超小银纳米颗粒的超声辅助绿色合成及其抗菌活性研究

IF 0.6 4区 化学 Q4 CHEMISTRY, APPLIED
Kim-Phuong T. Dang, Nguyen-Vu Ngo, Hong-Phuc Nguyen, T. Ngoc-Han Pham, Hieu Vu Quang, Thanh-Danh Nguyen
{"title":"超小银纳米颗粒的超声辅助绿色合成及其抗菌活性研究","authors":"Kim-Phuong T. Dang,&nbsp;Nguyen-Vu Ngo,&nbsp;Hong-Phuc Nguyen,&nbsp;T. Ngoc-Han Pham,&nbsp;Hieu Vu Quang,&nbsp;Thanh-Danh Nguyen","doi":"10.1134/S1070427225040056","DOIUrl":null,"url":null,"abstract":"<p>The green synthesis of silver nanoparticles (AgNPs) has garnered significant attention due to its eco-friendliness, safety, and time efficiency. This study explores the ultrasound-assisted synthesis of AgNPs using an aqueous extract of <i>Hopea odorata</i> (HO) and evaluates their antibacterial properties. The reaction conditions, silver ion concentration, ultrasound amplitude, and time, were optimized using UV-Vis spectroscopy, achieving nanoparticle synthesis in just 30 min. Comprehensive characterization revealed ultra-small HO-AgNPs with an average size of 2.8 nm, confirmed by SEM, TEM, FTIR, XRD, DLS, and zeta potential analyses. FTIR results suggested phenolic compounds in the extract act as stabilizing and reducing agents, while the highly negative zeta potential (–40.9 mV) indicated excellent stability. Antibacterial tests demonstrated strong activity against <i>Staphylococcus aureus</i>, <i>Bacillus cereus</i>, <i>Escherichia coli</i>, and <i>Pseudomonas aeruginosa</i>, with the highest efficacy against <i>P. aeruginosa</i>. These findings highlight HO-AgNPs as promising ultra-small nanoparticles with potent antimicrobial potential.</p>","PeriodicalId":757,"journal":{"name":"Russian Journal of Applied Chemistry","volume":"98 4","pages":"201 - 212"},"PeriodicalIF":0.6000,"publicationDate":"2025-09-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Ultrasound-Assisted Green Synthesis of Ultra-Small Silver Nanoparticles and Their Antibacterial Activity\",\"authors\":\"Kim-Phuong T. Dang,&nbsp;Nguyen-Vu Ngo,&nbsp;Hong-Phuc Nguyen,&nbsp;T. Ngoc-Han Pham,&nbsp;Hieu Vu Quang,&nbsp;Thanh-Danh Nguyen\",\"doi\":\"10.1134/S1070427225040056\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p>The green synthesis of silver nanoparticles (AgNPs) has garnered significant attention due to its eco-friendliness, safety, and time efficiency. This study explores the ultrasound-assisted synthesis of AgNPs using an aqueous extract of <i>Hopea odorata</i> (HO) and evaluates their antibacterial properties. The reaction conditions, silver ion concentration, ultrasound amplitude, and time, were optimized using UV-Vis spectroscopy, achieving nanoparticle synthesis in just 30 min. Comprehensive characterization revealed ultra-small HO-AgNPs with an average size of 2.8 nm, confirmed by SEM, TEM, FTIR, XRD, DLS, and zeta potential analyses. FTIR results suggested phenolic compounds in the extract act as stabilizing and reducing agents, while the highly negative zeta potential (–40.9 mV) indicated excellent stability. Antibacterial tests demonstrated strong activity against <i>Staphylococcus aureus</i>, <i>Bacillus cereus</i>, <i>Escherichia coli</i>, and <i>Pseudomonas aeruginosa</i>, with the highest efficacy against <i>P. aeruginosa</i>. These findings highlight HO-AgNPs as promising ultra-small nanoparticles with potent antimicrobial potential.</p>\",\"PeriodicalId\":757,\"journal\":{\"name\":\"Russian Journal of Applied Chemistry\",\"volume\":\"98 4\",\"pages\":\"201 - 212\"},\"PeriodicalIF\":0.6000,\"publicationDate\":\"2025-09-15\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Russian Journal of Applied Chemistry\",\"FirstCategoryId\":\"92\",\"ListUrlMain\":\"https://link.springer.com/article/10.1134/S1070427225040056\",\"RegionNum\":4,\"RegionCategory\":\"化学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"CHEMISTRY, APPLIED\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Russian Journal of Applied Chemistry","FirstCategoryId":"92","ListUrlMain":"https://link.springer.com/article/10.1134/S1070427225040056","RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"CHEMISTRY, APPLIED","Score":null,"Total":0}
引用次数: 0

摘要

绿色合成纳米银粒子(AgNPs)因其环保性、安全性和时间效率而受到广泛关注。本研究探讨了超声辅助下,以希望草水提物(HO)为原料合成AgNPs的方法,并对其抗菌性能进行了评价。利用紫外可见光谱对反应条件、银离子浓度、超声振幅和时间进行优化,在30 min内合成了纳米颗粒。通过SEM、TEM、FTIR、XRD、DLS和zeta电位分析,发现了平均尺寸为2.8 nm的超小HO-AgNPs。FTIR结果表明,提取物中酚类化合物具有稳定和还原作用,zeta电位为负(-40.9 mV),具有良好的稳定性。抗菌试验表明,对金黄色葡萄球菌、蜡样芽孢杆菌、大肠杆菌和铜绿假单胞菌均有较强的抑菌活性,其中对铜绿假单胞菌的抑菌效果最好。这些发现突出了HO-AgNPs是具有强大抗菌潜力的有前途的超小纳米颗粒。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

Ultrasound-Assisted Green Synthesis of Ultra-Small Silver Nanoparticles and Their Antibacterial Activity

Ultrasound-Assisted Green Synthesis of Ultra-Small Silver Nanoparticles and Their Antibacterial Activity

Ultrasound-Assisted Green Synthesis of Ultra-Small Silver Nanoparticles and Their Antibacterial Activity

The green synthesis of silver nanoparticles (AgNPs) has garnered significant attention due to its eco-friendliness, safety, and time efficiency. This study explores the ultrasound-assisted synthesis of AgNPs using an aqueous extract of Hopea odorata (HO) and evaluates their antibacterial properties. The reaction conditions, silver ion concentration, ultrasound amplitude, and time, were optimized using UV-Vis spectroscopy, achieving nanoparticle synthesis in just 30 min. Comprehensive characterization revealed ultra-small HO-AgNPs with an average size of 2.8 nm, confirmed by SEM, TEM, FTIR, XRD, DLS, and zeta potential analyses. FTIR results suggested phenolic compounds in the extract act as stabilizing and reducing agents, while the highly negative zeta potential (–40.9 mV) indicated excellent stability. Antibacterial tests demonstrated strong activity against Staphylococcus aureus, Bacillus cereus, Escherichia coli, and Pseudomonas aeruginosa, with the highest efficacy against P. aeruginosa. These findings highlight HO-AgNPs as promising ultra-small nanoparticles with potent antimicrobial potential.

求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
CiteScore
1.60
自引率
11.10%
发文量
63
审稿时长
2-4 weeks
期刊介绍: Russian Journal of Applied Chemistry (Zhurnal prikladnoi khimii) was founded in 1928. It covers all application problems of modern chemistry, including the structure of inorganic and organic compounds, kinetics and mechanisms of chemical reactions, problems of chemical processes and apparatus, borderline problems of chemistry, and applied research.
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:604180095
Book学术官方微信