{"title":"用宏观表征技术分析锅炉管故障及根本原因","authors":"Beruna Baisa Muleta, Mesay Alemu Tolcha, Hirpa Gelgele Lemu","doi":"10.1007/s11085-025-10346-2","DOIUrl":null,"url":null,"abstract":"<div><p>This research investigates the boiler tube failure that was exposed to high-temperature service in the Arjo Didessa sugar factory, Ethiopia. The study aims to analyze the root cause and failure mechanisms of the water tube boiler exposed to high-temperature service for over eight years. Using a field-emission scanning electron microscope fitted with an energy-dispersive X-ray spectroscope and X-ray diffraction, the surface morphology and chemical composition of service-exposed boiler tube surface layers have been characterized. In addition, the research included the investigation of microstructural and micro hardness testing for both high-temperature service-exposed and virgin (new) tube samples. The composition analysis indicated the presence of calcium, magnesium, silicon, sodium, chlorine, and manganese, and deposit layers such as calcite and hematite (Fe<sub>2</sub>O<sub>3</sub>) were identified. This result revealed that the surface corrosion emerged from the interaction between the boiler tube surface wall materials and the boiler working environment. The metallurgical analysis result also confirmed the microstructural degradation in a boiler tube sample that was due to high-temperature service exposure for a long period. These microstructure changes brought on by exposure to high temperatures with surface oxidation during service deteriorate the mechanical strength of the material.</p></div>","PeriodicalId":724,"journal":{"name":"Oxidation of Metals","volume":"102 4","pages":""},"PeriodicalIF":1.5000,"publicationDate":"2025-07-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Analysis of Boiler Tube Failures and Root Causes Using Macroscopic Characterization Techniques\",\"authors\":\"Beruna Baisa Muleta, Mesay Alemu Tolcha, Hirpa Gelgele Lemu\",\"doi\":\"10.1007/s11085-025-10346-2\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p>This research investigates the boiler tube failure that was exposed to high-temperature service in the Arjo Didessa sugar factory, Ethiopia. The study aims to analyze the root cause and failure mechanisms of the water tube boiler exposed to high-temperature service for over eight years. Using a field-emission scanning electron microscope fitted with an energy-dispersive X-ray spectroscope and X-ray diffraction, the surface morphology and chemical composition of service-exposed boiler tube surface layers have been characterized. In addition, the research included the investigation of microstructural and micro hardness testing for both high-temperature service-exposed and virgin (new) tube samples. The composition analysis indicated the presence of calcium, magnesium, silicon, sodium, chlorine, and manganese, and deposit layers such as calcite and hematite (Fe<sub>2</sub>O<sub>3</sub>) were identified. This result revealed that the surface corrosion emerged from the interaction between the boiler tube surface wall materials and the boiler working environment. The metallurgical analysis result also confirmed the microstructural degradation in a boiler tube sample that was due to high-temperature service exposure for a long period. These microstructure changes brought on by exposure to high temperatures with surface oxidation during service deteriorate the mechanical strength of the material.</p></div>\",\"PeriodicalId\":724,\"journal\":{\"name\":\"Oxidation of Metals\",\"volume\":\"102 4\",\"pages\":\"\"},\"PeriodicalIF\":1.5000,\"publicationDate\":\"2025-07-22\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Oxidation of Metals\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://link.springer.com/article/10.1007/s11085-025-10346-2\",\"RegionNum\":3,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"METALLURGY & METALLURGICAL ENGINEERING\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Oxidation of Metals","FirstCategoryId":"88","ListUrlMain":"https://link.springer.com/article/10.1007/s11085-025-10346-2","RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"METALLURGY & METALLURGICAL ENGINEERING","Score":null,"Total":0}
Analysis of Boiler Tube Failures and Root Causes Using Macroscopic Characterization Techniques
This research investigates the boiler tube failure that was exposed to high-temperature service in the Arjo Didessa sugar factory, Ethiopia. The study aims to analyze the root cause and failure mechanisms of the water tube boiler exposed to high-temperature service for over eight years. Using a field-emission scanning electron microscope fitted with an energy-dispersive X-ray spectroscope and X-ray diffraction, the surface morphology and chemical composition of service-exposed boiler tube surface layers have been characterized. In addition, the research included the investigation of microstructural and micro hardness testing for both high-temperature service-exposed and virgin (new) tube samples. The composition analysis indicated the presence of calcium, magnesium, silicon, sodium, chlorine, and manganese, and deposit layers such as calcite and hematite (Fe2O3) were identified. This result revealed that the surface corrosion emerged from the interaction between the boiler tube surface wall materials and the boiler working environment. The metallurgical analysis result also confirmed the microstructural degradation in a boiler tube sample that was due to high-temperature service exposure for a long period. These microstructure changes brought on by exposure to high temperatures with surface oxidation during service deteriorate the mechanical strength of the material.
期刊介绍:
Oxidation of Metals is the premier source for the rapid dissemination of current research on all aspects of the science of gas-solid reactions at temperatures greater than about 400˚C, with primary focus on the high-temperature corrosion of bulk and coated systems. This authoritative bi-monthly publishes original scientific papers on kinetics, mechanisms, studies of scales from structural and morphological viewpoints, transport properties in scales, phase-boundary reactions, and much more. Articles may discuss both theoretical and experimental work related to gas-solid reactions at the surface or near-surface of a material exposed to elevated temperatures, including reactions with oxygen, nitrogen, sulfur, carbon and halogens. In addition, Oxidation of Metals publishes the results of frontier research concerned with deposit-induced attack. Review papers and short technical notes are encouraged.