通过基体加热和热处理消除IN738定向能高温合金的裂纹并协同提高其强度和塑性

IF 5.4 2区 工程技术 Q2 ENGINEERING, MANUFACTURING
Mingzhang Chen , Lin Hua , Zeqi Hu , Xunchen Liu , Xunpeng Qin
{"title":"通过基体加热和热处理消除IN738定向能高温合金的裂纹并协同提高其强度和塑性","authors":"Mingzhang Chen ,&nbsp;Lin Hua ,&nbsp;Zeqi Hu ,&nbsp;Xunchen Liu ,&nbsp;Xunpeng Qin","doi":"10.1016/j.cirpj.2025.08.009","DOIUrl":null,"url":null,"abstract":"<div><div>During the directed energy deposition (DED) process of IN738 superalloy, elevated thermal stresses and low-ductility γ′ phase can lead to crack formation. To tackle the cracking issue, this study developed a substrate heating platform within the DED apparatus, raising the substrate temperature to 300 °C to diminish the temperature gradient and thermal stress, while also optimizing laser power and scanning speed to achieve DED crack-free IN738. On-site thermal imaging and numerical simulations indicated that the temperature gradient and thermal stress in the samples gradually diminished with rising substrate temperatures and optimized process parameters. Moreover, microstructural characterization results revealed that heating the substrate to 300 °C reduced the content of the γ′ phase, while optimizing process parameters further refined the grains. The combination of reduced thermal stress, grain refinement, and diminished γ′ phase volume fraction collectively enabled the DED of crack-free IN738. On the crack-free DED IN738, a solution treatment at 1120°C for two hours notably improved its mechanical properties. The solution treatment simultaneously eliminated the Laves phase and generated finer γ′ phases along with a bimodal structure. These strengthening mechanisms effectively enhanced strength and ductility. Digital image correlation (DIC) and fractographic analyses substantiated that the solution treatment improved the coordinated deformation ability and the solubility of certain carbides reduced defects, further enhancing strength and ductility. Interestingly, a subsequent 24-hour aging treatment at 850°C did not significantly improve properties due to γ′ phase coarsening and δ phase precipitation.</div></div>","PeriodicalId":56011,"journal":{"name":"CIRP Journal of Manufacturing Science and Technology","volume":"62 ","pages":"Pages 59-74"},"PeriodicalIF":5.4000,"publicationDate":"2025-09-03","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Crack elimination and synergistic improvement of strength and ductility in directed energy deposited IN738 superalloy via substrate heating and heat treatment\",\"authors\":\"Mingzhang Chen ,&nbsp;Lin Hua ,&nbsp;Zeqi Hu ,&nbsp;Xunchen Liu ,&nbsp;Xunpeng Qin\",\"doi\":\"10.1016/j.cirpj.2025.08.009\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>During the directed energy deposition (DED) process of IN738 superalloy, elevated thermal stresses and low-ductility γ′ phase can lead to crack formation. To tackle the cracking issue, this study developed a substrate heating platform within the DED apparatus, raising the substrate temperature to 300 °C to diminish the temperature gradient and thermal stress, while also optimizing laser power and scanning speed to achieve DED crack-free IN738. On-site thermal imaging and numerical simulations indicated that the temperature gradient and thermal stress in the samples gradually diminished with rising substrate temperatures and optimized process parameters. Moreover, microstructural characterization results revealed that heating the substrate to 300 °C reduced the content of the γ′ phase, while optimizing process parameters further refined the grains. The combination of reduced thermal stress, grain refinement, and diminished γ′ phase volume fraction collectively enabled the DED of crack-free IN738. On the crack-free DED IN738, a solution treatment at 1120°C for two hours notably improved its mechanical properties. The solution treatment simultaneously eliminated the Laves phase and generated finer γ′ phases along with a bimodal structure. These strengthening mechanisms effectively enhanced strength and ductility. Digital image correlation (DIC) and fractographic analyses substantiated that the solution treatment improved the coordinated deformation ability and the solubility of certain carbides reduced defects, further enhancing strength and ductility. Interestingly, a subsequent 24-hour aging treatment at 850°C did not significantly improve properties due to γ′ phase coarsening and δ phase precipitation.</div></div>\",\"PeriodicalId\":56011,\"journal\":{\"name\":\"CIRP Journal of Manufacturing Science and Technology\",\"volume\":\"62 \",\"pages\":\"Pages 59-74\"},\"PeriodicalIF\":5.4000,\"publicationDate\":\"2025-09-03\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"CIRP Journal of Manufacturing Science and Technology\",\"FirstCategoryId\":\"5\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S1755581725001373\",\"RegionNum\":2,\"RegionCategory\":\"工程技术\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"ENGINEERING, MANUFACTURING\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"CIRP Journal of Manufacturing Science and Technology","FirstCategoryId":"5","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S1755581725001373","RegionNum":2,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"ENGINEERING, MANUFACTURING","Score":null,"Total":0}
引用次数: 0

摘要

在IN738高温合金定向能沉积(DED)过程中,较高的热应力和低塑性γ′相可导致裂纹的形成。为了解决裂纹问题,本研究在DED设备内开发了衬底加热平台,将衬底温度提高到300 °C,以减小温度梯度和热应力,同时优化激光功率和扫描速度,以实现DED无裂纹IN738。现场热成像和数值模拟结果表明,随着衬底温度的升高和工艺参数的优化,样品中的温度梯度和热应力逐渐减小。此外,显微组织表征结果表明,将衬底加热到300 °C降低了γ′相的含量,同时优化工艺参数进一步细化了晶粒。热应力的降低、晶粒的细化和γ′相体积分数的降低共同使IN738的DED无裂纹。对无裂纹DED IN738进行1120℃固溶处理2小时,其力学性能得到显著改善。固溶处理同时消除了Laves相,生成了更细的γ′相和双峰结构。这些强化机制有效地提高了强度和延展性。数字图像相关(DIC)和断口分析证实,固溶处理提高了合金的协调变形能力,某些碳化物的溶解度降低了缺陷,进一步提高了合金的强度和塑性。有趣的是,随后在850℃下进行24小时时效处理,由于γ′相粗化和δ相析出,性能没有显著改善。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Crack elimination and synergistic improvement of strength and ductility in directed energy deposited IN738 superalloy via substrate heating and heat treatment
During the directed energy deposition (DED) process of IN738 superalloy, elevated thermal stresses and low-ductility γ′ phase can lead to crack formation. To tackle the cracking issue, this study developed a substrate heating platform within the DED apparatus, raising the substrate temperature to 300 °C to diminish the temperature gradient and thermal stress, while also optimizing laser power and scanning speed to achieve DED crack-free IN738. On-site thermal imaging and numerical simulations indicated that the temperature gradient and thermal stress in the samples gradually diminished with rising substrate temperatures and optimized process parameters. Moreover, microstructural characterization results revealed that heating the substrate to 300 °C reduced the content of the γ′ phase, while optimizing process parameters further refined the grains. The combination of reduced thermal stress, grain refinement, and diminished γ′ phase volume fraction collectively enabled the DED of crack-free IN738. On the crack-free DED IN738, a solution treatment at 1120°C for two hours notably improved its mechanical properties. The solution treatment simultaneously eliminated the Laves phase and generated finer γ′ phases along with a bimodal structure. These strengthening mechanisms effectively enhanced strength and ductility. Digital image correlation (DIC) and fractographic analyses substantiated that the solution treatment improved the coordinated deformation ability and the solubility of certain carbides reduced defects, further enhancing strength and ductility. Interestingly, a subsequent 24-hour aging treatment at 850°C did not significantly improve properties due to γ′ phase coarsening and δ phase precipitation.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
CIRP Journal of Manufacturing Science and Technology
CIRP Journal of Manufacturing Science and Technology Engineering-Industrial and Manufacturing Engineering
CiteScore
9.10
自引率
6.20%
发文量
166
审稿时长
63 days
期刊介绍: The CIRP Journal of Manufacturing Science and Technology (CIRP-JMST) publishes fundamental papers on manufacturing processes, production equipment and automation, product design, manufacturing systems and production organisations up to the level of the production networks, including all the related technical, human and economic factors. Preference is given to contributions describing research results whose feasibility has been demonstrated either in a laboratory or in the industrial praxis. Case studies and review papers on specific issues in manufacturing science and technology are equally encouraged.
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:604180095
Book学术官方微信