电子束粉末床熔合制备不可焊镍基高温合金的微观到宏观裂纹和再结晶

IF 4.7 Q2 ENGINEERING, MANUFACTURING
Hamid Aghajani, Ehsan Toyserkani
{"title":"电子束粉末床熔合制备不可焊镍基高温合金的微观到宏观裂纹和再结晶","authors":"Hamid Aghajani,&nbsp;Ehsan Toyserkani","doi":"10.1016/j.addlet.2025.100323","DOIUrl":null,"url":null,"abstract":"<div><div>In the present study, CM247LC, a non-weldable Ni-base superalloy, was fabricated by electron beam powder bed fusion (EB-PBF) over a wide energy levels. For this purpose, variable process parameters were adjusted to investigate their effect on microstructure and crack formation. Samples fabricated at both low and high area energies exhibited pronounced crack susceptibility. At very low energy densities, lack of fusion (LoF) and porosities were observed, while higher energy densities produced denser samples. Adjustments to energy density and process parameters resulted in a grain structure transition from fine-columnar to coarse-columnar and near-single crystal morphologies. Despite these changes, the cracking issue persisted, with micro-cracks observed in low-energy samples and macro-scale cracks, several millimeters long, forming at higher energy densities, highlighting the material’s high sensitivity to crack formation. Both solidification and liquation cracking were identified— the former showing dendritic crack surfaces, and the latter associated with eutectic phases and grain boundary precipitates. Severe recrystallization around cracks was observed at high energy densities, characterized by elevated dislocation densities. EDS analysis revealed hafnium- and silicon-rich precipitates in interdendritic regions and near cracks, contributing to severe hot cracking in the material.</div></div>","PeriodicalId":72068,"journal":{"name":"Additive manufacturing letters","volume":"15 ","pages":"Article 100323"},"PeriodicalIF":4.7000,"publicationDate":"2025-09-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"From micro- to macro-cracks and recrystallization in a non-weldable Ni-based superalloy manufactured by electron beam powder bed fusion\",\"authors\":\"Hamid Aghajani,&nbsp;Ehsan Toyserkani\",\"doi\":\"10.1016/j.addlet.2025.100323\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>In the present study, CM247LC, a non-weldable Ni-base superalloy, was fabricated by electron beam powder bed fusion (EB-PBF) over a wide energy levels. For this purpose, variable process parameters were adjusted to investigate their effect on microstructure and crack formation. Samples fabricated at both low and high area energies exhibited pronounced crack susceptibility. At very low energy densities, lack of fusion (LoF) and porosities were observed, while higher energy densities produced denser samples. Adjustments to energy density and process parameters resulted in a grain structure transition from fine-columnar to coarse-columnar and near-single crystal morphologies. Despite these changes, the cracking issue persisted, with micro-cracks observed in low-energy samples and macro-scale cracks, several millimeters long, forming at higher energy densities, highlighting the material’s high sensitivity to crack formation. Both solidification and liquation cracking were identified— the former showing dendritic crack surfaces, and the latter associated with eutectic phases and grain boundary precipitates. Severe recrystallization around cracks was observed at high energy densities, characterized by elevated dislocation densities. EDS analysis revealed hafnium- and silicon-rich precipitates in interdendritic regions and near cracks, contributing to severe hot cracking in the material.</div></div>\",\"PeriodicalId\":72068,\"journal\":{\"name\":\"Additive manufacturing letters\",\"volume\":\"15 \",\"pages\":\"Article 100323\"},\"PeriodicalIF\":4.7000,\"publicationDate\":\"2025-09-11\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Additive manufacturing letters\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S2772369025000568\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"ENGINEERING, MANUFACTURING\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Additive manufacturing letters","FirstCategoryId":"1085","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S2772369025000568","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"ENGINEERING, MANUFACTURING","Score":null,"Total":0}
引用次数: 0

摘要

在本研究中,采用宽能级电子束粉末床熔合(EB-PBF)法制备了不可焊镍基高温合金CM247LC。为此,调整不同的工艺参数,研究其对显微组织和裂纹形成的影响。在低和高面积能下制备的样品都表现出明显的裂纹敏感性。在非常低的能量密度下,观察到缺乏熔合(LoF)和孔隙,而更高的能量密度产生更致密的样品。调整能量密度和工艺参数导致晶粒结构从细柱状转变为粗柱状和近单晶形态。尽管发生了这些变化,但裂纹问题仍然存在,在低能样品中观察到微裂纹,而在高能量密度下形成的宏观裂纹长达几毫米,这凸显了材料对裂纹形成的高敏感性。凝固开裂和液化开裂均被确定,前者表现为枝晶裂纹表面,后者表现为共晶相和晶界沉淀。在高能量密度下,观察到裂纹周围严重的再结晶,其特征是位错密度升高。EDS分析显示,在枝晶间区域和裂纹附近有富铪和富硅的析出物,导致材料出现严重的热裂。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
From micro- to macro-cracks and recrystallization in a non-weldable Ni-based superalloy manufactured by electron beam powder bed fusion
In the present study, CM247LC, a non-weldable Ni-base superalloy, was fabricated by electron beam powder bed fusion (EB-PBF) over a wide energy levels. For this purpose, variable process parameters were adjusted to investigate their effect on microstructure and crack formation. Samples fabricated at both low and high area energies exhibited pronounced crack susceptibility. At very low energy densities, lack of fusion (LoF) and porosities were observed, while higher energy densities produced denser samples. Adjustments to energy density and process parameters resulted in a grain structure transition from fine-columnar to coarse-columnar and near-single crystal morphologies. Despite these changes, the cracking issue persisted, with micro-cracks observed in low-energy samples and macro-scale cracks, several millimeters long, forming at higher energy densities, highlighting the material’s high sensitivity to crack formation. Both solidification and liquation cracking were identified— the former showing dendritic crack surfaces, and the latter associated with eutectic phases and grain boundary precipitates. Severe recrystallization around cracks was observed at high energy densities, characterized by elevated dislocation densities. EDS analysis revealed hafnium- and silicon-rich precipitates in interdendritic regions and near cracks, contributing to severe hot cracking in the material.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
Additive manufacturing letters
Additive manufacturing letters Materials Science (General), Industrial and Manufacturing Engineering, Mechanics of Materials
CiteScore
3.70
自引率
0.00%
发文量
0
审稿时长
37 days
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:604180095
Book学术官方微信