p型同轴HPGe探测器的性能评价:伽玛光谱关键参数的长期分析

IF 1.8 3区 工程技术 Q3 CHEMISTRY, INORGANIC & NUCLEAR
Zahra Rakeb , Sedigheh Sina , Rasool Safari , Mohammadreza Parishan
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引用次数: 0

摘要

每一个高纯度锗的参数的精确测定,HPGe探测器确保定量结果从光谱分析获得的精度。本研究对运行超过15年的高纯度锗(HPGe)伽马能谱系统进行了综合性能评估和长期质量控制评估。记录了关键的光谱测量指标,包括能量分辨率、峰形比、不对称性、峰-康普顿比、相对效率、电子噪声、最小可检测活性(MDA)以及系统的可重复性和再现性。在校准源Co-60的帮助下,探测器的能量分辨率达到了2.01 keV (FWHM),具有良好的峰形比(FWTM/FWHM = 1.73, FWFM/FWHM = 2.48)和52.2的峰-康普顿比,表明了高分辨率和零光谱失真。在1332.5 keV下,探测器的相对效率为33.88%,电子噪声为0.178%,可以忽略不计。某些放射性核素的MDA在0.048-0.605 Bq/kg范围内,即使对低活性峰也表现出良好的敏感性。重复性试验显示,所有测得的峰的变异系数(%CV)均小于1%,而重复性通过t检验和f检验进行统计检验。一个Shewhart X -control图表显示,在所有情况下,在任何时候,测量都在控制范围内,尽管在过去几年有轻微的下降趋势,表明可能需要重新校准或维护。调查结果证实,该系统持续符合ISO/IEC 17025质量标准,足以在放射性核素定量和环境监测中进行精确和可靠的伽马射线分析。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Performance evaluation of a p-type co-axial HPGe detector: Long-term analysis of key parameters for gamma spectroscopy
Accurate determination of the parameters of each high purity germanium, HPGe detectors ensure the precision of quantitative results obtained from spectrum analysis. This study presents a comprehensive performance evaluation and long-term quality control assessment of a high-purity germanium (HPGe) gamma spectrometry system that has been operational for over 15 years. Key spectrometric measures were recorded, including energy resolution, peak shape ratios, asymmetry, peak-to-Compton ratio, relative efficiency, electronic noise, minimum detectable activity (MDA), and repeatability and reproducibility of the system. With the assistance of a calibrated source Co-60, the detector exhibited a commendable energy resolution of 2.01 keV (FWHM), along with good peak shape ratios (FWTM/FWHM = 1.73, FWFM/FWHM = 2.48) and a peak-to-Compton ratio of 52.2, indicating high resolution and zero spectral distortion. Relative detector efficiency was 33.88 % at 1332.5 keV, and electronic noise was negligible at 0.178 %. MDA for certain radionuclides was found to be in the range 0.048–0.605 Bq/kg, which showed good sensitivity even for low-activity peaks. Repeatability tests gave a coefficient of variation (%CV) less than 1 % for all peaks measured, while reproducibility was confirmed with t-test and F-test statistical tests. A Shewhart X-control chart revealed that at all times in all cases, measurements were within control limits, though a slight downward trend in the last few years suggests potential need for recalibration or maintenance. The findings corroborate the sustained conformity of the system to ISO/IEC 17025 quality standards and its sufficiency for precise and trustworthy gamma-ray analysis in radionuclide quantification and environmental monitoring.
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来源期刊
Applied Radiation and Isotopes
Applied Radiation and Isotopes 工程技术-核科学技术
CiteScore
3.00
自引率
12.50%
发文量
406
审稿时长
13.5 months
期刊介绍: Applied Radiation and Isotopes provides a high quality medium for the publication of substantial, original and scientific and technological papers on the development and peaceful application of nuclear, radiation and radionuclide techniques in chemistry, physics, biochemistry, biology, medicine, security, engineering and in the earth, planetary and environmental sciences, all including dosimetry. Nuclear techniques are defined in the broadest sense and both experimental and theoretical papers are welcome. They include the development and use of α- and β-particles, X-rays and γ-rays, neutrons and other nuclear particles and radiations from all sources, including radionuclides, synchrotron sources, cyclotrons and reactors and from the natural environment. The journal aims to publish papers with significance to an international audience, containing substantial novelty and scientific impact. The Editors reserve the rights to reject, with or without external review, papers that do not meet these criteria. Papers dealing with radiation processing, i.e., where radiation is used to bring about a biological, chemical or physical change in a material, should be directed to our sister journal Radiation Physics and Chemistry.
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