegionNum\":2,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"MATERIALS SCIENCE, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Materials Science and Engineering: A","FirstCategoryId":"5","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0921509325014078","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
Effect of extrusion temperature and speed on texture evolution in Mg-Zn-Gd alloy and their correlation with mechanical properties
It is generally believed that the addition of rare earth (RE) elements can modify the texture distribution to form a distinct RE texture, which is typically weaker and more dispersed than conventional textures. In this study, we systematically investigated the influence of extrusion temperature and speed synergy on grain boundary segregation and texture evolution in Mg-2Zn-1Gd (wt.%) alloy. Further investigation using Electron Backscattered Diffraction (EBSD) and Energy Dispersive Spectroscopy (EDS) in Scanning transmission electron microscopy mode (STEM-EDS) revealed that rare earth magnesium alloys (Mg-RE alloys) do not invariably result in the formation of RE textures, that is under low-temperature and low-speed conditions, Zn/Gd co-segregation dominates RE texture formation by increasing the critical strain for dynamic recrystallization and promoting the nucleation of twins and shear bands. Under high-temperature and high-speed conditions, an imbalance in segregation kinetics (grain boundary migration rate > solute diffusion rate) activates basal slip. This basal slip is activated within recrystallized grains to accommodate imposed strain, contributing to the development of a strong basal texture. In addition, the effect of microstructure evolution with extrusion parameters on mechanical properties of Mg-2Zn-1Gd rods are also systematically investigated, and a numerical calculation are conducted to determine the mechanism on the effect of texture evolution on mechanical properties.
期刊介绍:
Materials Science and Engineering A provides an international medium for the publication of theoretical and experimental studies related to the load-bearing capacity of materials as influenced by their basic properties, processing history, microstructure and operating environment. Appropriate submissions to Materials Science and Engineering A should include scientific and/or engineering factors which affect the microstructure - strength relationships of materials and report the changes to mechanical behavior.