还原性氧化石墨烯与纳米Fe3O4复合材料的制备与研究

IF 1.5 3区 化学 Q3 CHEMISTRY, INORGANIC & NUCLEAR
V. R. Ibragimova, I. V. Sapkov, E. I. Efremova, Z. A. Kudryashova, E. G. Rustamova, D. V. Korolev, E. I. Kunitsyna, Yu. V. Ioni
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引用次数: 0

摘要

氧化石墨烯(GO)及其复合材料常用于通过热还原或化学还原制备类石墨烯材料,而还原方法对材料的性能影响很大。本研究提出了一种以还原氧化石墨烯(rGO)为基础,表面分散平均直径为18 nm的磁铁矿纳米颗粒(NPs)制备导电复合材料的新方法。该方法是在超临界异丙醇中处理氧化石墨烯基复合材料,表面有Fe3O4。采用红外光谱、x射线粉末衍射和扫描电镜对氧化石墨烯、还原氧化石墨烯和磁铁矿NPs复合材料进行了表征。结果表明,rgo基复合材料的致密膜样品的比表面电阻率为22 Ω cm-2,饱和磁化强度为32.3 emu/g。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

Preparation and Investigation of Composite Based on Reduced Graphene Oxide and Fe3O4 Nanoparticles

Preparation and Investigation of Composite Based on Reduced Graphene Oxide and Fe3O4 Nanoparticles

Graphene oxide (GO) and composites based on it are often used to produce graphene-like materials by thermal or chemical reduction, and the reduction method strongly affects the properties of the materials. In this study, a new method was proposed to prepare a conductive composite based on reduced graphene oxide (rGO) with magnetite nanoparticles (NPs) with an average diameter of 18 nm dispersed on its surface. The method consisted of treating a GO-based composite with Fe3O4 on the its surface in supercritical isopropanol. The composites based on GO and rGO and magnetite NPs were investigated by FTIR spectroscopy, X-ray powder diffraction analysis, and scanning electron microscopy. It is shown that the sample compact film of the rGO-based composite has specific surface resistivity is 22 Ω cm–2 and saturation magnetisation is 32.3 emu/g.

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来源期刊
Russian Journal of Inorganic Chemistry
Russian Journal of Inorganic Chemistry 化学-无机化学与核化学
CiteScore
3.10
自引率
38.10%
发文量
237
审稿时长
3 months
期刊介绍: Russian Journal of Inorganic Chemistry is a monthly periodical that covers the following topics of research: the synthesis and properties of inorganic compounds, coordination compounds, physicochemical analysis of inorganic systems, theoretical inorganic chemistry, physical methods of investigation, chemistry of solutions, inorganic materials, and nanomaterials.
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