用火花等离子烧结原位合成碳化物反应连接C/C复合材料

IF 2.3 4区 材料科学 Q2 MATERIALS SCIENCE, CERAMICS
Ben Chai, Xincheng Wang, Laifu Wu, Xueke Feng, Li Fu, Jian Qin
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引用次数: 0

摘要

采用火花等离子烧结的方法将C/C复合材料与Ti/Zr粉末作为中间层进行反应连接。Ti粉原位反应接头在1600℃、50 MPa、30 min条件下完成,Zr粉原位反应接头在1800℃、相同时间和压力条件下完成。两者的烧结温度均低于熔点。研究了其显微组织和力学性能。在反应节理处原位合成TiC或ZrC陶瓷夹层,相应的平均抗剪强度分别为17.78±1.23和16.56±1.14 MPa。断裂发生在C/C界面和陶瓷中间层内部,炭化不足的中心层塑性较好,有助于提高接头强度。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

In situ synthesized carbide for reaction joining C/C composites by spark plasma sintering

In situ synthesized carbide for reaction joining C/C composites by spark plasma sintering

C/C composites were reaction-joined with Ti/Zr powder as interlayer by spark plasma sintering in this study. Ti powder in situ reaction joint was achieved at 1600°C for 30 min with pressure of 50 MPa, while Zr powder in situ reaction joint was accomplished at 1800°C for the same time and pressure. Both their sintering temperature was below melting point. Microstructure and mechanical properties were investigated. TiC or ZrC ceramics interlayer were in situ synthesized in the reaction joint, corresponding average shear strength was 17.78 ± 1.23 and 16.56 ± 1.14 MPa, respectively. The fracture occurred along the C/C interface and inside the ceramics interlayer, and the center layer with inadequate carbonization contributed to joint strength due to its better plasticity.

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来源期刊
International Journal of Applied Ceramic Technology
International Journal of Applied Ceramic Technology 工程技术-材料科学:硅酸盐
CiteScore
3.90
自引率
9.50%
发文量
280
审稿时长
4.5 months
期刊介绍: The International Journal of Applied Ceramic Technology publishes cutting edge applied research and development work focused on commercialization of engineered ceramics, products and processes. The publication also explores the barriers to commercialization, design and testing, environmental health issues, international standardization activities, databases, and cost models. Designed to get high quality information to end-users quickly, the peer process is led by an editorial board of experts from industry, government, and universities. Each issue focuses on a high-interest, high-impact topic plus includes a range of papers detailing applications of ceramics. Papers on all aspects of applied ceramics are welcome including those in the following areas: Nanotechnology applications; Ceramic Armor; Ceramic and Technology for Energy Applications (e.g., Fuel Cells, Batteries, Solar, Thermoelectric, and HT Superconductors); Ceramic Matrix Composites; Functional Materials; Thermal and Environmental Barrier Coatings; Bioceramic Applications; Green Manufacturing; Ceramic Processing; Glass Technology; Fiber optics; Ceramics in Environmental Applications; Ceramics in Electronic, Photonic and Magnetic Applications;
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