{"title":"低温下光谱发射率测量的高精度温度标定方法","authors":"Zeye Yuan , Longfei Li , Kun Yu , Yufang Liu","doi":"10.1016/j.infrared.2025.106119","DOIUrl":null,"url":null,"abstract":"<div><div>Under low-temperature conditions, temperature measurement uncertainties of radiation sources introduce non-negligible systematic errors in weak radiation detection. This study proposes a novel equivalent temperature calibration method that iteratively determines the temperature of the central radiation zone based on temperature measurements in non-detection areas. A proportional heat transfer model of the sample radiation source is developed to simulate the surface temperature distribution under high-vacuum cryogenic conditions, optimizing the temperature iteration range. Temperature fluctuation theory is incorporated to quantitatively analyze the impact of radiation source temperature uncertainties on direct emissivity measurement accuracy. The accuracy of the proposed temperature calculation method is systematically evaluated through a comparative analysis of temperature measurement results for copper-based high-emissivity coating samples across various temperature conditions. The reliability of the experimental setup is further validated using a VO<sub>2</sub>-sapphire sample, demonstrating spectral emissivity measurements within the temperature range of 213–363 K, with an overall expanded measurement uncertainty better than 0.01.</div></div>","PeriodicalId":13549,"journal":{"name":"Infrared Physics & Technology","volume":"151 ","pages":"Article 106119"},"PeriodicalIF":3.4000,"publicationDate":"2025-08-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"High-precision temperature calibration method for spectral emissivity measurement at low temperatures\",\"authors\":\"Zeye Yuan , Longfei Li , Kun Yu , Yufang Liu\",\"doi\":\"10.1016/j.infrared.2025.106119\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>Under low-temperature conditions, temperature measurement uncertainties of radiation sources introduce non-negligible systematic errors in weak radiation detection. This study proposes a novel equivalent temperature calibration method that iteratively determines the temperature of the central radiation zone based on temperature measurements in non-detection areas. A proportional heat transfer model of the sample radiation source is developed to simulate the surface temperature distribution under high-vacuum cryogenic conditions, optimizing the temperature iteration range. Temperature fluctuation theory is incorporated to quantitatively analyze the impact of radiation source temperature uncertainties on direct emissivity measurement accuracy. The accuracy of the proposed temperature calculation method is systematically evaluated through a comparative analysis of temperature measurement results for copper-based high-emissivity coating samples across various temperature conditions. The reliability of the experimental setup is further validated using a VO<sub>2</sub>-sapphire sample, demonstrating spectral emissivity measurements within the temperature range of 213–363 K, with an overall expanded measurement uncertainty better than 0.01.</div></div>\",\"PeriodicalId\":13549,\"journal\":{\"name\":\"Infrared Physics & Technology\",\"volume\":\"151 \",\"pages\":\"Article 106119\"},\"PeriodicalIF\":3.4000,\"publicationDate\":\"2025-08-28\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Infrared Physics & Technology\",\"FirstCategoryId\":\"101\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S1350449525004128\",\"RegionNum\":3,\"RegionCategory\":\"物理与天体物理\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"INSTRUMENTS & INSTRUMENTATION\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Infrared Physics & Technology","FirstCategoryId":"101","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S1350449525004128","RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"INSTRUMENTS & INSTRUMENTATION","Score":null,"Total":0}
High-precision temperature calibration method for spectral emissivity measurement at low temperatures
Under low-temperature conditions, temperature measurement uncertainties of radiation sources introduce non-negligible systematic errors in weak radiation detection. This study proposes a novel equivalent temperature calibration method that iteratively determines the temperature of the central radiation zone based on temperature measurements in non-detection areas. A proportional heat transfer model of the sample radiation source is developed to simulate the surface temperature distribution under high-vacuum cryogenic conditions, optimizing the temperature iteration range. Temperature fluctuation theory is incorporated to quantitatively analyze the impact of radiation source temperature uncertainties on direct emissivity measurement accuracy. The accuracy of the proposed temperature calculation method is systematically evaluated through a comparative analysis of temperature measurement results for copper-based high-emissivity coating samples across various temperature conditions. The reliability of the experimental setup is further validated using a VO2-sapphire sample, demonstrating spectral emissivity measurements within the temperature range of 213–363 K, with an overall expanded measurement uncertainty better than 0.01.
期刊介绍:
The Journal covers the entire field of infrared physics and technology: theory, experiment, application, devices and instrumentation. Infrared'' is defined as covering the near, mid and far infrared (terahertz) regions from 0.75um (750nm) to 1mm (300GHz.) Submissions in the 300GHz to 100GHz region may be accepted at the editors discretion if their content is relevant to shorter wavelengths. Submissions must be primarily concerned with and directly relevant to this spectral region.
Its core topics can be summarized as the generation, propagation and detection, of infrared radiation; the associated optics, materials and devices; and its use in all fields of science, industry, engineering and medicine.
Infrared techniques occur in many different fields, notably spectroscopy and interferometry; material characterization and processing; atmospheric physics, astronomy and space research. Scientific aspects include lasers, quantum optics, quantum electronics, image processing and semiconductor physics. Some important applications are medical diagnostics and treatment, industrial inspection and environmental monitoring.