Yabin Cao , Liuyan Zhao , Yixuan Zhu , Qiufeng Wang , Yahui Liu , Simin Wang , Yinan Jiao
{"title":"集成机器学习和微观结构分析的高性能陶瓷增强包层设计","authors":"Yabin Cao , Liuyan Zhao , Yixuan Zhu , Qiufeng Wang , Yahui Liu , Simin Wang , Yinan Jiao","doi":"10.1016/j.matchar.2025.115560","DOIUrl":null,"url":null,"abstract":"<div><div>The preparation of ceramic-reinforced, metal-based fusion cladding steel surfaces is an effective way to improve the wear resistance of cutter rings in shield machine. However, designing high-performance metal-ceramic powders is challenging due to their complex composition, often requiring extensive experimental work. To address this problem, this study utilizes experimental data to predict the wear resistance of ceramic-reinforced, iron-based plasma fusion cladding layers through machine learning. The goal is to support the design of high-performance metal-ceramic powders. First, four nonlinear regression models were established. The optimal model was selected after optimization and comparison to predict the wear resistance of the cladding layer. Experiments were then conducted to validate the reliability of the prediction model. Finally, model interpretation, microstructural analysis of the cladding layer, and thermodynamic calculations were performed to elucidate the relationship between powder composition, microstructure, and performances of the cladding layer. The results show that the random forest model (RF) has the best prediction accuracy, achieving an coefficient of determination (R<sup>2</sup>) of 0.84 after optimization. This model effectively predicts the trends in wear resistance of the cladding layer. Based on the predicted results, a metal-ceramic powder was designed and used to prepare plasma cladding layers with excellent wear resistance. The interaction between powder compositions significantly influences the microstructure and, consequently, the wear resistance of the cladding layer. In particular, coupling effects, such as Cr<sub>3</sub>C<sub>2</sub> & NbC and Fe60 & NbC, showed a stronger impact on wear resistance than individual compositions. The excellent wear resistance of the optimized cladding layer is attributed to a multi-scale strengthening mechanism. The micron-szied primary M<sub>7</sub>C<sub>3</sub> carbides are well bonded to the substrate. Their elongated shape and high hardness contribute to improved wear resistance. The matrix of the cladding layer consists of eutectic structure composed of micron-sized M<sub>23</sub>C<sub>6</sub> hard phase and submicron-sized ductile α-Fe phase. The honeycomb-like structure helps prevent excessive wear of α-Fe and the detachment of M<sub>23</sub>C<sub>6</sub> during abrasion, which is crucial for enhancing overall wear resistance. The nanoscale precipitates strengthen the α-Fe phase, further improving the wear resistance of the fused cladding.</div></div>","PeriodicalId":18727,"journal":{"name":"Materials Characterization","volume":"229 ","pages":"Article 115560"},"PeriodicalIF":5.5000,"publicationDate":"2025-09-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Integrating machine learning and microstructure analysis for the design of high-performance ceramic-reinforced cladding layers\",\"authors\":\"Yabin Cao , Liuyan Zhao , Yixuan Zhu , Qiufeng Wang , Yahui Liu , Simin Wang , Yinan Jiao\",\"doi\":\"10.1016/j.matchar.2025.115560\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>The preparation of ceramic-reinforced, metal-based fusion cladding steel surfaces is an effective way to improve the wear resistance of cutter rings in shield machine. However, designing high-performance metal-ceramic powders is challenging due to their complex composition, often requiring extensive experimental work. To address this problem, this study utilizes experimental data to predict the wear resistance of ceramic-reinforced, iron-based plasma fusion cladding layers through machine learning. The goal is to support the design of high-performance metal-ceramic powders. First, four nonlinear regression models were established. The optimal model was selected after optimization and comparison to predict the wear resistance of the cladding layer. Experiments were then conducted to validate the reliability of the prediction model. Finally, model interpretation, microstructural analysis of the cladding layer, and thermodynamic calculations were performed to elucidate the relationship between powder composition, microstructure, and performances of the cladding layer. The results show that the random forest model (RF) has the best prediction accuracy, achieving an coefficient of determination (R<sup>2</sup>) of 0.84 after optimization. This model effectively predicts the trends in wear resistance of the cladding layer. Based on the predicted results, a metal-ceramic powder was designed and used to prepare plasma cladding layers with excellent wear resistance. The interaction between powder compositions significantly influences the microstructure and, consequently, the wear resistance of the cladding layer. In particular, coupling effects, such as Cr<sub>3</sub>C<sub>2</sub> & NbC and Fe60 & NbC, showed a stronger impact on wear resistance than individual compositions. The excellent wear resistance of the optimized cladding layer is attributed to a multi-scale strengthening mechanism. The micron-szied primary M<sub>7</sub>C<sub>3</sub> carbides are well bonded to the substrate. Their elongated shape and high hardness contribute to improved wear resistance. The matrix of the cladding layer consists of eutectic structure composed of micron-sized M<sub>23</sub>C<sub>6</sub> hard phase and submicron-sized ductile α-Fe phase. The honeycomb-like structure helps prevent excessive wear of α-Fe and the detachment of M<sub>23</sub>C<sub>6</sub> during abrasion, which is crucial for enhancing overall wear resistance. The nanoscale precipitates strengthen the α-Fe phase, further improving the wear resistance of the fused cladding.</div></div>\",\"PeriodicalId\":18727,\"journal\":{\"name\":\"Materials Characterization\",\"volume\":\"229 \",\"pages\":\"Article 115560\"},\"PeriodicalIF\":5.5000,\"publicationDate\":\"2025-09-12\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Materials Characterization\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S1044580325008496\",\"RegionNum\":2,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"MATERIALS SCIENCE, CHARACTERIZATION & TESTING\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Materials Characterization","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S1044580325008496","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"MATERIALS SCIENCE, CHARACTERIZATION & TESTING","Score":null,"Total":0}
Integrating machine learning and microstructure analysis for the design of high-performance ceramic-reinforced cladding layers
The preparation of ceramic-reinforced, metal-based fusion cladding steel surfaces is an effective way to improve the wear resistance of cutter rings in shield machine. However, designing high-performance metal-ceramic powders is challenging due to their complex composition, often requiring extensive experimental work. To address this problem, this study utilizes experimental data to predict the wear resistance of ceramic-reinforced, iron-based plasma fusion cladding layers through machine learning. The goal is to support the design of high-performance metal-ceramic powders. First, four nonlinear regression models were established. The optimal model was selected after optimization and comparison to predict the wear resistance of the cladding layer. Experiments were then conducted to validate the reliability of the prediction model. Finally, model interpretation, microstructural analysis of the cladding layer, and thermodynamic calculations were performed to elucidate the relationship between powder composition, microstructure, and performances of the cladding layer. The results show that the random forest model (RF) has the best prediction accuracy, achieving an coefficient of determination (R2) of 0.84 after optimization. This model effectively predicts the trends in wear resistance of the cladding layer. Based on the predicted results, a metal-ceramic powder was designed and used to prepare plasma cladding layers with excellent wear resistance. The interaction between powder compositions significantly influences the microstructure and, consequently, the wear resistance of the cladding layer. In particular, coupling effects, such as Cr3C2 & NbC and Fe60 & NbC, showed a stronger impact on wear resistance than individual compositions. The excellent wear resistance of the optimized cladding layer is attributed to a multi-scale strengthening mechanism. The micron-szied primary M7C3 carbides are well bonded to the substrate. Their elongated shape and high hardness contribute to improved wear resistance. The matrix of the cladding layer consists of eutectic structure composed of micron-sized M23C6 hard phase and submicron-sized ductile α-Fe phase. The honeycomb-like structure helps prevent excessive wear of α-Fe and the detachment of M23C6 during abrasion, which is crucial for enhancing overall wear resistance. The nanoscale precipitates strengthen the α-Fe phase, further improving the wear resistance of the fused cladding.
期刊介绍:
Materials Characterization features original articles and state-of-the-art reviews on theoretical and practical aspects of the structure and behaviour of materials.
The Journal focuses on all characterization techniques, including all forms of microscopy (light, electron, acoustic, etc.,) and analysis (especially microanalysis and surface analytical techniques). Developments in both this wide range of techniques and their application to the quantification of the microstructure of materials are essential facets of the Journal.
The Journal provides the Materials Scientist/Engineer with up-to-date information on many types of materials with an underlying theme of explaining the behavior of materials using novel approaches. Materials covered by the journal include:
Metals & Alloys
Ceramics
Nanomaterials
Biomedical materials
Optical materials
Composites
Natural Materials.