二维位置敏感探测器中子实验的背景计算

IF 0.5 4区 材料科学 Q4 CRYSTALLOGRAPHY
N. N. Isakova, A. I. Kalyukanov, I. P. Makarova, V. T. Em
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引用次数: 0

摘要

提出了一种用位置敏感探测器测量和考虑单晶中子实验背景的方法。这种方法可以提高衍射反射的积分强度与标准差I/σ(I)的比值,从而补充了以前不满足条件I/σ(I) >; 3且在晶体学计算中未考虑的弱反射的实验数据集。在库尔恰托夫研究所国家研究中心IR-8反应堆的MOND衍射仪上对Cs4(HSO4)3(H2PO4)晶体结构的实验数据进行了验证。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

Accounting for the Background in a Neutron Experiment with a 2D Position-Sensitive Detector

Accounting for the Background in a Neutron Experiment with a 2D Position-Sensitive Detector

A methodology for measuring and taking into account the background in a single-crystal neutron experiment with a position-sensitive detector is proposed. This methodology makes it possible to increase the ratio of integrated intensities to the standard deviation I/σ(I) for diffraction reflections and thereby supplement the experimental dataset with weak reflections that previously did not meet the condition I/σ(I) > 3 and were not taken into account in crystallographic calculations. The methodology was tested on experimental data during structural studies of Cs4(HSO4)3(H2PO4) crystals on the MOND diffractometer at the IR-8 reactor of the National Research Centre “Kurchatov Institute.”

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来源期刊
Crystallography Reports
Crystallography Reports 化学-晶体学
CiteScore
1.10
自引率
28.60%
发文量
96
审稿时长
4-8 weeks
期刊介绍: Crystallography Reports is a journal that publishes original articles short communications, and reviews on various aspects of crystallography: diffraction and scattering of X-rays, electrons, and neutrons, determination of crystal structure of inorganic and organic substances, including proteins and other biological substances; UV-VIS and IR spectroscopy; growth, imperfect structure and physical properties of crystals; thin films, liquid crystals, nanomaterials, partially disordered systems, and the methods of studies.
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