Larissa Queiroz Minillo, Mariana Natale Fiorelli Fabiche, Vanessa Carolina Lombardi Ambrosio, Bruno César de Castro Cardoso, Altibano Ortenzi
{"title":"未处理龙葵纤维在环氧复合材料中的界面性能","authors":"Larissa Queiroz Minillo, Mariana Natale Fiorelli Fabiche, Vanessa Carolina Lombardi Ambrosio, Bruno César de Castro Cardoso, Altibano Ortenzi","doi":"10.1007/s12221-025-01047-3","DOIUrl":null,"url":null,"abstract":"<div><p>This study evaluates the potential of <i>Dracaena trifasciata</i> (DT) fibers as reinforcement in epoxy composites by analyzing mechanical, thermal, and microstructural properties. Fibers underwent water-retting and drying, and were characterized via SEM and FTIR. Composites were fabricated by vacuum infusion with 55% fiber volume fraction and tested according to ASTM D638. Two epoxy systems were investigated: a rigid matrix (LY5052) and a flexible matrix (AR324). With LY5052, DT fiber incorporation led to a 101% increase in elastic modulus but caused a 26% reduction in tensile strength, attributed to stress concentration at the fiber–matrix interface and brittle matrix behavior. In contrast, composites with AR324 exhibited a 908% increase in stiffness and nearly 1000% improvement in tensile strength, enabled by superior strain compatibility between the flexible matrix and the fiber reinforcement. TGA analysis showed thermal stability above 400 °C and ~ 5% increase in residual mass due to inorganic components in DT fibers. SEM revealed predominant fiber pull-out, 40 µm voids, and resin penetration into the fiber lumen. These findings highlight the importance of matrix selection in maximizing the mechanical potential of natural fibers. DT/epoxy composites are promising for lightweight applications, particularly when paired with ductile matrices that mitigate premature failure mechanisms.</p></div>","PeriodicalId":557,"journal":{"name":"Fibers and Polymers","volume":"26 8","pages":"3621 - 3630"},"PeriodicalIF":2.3000,"publicationDate":"2025-06-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Interface Performance of Untreated Dracaena trifasciata Fibers in Epoxy Composites\",\"authors\":\"Larissa Queiroz Minillo, Mariana Natale Fiorelli Fabiche, Vanessa Carolina Lombardi Ambrosio, Bruno César de Castro Cardoso, Altibano Ortenzi\",\"doi\":\"10.1007/s12221-025-01047-3\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p>This study evaluates the potential of <i>Dracaena trifasciata</i> (DT) fibers as reinforcement in epoxy composites by analyzing mechanical, thermal, and microstructural properties. Fibers underwent water-retting and drying, and were characterized via SEM and FTIR. Composites were fabricated by vacuum infusion with 55% fiber volume fraction and tested according to ASTM D638. Two epoxy systems were investigated: a rigid matrix (LY5052) and a flexible matrix (AR324). With LY5052, DT fiber incorporation led to a 101% increase in elastic modulus but caused a 26% reduction in tensile strength, attributed to stress concentration at the fiber–matrix interface and brittle matrix behavior. In contrast, composites with AR324 exhibited a 908% increase in stiffness and nearly 1000% improvement in tensile strength, enabled by superior strain compatibility between the flexible matrix and the fiber reinforcement. TGA analysis showed thermal stability above 400 °C and ~ 5% increase in residual mass due to inorganic components in DT fibers. SEM revealed predominant fiber pull-out, 40 µm voids, and resin penetration into the fiber lumen. These findings highlight the importance of matrix selection in maximizing the mechanical potential of natural fibers. DT/epoxy composites are promising for lightweight applications, particularly when paired with ductile matrices that mitigate premature failure mechanisms.</p></div>\",\"PeriodicalId\":557,\"journal\":{\"name\":\"Fibers and Polymers\",\"volume\":\"26 8\",\"pages\":\"3621 - 3630\"},\"PeriodicalIF\":2.3000,\"publicationDate\":\"2025-06-21\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Fibers and Polymers\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://link.springer.com/article/10.1007/s12221-025-01047-3\",\"RegionNum\":4,\"RegionCategory\":\"工程技术\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"MATERIALS SCIENCE, TEXTILES\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Fibers and Polymers","FirstCategoryId":"88","ListUrlMain":"https://link.springer.com/article/10.1007/s12221-025-01047-3","RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"MATERIALS SCIENCE, TEXTILES","Score":null,"Total":0}
Interface Performance of Untreated Dracaena trifasciata Fibers in Epoxy Composites
This study evaluates the potential of Dracaena trifasciata (DT) fibers as reinforcement in epoxy composites by analyzing mechanical, thermal, and microstructural properties. Fibers underwent water-retting and drying, and were characterized via SEM and FTIR. Composites were fabricated by vacuum infusion with 55% fiber volume fraction and tested according to ASTM D638. Two epoxy systems were investigated: a rigid matrix (LY5052) and a flexible matrix (AR324). With LY5052, DT fiber incorporation led to a 101% increase in elastic modulus but caused a 26% reduction in tensile strength, attributed to stress concentration at the fiber–matrix interface and brittle matrix behavior. In contrast, composites with AR324 exhibited a 908% increase in stiffness and nearly 1000% improvement in tensile strength, enabled by superior strain compatibility between the flexible matrix and the fiber reinforcement. TGA analysis showed thermal stability above 400 °C and ~ 5% increase in residual mass due to inorganic components in DT fibers. SEM revealed predominant fiber pull-out, 40 µm voids, and resin penetration into the fiber lumen. These findings highlight the importance of matrix selection in maximizing the mechanical potential of natural fibers. DT/epoxy composites are promising for lightweight applications, particularly when paired with ductile matrices that mitigate premature failure mechanisms.
期刊介绍:
-Chemistry of Fiber Materials, Polymer Reactions and Synthesis-
Physical Properties of Fibers, Polymer Blends and Composites-
Fiber Spinning and Textile Processing, Polymer Physics, Morphology-
Colorants and Dyeing, Polymer Analysis and Characterization-
Chemical Aftertreatment of Textiles, Polymer Processing and Rheology-
Textile and Apparel Science, Functional Polymers