Ti-13Nb-13Zr合金阳极氧化后拉伸性能的数值分析

Dragana Mihajlović , Bojan Međo , Nenad Gubeljak , Ivana Cvijović-Alagić , Veljko Đokić , Marko Rakin
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引用次数: 0

摘要

采用阳极氧化法对粗晶Ti-13Nb-13Zr (CG - TNZ)合金进行表面改性。为了获得纳米结构的氧化层,在表面改性过程中使用1M H3PO4 + NaF作为电解液,阳极氧化时间为90分钟。利用场发射扫描电镜(FE-SEM)分析了改性后的表面形貌。人们认识到阳极氧化导致了由纳米管组成的氧化层的产生。通过拉伸试验测定了CG TNZ合金阳极氧化前后的拉伸特性。拉伸试验使用矩形截面的微拉伸试样(MTS)进行。阳极氧化导致cgtnz合金的拉伸性能下降。为了更好地了解CG TNZ合金阳极氧化后的拉伸行为,对其进行了数值分析。利用Abaqus软件建立了模拟拉伸试验的MTS三维数值模型。采用完全Gurson模型(complete Gurson model, CGM)进行了数值计算,该模型是金属材料韧性断裂的微观力学模型。量化材料损伤的参数,即空隙或孔隙率的体积分数,是变化的。因此,损伤参数初始孔隙体积分数f0分别为0.01和0.005。除了考虑MTS的伸长率外,还考虑了MTS颈部横截面厚度的减小。结果表明,损伤参数初始值为0.005时的CGM预测了相应减薄值下MTS的失效。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Numerical analysis of tensile behaviour of Ti-13Nb-13Zr alloy after anodic oxidation
The surface of coarse-grained Ti-13Nb-13Zr (CG TNZ) alloy was modified using the anodic oxidation. In order to obtained nanostructured oxide layer, as electrolyte in surface modification process 1M H3PO4 + NaF was used, while anodizing time was 90 minutes. The modified surface morphology was analyzed using the field emission scanning electron microscopy (FE-SEM)). It was realized that anodic oxidation led to the creation of the oxide layer consisted of nanotubes. Tensile characteristics of the CG TNZ alloy, before and after anodic oxidation, were determined by tensile testing. Tensile testing was performed using Micro Tensile Specimens (MTS) with a rectangular cross-section. The anodic oxidation led to a decrease of tensile characteristics of the CG TNZ alloy. In order to better understand tensile behaviour of the CG TNZ alloy after anodic oxidation, numerical analysis was done. The 3D numerical model of MTS, which simulated the tensile test, was made in Abaqus software package. Numerical results were obtained using the complete Gurson model (CGM), which is micromechanical model used for the ductile fracture of metallic materials. The parameter that quantifies the damage in the material, that is, the volume fraction of voids or porosity, is varied. So the value of the damage parameter, the initial void volume fraction, f0, was 0.01 and 0.005. In addition to the elongation of the MTS, the reduction of the cross-sectional thickness at the neck of MTS was also considered. Results showed that CGM for the initial value of the damage parameter 0.005 predicts the failure of the MTS at the corresponding value of thickness reduction.
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