R. A. Shaposhikov, V. N. Polkovonikov, N. I. Chkhalo
{"title":"碳阻挡层对Cr/V材料对多层x射线反射镜结构和反射性能影响的研究","authors":"R. A. Shaposhikov, V. N. Polkovonikov, N. I. Chkhalo","doi":"10.1134/S1027451025701022","DOIUrl":null,"url":null,"abstract":"<p>The structural parameters and reflective properties of multilayer X-ray mirrors based on a chromium–vanadium material pair were studied. These mirrors are optimized for operation in the spectral range of 2.42–2.73 nm. One of the key practical applications of such mirrors is X-ray microscopy, which enables real-time studies of biological samples. Achieving the highest possible reflectivity of X-ray mirrors is essential for maximizing the temporal resolution of such experiments. It was shown that Cr/V mirrors exhibit large interfacial transition zones (arising at layer boundaries due to intermixing and chemical interactions between materials), which reduce the reflectivity of the mirror. It was also found that the transition zones between different materials are uniform both within a single bilayer and across multiple periods of the mirror structure. To reduce the thickness of these transition zones, carbon barrier layers were introduced into the mirror structure. This approach significantly decreased the interfacial zone thickness, which in turn led to an increase in mirror reflectivity.</p>","PeriodicalId":671,"journal":{"name":"Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques","volume":"19 3","pages":"692 - 696"},"PeriodicalIF":0.4000,"publicationDate":"2025-09-25","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Study of the Effect of Carbon Barrier Layers on the Structural and Reflective Properties of Multilayer X-ray Mirrors Based on the Cr/V Material Pair\",\"authors\":\"R. A. Shaposhikov, V. N. Polkovonikov, N. I. Chkhalo\",\"doi\":\"10.1134/S1027451025701022\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p>The structural parameters and reflective properties of multilayer X-ray mirrors based on a chromium–vanadium material pair were studied. These mirrors are optimized for operation in the spectral range of 2.42–2.73 nm. One of the key practical applications of such mirrors is X-ray microscopy, which enables real-time studies of biological samples. Achieving the highest possible reflectivity of X-ray mirrors is essential for maximizing the temporal resolution of such experiments. It was shown that Cr/V mirrors exhibit large interfacial transition zones (arising at layer boundaries due to intermixing and chemical interactions between materials), which reduce the reflectivity of the mirror. It was also found that the transition zones between different materials are uniform both within a single bilayer and across multiple periods of the mirror structure. To reduce the thickness of these transition zones, carbon barrier layers were introduced into the mirror structure. This approach significantly decreased the interfacial zone thickness, which in turn led to an increase in mirror reflectivity.</p>\",\"PeriodicalId\":671,\"journal\":{\"name\":\"Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques\",\"volume\":\"19 3\",\"pages\":\"692 - 696\"},\"PeriodicalIF\":0.4000,\"publicationDate\":\"2025-09-25\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://link.springer.com/article/10.1134/S1027451025701022\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"PHYSICS, CONDENSED MATTER\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques","FirstCategoryId":"1085","ListUrlMain":"https://link.springer.com/article/10.1134/S1027451025701022","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"PHYSICS, CONDENSED MATTER","Score":null,"Total":0}
Study of the Effect of Carbon Barrier Layers on the Structural and Reflective Properties of Multilayer X-ray Mirrors Based on the Cr/V Material Pair
The structural parameters and reflective properties of multilayer X-ray mirrors based on a chromium–vanadium material pair were studied. These mirrors are optimized for operation in the spectral range of 2.42–2.73 nm. One of the key practical applications of such mirrors is X-ray microscopy, which enables real-time studies of biological samples. Achieving the highest possible reflectivity of X-ray mirrors is essential for maximizing the temporal resolution of such experiments. It was shown that Cr/V mirrors exhibit large interfacial transition zones (arising at layer boundaries due to intermixing and chemical interactions between materials), which reduce the reflectivity of the mirror. It was also found that the transition zones between different materials are uniform both within a single bilayer and across multiple periods of the mirror structure. To reduce the thickness of these transition zones, carbon barrier layers were introduced into the mirror structure. This approach significantly decreased the interfacial zone thickness, which in turn led to an increase in mirror reflectivity.
期刊介绍:
Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques publishes original articles on the topical problems of solid-state physics, materials science, experimental techniques, condensed media, nanostructures, surfaces of thin films, and phase boundaries: geometric and energetical structures of surfaces, the methods of computer simulations; physical and chemical properties and their changes upon radiation and other treatments; the methods of studies of films and surface layers of crystals (XRD, XPS, synchrotron radiation, neutron and electron diffraction, electron microscopic, scanning tunneling microscopic, atomic force microscopic studies, and other methods that provide data on the surfaces and thin films). Articles related to the methods and technics of structure studies are the focus of the journal. The journal accepts manuscripts of regular articles and reviews in English or Russian language from authors of all countries. All manuscripts are peer-reviewed.