Nurulhuda Abdullah, Nurul Hayati Yusof, Khairul Basyar Baharudin, Nur Aziah Alias, Kok Lang Mok
{"title":"响应面法制备天然橡胶薄膜的参数操纵研究","authors":"Nurulhuda Abdullah, Nurul Hayati Yusof, Khairul Basyar Baharudin, Nur Aziah Alias, Kok Lang Mok","doi":"10.1007/s42464-025-00301-w","DOIUrl":null,"url":null,"abstract":"<div><p>In this research paper, a comprehensive parameter manipulation study was conducted to investigate the challenges and opportunities involved in producing thinner natural rubber films. Employing the design of the experiment (DOE) method and response surface methodology (RSM) allowed tuning and manipulating various dipping protocols in exploring critical factors such as total solid content of the compounded latex, coagulant concentration, and dipping time. As such, the aim is to discern their individual and collective influence on film thickness and subsequently physical properties such as tensile strength and thermal ageing. In this study, the response surface refinement was conducted via central composite design (CCD) using these three factors: total solid content of the compounded latex, coagulant concentration, and dipping time. Based on the regression analysis, the optimum condition for thinner NR films with good tensile strength and ageing properties was achieved with final dipping protocols comprising 20% TSC, 5% coagulant concentration, and 5 s dipping time. The resulting responses from the validation experiments for thickness, tensile strength, and ageing were 0.073 mm, 18.11 MPa and 20.82 MPa, respectively. The implications of these findings are significant for the latex-dipped product sector, particularly in glove manufacturing. They facilitate the creation of cost-effective, thinner gloves while maintaining essential mechanical and ageing properties, which is vital for both medical and industrial uses. The result also shows that, perhaps with extra caution, RSM can be applied effectively in optimising the properties of the dipped film.</p></div>","PeriodicalId":662,"journal":{"name":"Journal of Rubber Research","volume":"28 2","pages":"239 - 253"},"PeriodicalIF":1.5000,"publicationDate":"2025-05-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Parameter manipulation study in producing thinner natural rubber films via response surface methodology\",\"authors\":\"Nurulhuda Abdullah, Nurul Hayati Yusof, Khairul Basyar Baharudin, Nur Aziah Alias, Kok Lang Mok\",\"doi\":\"10.1007/s42464-025-00301-w\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p>In this research paper, a comprehensive parameter manipulation study was conducted to investigate the challenges and opportunities involved in producing thinner natural rubber films. Employing the design of the experiment (DOE) method and response surface methodology (RSM) allowed tuning and manipulating various dipping protocols in exploring critical factors such as total solid content of the compounded latex, coagulant concentration, and dipping time. As such, the aim is to discern their individual and collective influence on film thickness and subsequently physical properties such as tensile strength and thermal ageing. In this study, the response surface refinement was conducted via central composite design (CCD) using these three factors: total solid content of the compounded latex, coagulant concentration, and dipping time. Based on the regression analysis, the optimum condition for thinner NR films with good tensile strength and ageing properties was achieved with final dipping protocols comprising 20% TSC, 5% coagulant concentration, and 5 s dipping time. The resulting responses from the validation experiments for thickness, tensile strength, and ageing were 0.073 mm, 18.11 MPa and 20.82 MPa, respectively. The implications of these findings are significant for the latex-dipped product sector, particularly in glove manufacturing. They facilitate the creation of cost-effective, thinner gloves while maintaining essential mechanical and ageing properties, which is vital for both medical and industrial uses. The result also shows that, perhaps with extra caution, RSM can be applied effectively in optimising the properties of the dipped film.</p></div>\",\"PeriodicalId\":662,\"journal\":{\"name\":\"Journal of Rubber Research\",\"volume\":\"28 2\",\"pages\":\"239 - 253\"},\"PeriodicalIF\":1.5000,\"publicationDate\":\"2025-05-15\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Rubber Research\",\"FirstCategoryId\":\"92\",\"ListUrlMain\":\"https://link.springer.com/article/10.1007/s42464-025-00301-w\",\"RegionNum\":4,\"RegionCategory\":\"化学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"POLYMER SCIENCE\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Rubber Research","FirstCategoryId":"92","ListUrlMain":"https://link.springer.com/article/10.1007/s42464-025-00301-w","RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"POLYMER SCIENCE","Score":null,"Total":0}
Parameter manipulation study in producing thinner natural rubber films via response surface methodology
In this research paper, a comprehensive parameter manipulation study was conducted to investigate the challenges and opportunities involved in producing thinner natural rubber films. Employing the design of the experiment (DOE) method and response surface methodology (RSM) allowed tuning and manipulating various dipping protocols in exploring critical factors such as total solid content of the compounded latex, coagulant concentration, and dipping time. As such, the aim is to discern their individual and collective influence on film thickness and subsequently physical properties such as tensile strength and thermal ageing. In this study, the response surface refinement was conducted via central composite design (CCD) using these three factors: total solid content of the compounded latex, coagulant concentration, and dipping time. Based on the regression analysis, the optimum condition for thinner NR films with good tensile strength and ageing properties was achieved with final dipping protocols comprising 20% TSC, 5% coagulant concentration, and 5 s dipping time. The resulting responses from the validation experiments for thickness, tensile strength, and ageing were 0.073 mm, 18.11 MPa and 20.82 MPa, respectively. The implications of these findings are significant for the latex-dipped product sector, particularly in glove manufacturing. They facilitate the creation of cost-effective, thinner gloves while maintaining essential mechanical and ageing properties, which is vital for both medical and industrial uses. The result also shows that, perhaps with extra caution, RSM can be applied effectively in optimising the properties of the dipped film.
期刊介绍:
The Journal of Rubber Research is devoted to both natural and synthetic rubbers, as well as to related disciplines. The scope of the journal encompasses all aspects of rubber from the core disciplines of biology, physics and chemistry, as well as economics. As a specialised field, rubber science includes within its niche a vast potential of innovative and value-added research areas yet to be explored. This peer reviewed publication focuses on the results of active experimental research and authoritative reviews on all aspects of rubber science.
The Journal of Rubber Research welcomes research on:
the upstream, including crop management, crop improvement and protection, and biotechnology;
the midstream, including processing and effluent management;
the downstream, including rubber engineering and product design, advanced rubber technology, latex science and technology, and chemistry and materials exploratory;
economics, including the economics of rubber production, consumption, and market analysis.
The Journal of Rubber Research serves to build a collective knowledge base while communicating information and validating the quality of research within the discipline, and bringing together work from experts in rubber science and related disciplines.
Scientists in both academia and industry involved in researching and working with all aspects of rubber will find this journal to be both source of information and a gateway for their own publications.