{"title":"高温损伤作用下砂岩渗透率特征及孔隙结构演化","authors":"Jiang-Feng Liu, Hong-Yang Ni, Xu Chen, Shi-Jia Ma, Zhi-Peng Wang, Rui-Nian Sun","doi":"10.1016/j.ijrmms.2025.106277","DOIUrl":null,"url":null,"abstract":"<div><div>This study investigates the gas permeability characteristics and pore structure evolution of fine-grained sandstone under high-temperature conditions. Sandstone specimens were subjected to temperatures ranging from 20 °C to 800 °C, followed by gas permeability, scanning electron microscopy (SEM), mercury intrusion porosimetry (MIP), and X-ray diffraction (XRD) tests. The results indicate that gas permeability demonstrates a three-stage variation with temperature: a gradual increase up to 400 °C due to the expansion of mineral grains and dehydration, a reduction from 400 °C to 600 °C associated with pore closure and microstructural collapse, and a dramatic increase beyond 600 °C driven by thermal cracking and mineral decomposition. The confining pressure significantly influenced gas permeability, exhibiting a reduction of over 90 % at pressures above 50 MPa across all temperatures. The Klinkenberg slip effect, characterized by enhanced gas flow in low-permeability pores, was prominent at low gas pressures but diminished with increasing gas pressure, suggesting critical thresholds for slip behavior under thermal effects. Porosity increased exponentially with temperature, particularly after 500 °C, as new pores and microcracks formed. Microstructural analysis revealed that high temperatures led to the transformation of kaolinite into mixed-layer illite, which played a pivotal role in altering pore structures and gas permeability. These findings provide a systematic understanding of the coupled thermal-mechanical effects on sandstone and have implications for geothermal energy extraction, underground coal gasification, and other subsurface engineering applications.</div></div>","PeriodicalId":54941,"journal":{"name":"International Journal of Rock Mechanics and Mining Sciences","volume":"195 ","pages":"Article 106277"},"PeriodicalIF":7.5000,"publicationDate":"2025-09-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Gas permeability characteristics and pore structure evolution of sandstones with high-temperature damage effects\",\"authors\":\"Jiang-Feng Liu, Hong-Yang Ni, Xu Chen, Shi-Jia Ma, Zhi-Peng Wang, Rui-Nian Sun\",\"doi\":\"10.1016/j.ijrmms.2025.106277\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>This study investigates the gas permeability characteristics and pore structure evolution of fine-grained sandstone under high-temperature conditions. Sandstone specimens were subjected to temperatures ranging from 20 °C to 800 °C, followed by gas permeability, scanning electron microscopy (SEM), mercury intrusion porosimetry (MIP), and X-ray diffraction (XRD) tests. The results indicate that gas permeability demonstrates a three-stage variation with temperature: a gradual increase up to 400 °C due to the expansion of mineral grains and dehydration, a reduction from 400 °C to 600 °C associated with pore closure and microstructural collapse, and a dramatic increase beyond 600 °C driven by thermal cracking and mineral decomposition. The confining pressure significantly influenced gas permeability, exhibiting a reduction of over 90 % at pressures above 50 MPa across all temperatures. The Klinkenberg slip effect, characterized by enhanced gas flow in low-permeability pores, was prominent at low gas pressures but diminished with increasing gas pressure, suggesting critical thresholds for slip behavior under thermal effects. Porosity increased exponentially with temperature, particularly after 500 °C, as new pores and microcracks formed. Microstructural analysis revealed that high temperatures led to the transformation of kaolinite into mixed-layer illite, which played a pivotal role in altering pore structures and gas permeability. These findings provide a systematic understanding of the coupled thermal-mechanical effects on sandstone and have implications for geothermal energy extraction, underground coal gasification, and other subsurface engineering applications.</div></div>\",\"PeriodicalId\":54941,\"journal\":{\"name\":\"International Journal of Rock Mechanics and Mining Sciences\",\"volume\":\"195 \",\"pages\":\"Article 106277\"},\"PeriodicalIF\":7.5000,\"publicationDate\":\"2025-09-11\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"International Journal of Rock Mechanics and Mining Sciences\",\"FirstCategoryId\":\"5\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S1365160925002540\",\"RegionNum\":1,\"RegionCategory\":\"工程技术\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"ENGINEERING, GEOLOGICAL\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"International Journal of Rock Mechanics and Mining Sciences","FirstCategoryId":"5","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S1365160925002540","RegionNum":1,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"ENGINEERING, GEOLOGICAL","Score":null,"Total":0}
Gas permeability characteristics and pore structure evolution of sandstones with high-temperature damage effects
This study investigates the gas permeability characteristics and pore structure evolution of fine-grained sandstone under high-temperature conditions. Sandstone specimens were subjected to temperatures ranging from 20 °C to 800 °C, followed by gas permeability, scanning electron microscopy (SEM), mercury intrusion porosimetry (MIP), and X-ray diffraction (XRD) tests. The results indicate that gas permeability demonstrates a three-stage variation with temperature: a gradual increase up to 400 °C due to the expansion of mineral grains and dehydration, a reduction from 400 °C to 600 °C associated with pore closure and microstructural collapse, and a dramatic increase beyond 600 °C driven by thermal cracking and mineral decomposition. The confining pressure significantly influenced gas permeability, exhibiting a reduction of over 90 % at pressures above 50 MPa across all temperatures. The Klinkenberg slip effect, characterized by enhanced gas flow in low-permeability pores, was prominent at low gas pressures but diminished with increasing gas pressure, suggesting critical thresholds for slip behavior under thermal effects. Porosity increased exponentially with temperature, particularly after 500 °C, as new pores and microcracks formed. Microstructural analysis revealed that high temperatures led to the transformation of kaolinite into mixed-layer illite, which played a pivotal role in altering pore structures and gas permeability. These findings provide a systematic understanding of the coupled thermal-mechanical effects on sandstone and have implications for geothermal energy extraction, underground coal gasification, and other subsurface engineering applications.
期刊介绍:
The International Journal of Rock Mechanics and Mining Sciences focuses on original research, new developments, site measurements, and case studies within the fields of rock mechanics and rock engineering. Serving as an international platform, it showcases high-quality papers addressing rock mechanics and the application of its principles and techniques in mining and civil engineering projects situated on or within rock masses. These projects encompass a wide range, including slopes, open-pit mines, quarries, shafts, tunnels, caverns, underground mines, metro systems, dams, hydro-electric stations, geothermal energy, petroleum engineering, and radioactive waste disposal. The journal welcomes submissions on various topics, with particular interest in theoretical advancements, analytical and numerical methods, rock testing, site investigation, and case studies.