Xinjie Zhang, Shuai Liu, Yude Liu, Wentian Shi, Fu Zhao, Yi Liu
{"title":"选择性激光熔化制备Ti6Al4V支架:化学蚀刻对粉末去除和力学性能的影响","authors":"Xinjie Zhang, Shuai Liu, Yude Liu, Wentian Shi, Fu Zhao, Yi Liu","doi":"10.1007/s11665-024-10080-x","DOIUrl":null,"url":null,"abstract":"<div><p>Additive manufacturing is being used to produce medical orthopedic implants. However, the Ti6Al4V scaffolds formed by selective laser melting (SLM) limited by surface roughness. The chemical etching method have used to treat Ti6Al4V owing to the liquidity. The aim of this study is to investigate the effects of different concentration of hydrofluoric and nitric acids mixtures and times on the surface morphology and mechanical properties of Ti6Al4V scaffolds formed by SLM. The results showed that with the increase of concentration of etchant and times, the surface roughness decreased, and the mechanical properties decreased. Different concentration of etchant be conducive to remove the different shapes of adhering powder. As the best condition of concentration is 1:8 and the time is 16 min, the surface roughness is 8.4 μm, the adhering powder of 96% are removed. Too much time can cause overcorrosion. However, chemical etching weaken the strength of the Ti6Al4V scaffolds in comparison with an as-built structure. The addition of nitric acid can effectively prevent the degradation of mechanical properties by dissolving hydrogen.</p></div>","PeriodicalId":644,"journal":{"name":"Journal of Materials Engineering and Performance","volume":"34 13","pages":"12597 - 12611"},"PeriodicalIF":2.0000,"publicationDate":"2025-04-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Ti6Al4V Scaffolds Produced by Selective Laser Melting: Influence of Chemical Etching on Powder Removal and Mechanical Properties\",\"authors\":\"Xinjie Zhang, Shuai Liu, Yude Liu, Wentian Shi, Fu Zhao, Yi Liu\",\"doi\":\"10.1007/s11665-024-10080-x\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p>Additive manufacturing is being used to produce medical orthopedic implants. However, the Ti6Al4V scaffolds formed by selective laser melting (SLM) limited by surface roughness. The chemical etching method have used to treat Ti6Al4V owing to the liquidity. The aim of this study is to investigate the effects of different concentration of hydrofluoric and nitric acids mixtures and times on the surface morphology and mechanical properties of Ti6Al4V scaffolds formed by SLM. The results showed that with the increase of concentration of etchant and times, the surface roughness decreased, and the mechanical properties decreased. Different concentration of etchant be conducive to remove the different shapes of adhering powder. As the best condition of concentration is 1:8 and the time is 16 min, the surface roughness is 8.4 μm, the adhering powder of 96% are removed. Too much time can cause overcorrosion. However, chemical etching weaken the strength of the Ti6Al4V scaffolds in comparison with an as-built structure. The addition of nitric acid can effectively prevent the degradation of mechanical properties by dissolving hydrogen.</p></div>\",\"PeriodicalId\":644,\"journal\":{\"name\":\"Journal of Materials Engineering and Performance\",\"volume\":\"34 13\",\"pages\":\"12597 - 12611\"},\"PeriodicalIF\":2.0000,\"publicationDate\":\"2025-04-30\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Materials Engineering and Performance\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://link.springer.com/article/10.1007/s11665-024-10080-x\",\"RegionNum\":4,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q3\",\"JCRName\":\"MATERIALS SCIENCE, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Materials Engineering and Performance","FirstCategoryId":"88","ListUrlMain":"https://link.springer.com/article/10.1007/s11665-024-10080-x","RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
Ti6Al4V Scaffolds Produced by Selective Laser Melting: Influence of Chemical Etching on Powder Removal and Mechanical Properties
Additive manufacturing is being used to produce medical orthopedic implants. However, the Ti6Al4V scaffolds formed by selective laser melting (SLM) limited by surface roughness. The chemical etching method have used to treat Ti6Al4V owing to the liquidity. The aim of this study is to investigate the effects of different concentration of hydrofluoric and nitric acids mixtures and times on the surface morphology and mechanical properties of Ti6Al4V scaffolds formed by SLM. The results showed that with the increase of concentration of etchant and times, the surface roughness decreased, and the mechanical properties decreased. Different concentration of etchant be conducive to remove the different shapes of adhering powder. As the best condition of concentration is 1:8 and the time is 16 min, the surface roughness is 8.4 μm, the adhering powder of 96% are removed. Too much time can cause overcorrosion. However, chemical etching weaken the strength of the Ti6Al4V scaffolds in comparison with an as-built structure. The addition of nitric acid can effectively prevent the degradation of mechanical properties by dissolving hydrogen.
期刊介绍:
ASM International''s Journal of Materials Engineering and Performance focuses on solving day-to-day engineering challenges, particularly those involving components for larger systems. The journal presents a clear understanding of relationships between materials selection, processing, applications and performance.
The Journal of Materials Engineering covers all aspects of materials selection, design, processing, characterization and evaluation, including how to improve materials properties through processes and process control of casting, forming, heat treating, surface modification and coating, and fabrication.
Testing and characterization (including mechanical and physical tests, NDE, metallography, failure analysis, corrosion resistance, chemical analysis, surface characterization, and microanalysis of surfaces, features and fractures), and industrial performance measurement are also covered