{"title":"控制时效处理Mg-Sn二元合金中Mg2Sn动态析出的原位观察","authors":"Shujing Wu , Chong Cao , Qingjun Zhang","doi":"10.1016/j.matdes.2025.114766","DOIUrl":null,"url":null,"abstract":"<div><div>The dynamic precipitation and growth of Mg<sub>2</sub>Sn in a binary Mg-9.76wt.%Sn alloy aged in the temperature range of 180 °C-330 °C were observed in real time by applying <em>in situ</em> transmission electron microscopy techniques, showing the details where and how precipitates nucleate, grow, or dissolve. The dispersive nanoparticles were observed in the Mg matrix at 180 °C, then gradually grew to a lath-like shape on the basal plane at 240 °C-250 °C. The dynamic re-dissolution process of precipitates at the appropriate temperature of 300 °C-330 °C was observed, which was also found to mainly be related to temperature, aging time, surface tension, and vacancies. Meanwhile, a new orientation relationship between the stable precipitates and the Mg matrix was revealed. The results will give a significant insight into the microstructural factors regarding the formation of the orientation relationships, and provide a theoretical guidance for the optimization of alloy performance.</div></div>","PeriodicalId":383,"journal":{"name":"Materials & Design","volume":"259 ","pages":"Article 114766"},"PeriodicalIF":7.9000,"publicationDate":"2025-09-19","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"In situ observation of the dynamic precipitation of Mg2Sn in Mg-Sn binary alloy processed by controlled aging treatment\",\"authors\":\"Shujing Wu , Chong Cao , Qingjun Zhang\",\"doi\":\"10.1016/j.matdes.2025.114766\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>The dynamic precipitation and growth of Mg<sub>2</sub>Sn in a binary Mg-9.76wt.%Sn alloy aged in the temperature range of 180 °C-330 °C were observed in real time by applying <em>in situ</em> transmission electron microscopy techniques, showing the details where and how precipitates nucleate, grow, or dissolve. The dispersive nanoparticles were observed in the Mg matrix at 180 °C, then gradually grew to a lath-like shape on the basal plane at 240 °C-250 °C. The dynamic re-dissolution process of precipitates at the appropriate temperature of 300 °C-330 °C was observed, which was also found to mainly be related to temperature, aging time, surface tension, and vacancies. Meanwhile, a new orientation relationship between the stable precipitates and the Mg matrix was revealed. The results will give a significant insight into the microstructural factors regarding the formation of the orientation relationships, and provide a theoretical guidance for the optimization of alloy performance.</div></div>\",\"PeriodicalId\":383,\"journal\":{\"name\":\"Materials & Design\",\"volume\":\"259 \",\"pages\":\"Article 114766\"},\"PeriodicalIF\":7.9000,\"publicationDate\":\"2025-09-19\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Materials & Design\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S0264127525011864\",\"RegionNum\":2,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"MATERIALS SCIENCE, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Materials & Design","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0264127525011864","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
In situ observation of the dynamic precipitation of Mg2Sn in Mg-Sn binary alloy processed by controlled aging treatment
The dynamic precipitation and growth of Mg2Sn in a binary Mg-9.76wt.%Sn alloy aged in the temperature range of 180 °C-330 °C were observed in real time by applying in situ transmission electron microscopy techniques, showing the details where and how precipitates nucleate, grow, or dissolve. The dispersive nanoparticles were observed in the Mg matrix at 180 °C, then gradually grew to a lath-like shape on the basal plane at 240 °C-250 °C. The dynamic re-dissolution process of precipitates at the appropriate temperature of 300 °C-330 °C was observed, which was also found to mainly be related to temperature, aging time, surface tension, and vacancies. Meanwhile, a new orientation relationship between the stable precipitates and the Mg matrix was revealed. The results will give a significant insight into the microstructural factors regarding the formation of the orientation relationships, and provide a theoretical guidance for the optimization of alloy performance.
期刊介绍:
Materials and Design is a multi-disciplinary journal that publishes original research reports, review articles, and express communications. The journal focuses on studying the structure and properties of inorganic and organic materials, advancements in synthesis, processing, characterization, and testing, the design of materials and engineering systems, and their applications in technology. It aims to bring together various aspects of materials science, engineering, physics, and chemistry.
The journal explores themes ranging from materials to design and aims to reveal the connections between natural and artificial materials, as well as experiment and modeling. Manuscripts submitted to Materials and Design should contain elements of discovery and surprise, as they often contribute new insights into the architecture and function of matter.