纯镍轧制电退火过程中电流增强再结晶和晶粒长大的行为和机制

IF 7 2区 材料科学 Q1 MATERIALS SCIENCE, MULTIDISCIPLINARY
Pao-Hsuan Yang, Meng-Chun Chiu, Hsuan-Cheng Huang, Chien-Lung Liang
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引用次数: 0

摘要

研究了轧制态纯镍的电退火诱导的金相行为和机制,重点研究了显微组织、显微硬度和电阻率之间的关系。在3.00-3.30 × 104 A/cm2下施加1小时的直流电应力可显著降低显微硬度(高达35.4%)和电阻率(高达9.9%)。综合电子背散射衍射(EBSD)分析表明,由于晶界迁移增强,晶粒逐渐再结晶和长大,表现为晶粒尺寸增大,亚晶界和低角度晶界转变为高角度晶界和Σ3 60°<;111> ATBs,残余应力消除和位错湮灭;铜型轧制织构(Copper, Brass, Goss)转变为保留S组分的立方体取向再结晶织构。微观结构和性能变化的阈值行为发生在电流密度较窄的过渡范围内。定量分析进一步揭示了正常晶界(59.2%)、ATBs(52.6%)和位错(36.1%)对显微硬度的贡献,支持了ATBs优越的热力学稳定性。采用与电退火相同热历史的比较退火基准,突出了电流应力下非热效应的主导作用。观察到的显微硬度降低的电流增强再结晶和晶粒长大主要由非热效应驱动,而热激活恢复更多地受热效应控制。最后,能量消耗估计表明,电退火比传统的热退火能耗低99%以上,取得了更好的冶金效果。这些结果表明,电退火为处理镍基金属提供了一种高效和有效的选择,在显著较低的温度下。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
The behaviors and mechanisms of current-enhanced recrystallization and grain growth in as-rolled pure nickel during electrical annealing
This study investigated the metallurgical behaviors and mechanisms induced by electrical annealing in as-rolled pure nickel, with a focus on the relationships among microstructure, micro-hardness, and electrical resistivity. Direct current stressing at 3.00–3.30 × 104 A/cm2 for 1 h induced significant micro-hardness reduction (up to 35.4 %) and electrical resistivity (up to 9.9 %). Comprehensive electron backscattered diffraction (EBSD) analyses revealed progressive recrystallization and grain growth due to enhanced grain boundary migration, characterized by grain size increase, transformation of subboundaries and low-angle grain boundaries into high-angle grain boundaries and Σ3 60°<111> ATBs, relief of residual stress and dislocation annihilation; and transformation of Copper-type rolling textures (Copper, Brass, and Goss) into Cube-oriented recrystallization texture with retained S components. Threshold behaviors for microstructure and property changes occurred at current densities in a narrow transition range. The quantitative analyses further reveal declines in the micro-hardness contributions from normal grain boundaries (59.2 %), ATBs (52.6 %), and dislocations (36.1 %), supporting superior thermodynamic stability of ATBs. Comparative thermal annealing benchmark using identical thermal history as electrical annealing highlighted the dominant role of athermal effects under electric current stressing. Current-enhanced recrystallization and grain growth for the observed micro-hardness reduction are predominantly driven by athermal effects, while thermally activated recovery is more governed by thermal effects. Finally, energy consumption estimations reveal that electrical annealing achieved superior metallurgical effects with over 99 % lower energy than conventional thermal annealing. These results suggest that electrical annealing offers a highly efficient and effective alternative for processing nickel-based metals, at significantly lower temperatures.
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来源期刊
Materials Science and Engineering: A
Materials Science and Engineering: A 工程技术-材料科学:综合
CiteScore
11.50
自引率
15.60%
发文量
1811
审稿时长
31 days
期刊介绍: Materials Science and Engineering A provides an international medium for the publication of theoretical and experimental studies related to the load-bearing capacity of materials as influenced by their basic properties, processing history, microstructure and operating environment. Appropriate submissions to Materials Science and Engineering A should include scientific and/or engineering factors which affect the microstructure - strength relationships of materials and report the changes to mechanical behavior.
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