工艺参数对选择性激光熔化Ti15Zr5Cu合金组织和性能的影响

IF 3.9 2区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING
Yao-Zong Mao, Ya-Hui Zhang, De-Chun Ren, Diao-Feng Li, Hai-Bin Ji, Hai-Chang Jiang, Chun-Guang Bai
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引用次数: 0

摘要

Ti-Zr-Cu合金因其优异的生物相容性、抗菌性能和潜在的可控力学性能而在种植体领域受到广泛关注。然而,选择性激光熔化(SLM)制备Ti-Zr-Cu合金仍面临两个关键挑战:首先,Cu元素的高导热性容易破坏熔池的凝固行为,导致无法控制的孔隙缺陷演变;其次,工艺参数对锆溶液强化和铜沉淀强化协同效应的影响尚不清楚,阻碍了对材料力学性能的精确控制。为了解决这些问题,本研究系统地阐明了能量输入对Ti15Zr5Cu合金SLM加工缺陷形成机制和强化效果的定量影响。通过全因素实验设计优化激光功率(120 ~ 200 W)和扫描速度(450 ~ 1200 mm/s),综合分析了能量输入对缺陷形貌、微观组织演变和力学性能的影响。结果表明:随着能量密度的降低,缺陷类型由球形孔隙转变为不规则孔隙,对材料的力学性能有显著影响;根据缺陷的演化趋势,确定了三个不同的能量密度区:高能量区、低能区和过渡区。在激光功率为180 W、扫描速度为1200 mm/s的最佳加工条件下,Ti15Zr5Cu合金的相对密度为99.998%,抗拉强度为1490±11 MPa,断裂伸长率为6.0%±0.5%。这些特性确保该材料满足用于上颌前牙区的窄直径种植体的高强度的严格要求。本研究为Ti-Zr-Cu合金在增材制造中的工艺性能优化提供了理论和实验支持,促进了其在高性能、抗菌牙种植体制造中的应用。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

Effect of Process Parameters on the Microstructure and Properties of Ti15Zr5Cu Alloy Fabricated via Selective Laser Melting

Effect of Process Parameters on the Microstructure and Properties of Ti15Zr5Cu Alloy Fabricated via Selective Laser Melting

Ti-Zr-Cu alloy has garnered significant attention in the field of dental implants due to its excellent biocompatibility, antibacterial properties, and potentially controllable mechanical properties. However, two critical challenges remain in the selective laser melting (SLM) fabrication of Ti-Zr-Cu alloy: First, the high thermal conductivity of the Cu element tends to destabilize the solidification behavior of the molten pool, leading to uncontrollable pore defect evolution; Second, the influence of process parameters on the synergistic effects of zirconium solution strengthening and copper precipitation strengthening is not well understood, hindering precise control over the material's mechanical properties. To address these issues, this study systematically elucidates the quantitative impact of energy input on the defect formation mechanisms and strengthening effects in the SLM processing of Ti15Zr5Cu alloy. By optimizing laser power (120–200 W) and scanning speed (450–1200 mm/s) through a full-factor experimental design, we comprehensively analyze the effects of energy input on defect morphology, microstructure evolution, and mechanical performance. The results demonstrate that as energy density decreases, defect types transition from spherical pores to irregular pores, significantly influencing mechanical properties. Based on the defect evolution trends, three distinct energy density regions are identified: the high-energy region, the low-energy region, and the transition region. Under the optimal processing conditions of a laser power of 180 W and a scanning speed of 1200 mm/s, the Ti15Zr5Cu alloy exhibits a relative density of 99.998%, a tensile strength of 1490 ± 11 MPa, and an elongation at break of 6.0% ± 0.5%. These properties ensure that the material satisfies the stringent requirements for high strength in narrow-diameter implants used in the maxilloanterior region. This study provides theoretical and experimental support for the process-property optimization of Ti-Zr-Cu alloys in additive manufacturing and promotes their application in the fabrication of high-performance, antibacterial dental implants.

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来源期刊
Acta Metallurgica Sinica-English Letters
Acta Metallurgica Sinica-English Letters METALLURGY & METALLURGICAL ENGINEERING-
CiteScore
6.60
自引率
14.30%
发文量
122
审稿时长
2 months
期刊介绍: This international journal presents compact reports of significant, original and timely research reflecting progress in metallurgy, materials science and engineering, including materials physics, physical metallurgy, and process metallurgy.
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