搅拌叶片对塔式连续结晶器纯化对甲酚影响的实验与模拟

IF 5.9 2区 工程技术 Q1 ENGINEERING, MULTIDISCIPLINARY
Wenlong Xiao , Xu Ma , He’an Luo , Zhengming Yi , Sheng Yang
{"title":"搅拌叶片对塔式连续结晶器纯化对甲酚影响的实验与模拟","authors":"Wenlong Xiao ,&nbsp;Xu Ma ,&nbsp;He’an Luo ,&nbsp;Zhengming Yi ,&nbsp;Sheng Yang","doi":"10.1016/j.asej.2025.103711","DOIUrl":null,"url":null,"abstract":"<div><div>The design of stirrer blade is investigated to solve the shortcomings of continuous melt crystallization, such as discontinuous crystal bed and crystallizer blockage. Through experiments and computational fluid dynamics simulations, it was determined that the crystallization bed was the key factor affecting the purification effect. A three-stage structure for the stirrer blade was proposed, consisting of a rushton turbine, a special type of helical ribbon impeller, and an impeller. The optimal parameters were established by single-phase flow simulation as an agitator blade radius of 19 mm, a propeller blade height of 25 mm, a propeller series of 5, and a stirring speed of 120 rpm. The two-phase flow simulation further verified the feasibility of the three-stage stirring structure. The optimized stirrer blade effectively ensured the height and continuity of the crystal bed. This provides the basis for achieving continuous crystallization and promotes the development of industrial separation technology.</div></div>","PeriodicalId":48648,"journal":{"name":"Ain Shams Engineering Journal","volume":"16 11","pages":"Article 103711"},"PeriodicalIF":5.9000,"publicationDate":"2025-08-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Experiment and simulation of the effect of stirrer blade on the purification of p-cresol by tower continuous crystallizer\",\"authors\":\"Wenlong Xiao ,&nbsp;Xu Ma ,&nbsp;He’an Luo ,&nbsp;Zhengming Yi ,&nbsp;Sheng Yang\",\"doi\":\"10.1016/j.asej.2025.103711\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>The design of stirrer blade is investigated to solve the shortcomings of continuous melt crystallization, such as discontinuous crystal bed and crystallizer blockage. Through experiments and computational fluid dynamics simulations, it was determined that the crystallization bed was the key factor affecting the purification effect. A three-stage structure for the stirrer blade was proposed, consisting of a rushton turbine, a special type of helical ribbon impeller, and an impeller. The optimal parameters were established by single-phase flow simulation as an agitator blade radius of 19 mm, a propeller blade height of 25 mm, a propeller series of 5, and a stirring speed of 120 rpm. The two-phase flow simulation further verified the feasibility of the three-stage stirring structure. The optimized stirrer blade effectively ensured the height and continuity of the crystal bed. This provides the basis for achieving continuous crystallization and promotes the development of industrial separation technology.</div></div>\",\"PeriodicalId\":48648,\"journal\":{\"name\":\"Ain Shams Engineering Journal\",\"volume\":\"16 11\",\"pages\":\"Article 103711\"},\"PeriodicalIF\":5.9000,\"publicationDate\":\"2025-08-26\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Ain Shams Engineering Journal\",\"FirstCategoryId\":\"5\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S2090447925004526\",\"RegionNum\":2,\"RegionCategory\":\"工程技术\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"ENGINEERING, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Ain Shams Engineering Journal","FirstCategoryId":"5","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S2090447925004526","RegionNum":2,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"ENGINEERING, MULTIDISCIPLINARY","Score":null,"Total":0}
引用次数: 0

摘要

为解决熔体连续结晶存在的结晶床不连续、结晶器堵塞等缺点,研究了搅拌叶片的设计。通过实验和计算流体力学模拟,确定了结晶床是影响提纯效果的关键因素。提出了一种由拉什顿涡轮、特殊类型的螺旋带叶轮和叶轮组成的搅拌叶片三级结构。通过单相流模拟,确定了搅拌桨桨叶半径为19 mm,桨叶高度为25 mm,桨叶级数为5个,搅拌转速为120 rpm的最佳参数。两相流仿真进一步验证了三级搅拌结构的可行性。优化后的搅拌叶片有效保证了结晶床的高度和连续性。这为实现连续结晶提供了基础,促进了工业分离技术的发展。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Experiment and simulation of the effect of stirrer blade on the purification of p-cresol by tower continuous crystallizer
The design of stirrer blade is investigated to solve the shortcomings of continuous melt crystallization, such as discontinuous crystal bed and crystallizer blockage. Through experiments and computational fluid dynamics simulations, it was determined that the crystallization bed was the key factor affecting the purification effect. A three-stage structure for the stirrer blade was proposed, consisting of a rushton turbine, a special type of helical ribbon impeller, and an impeller. The optimal parameters were established by single-phase flow simulation as an agitator blade radius of 19 mm, a propeller blade height of 25 mm, a propeller series of 5, and a stirring speed of 120 rpm. The two-phase flow simulation further verified the feasibility of the three-stage stirring structure. The optimized stirrer blade effectively ensured the height and continuity of the crystal bed. This provides the basis for achieving continuous crystallization and promotes the development of industrial separation technology.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
Ain Shams Engineering Journal
Ain Shams Engineering Journal Engineering-General Engineering
CiteScore
10.80
自引率
13.30%
发文量
441
审稿时长
49 weeks
期刊介绍: in Shams Engineering Journal is an international journal devoted to publication of peer reviewed original high-quality research papers and review papers in both traditional topics and those of emerging science and technology. Areas of both theoretical and fundamental interest as well as those concerning industrial applications, emerging instrumental techniques and those which have some practical application to an aspect of human endeavor, such as the preservation of the environment, health, waste disposal are welcome. The overall focus is on original and rigorous scientific research results which have generic significance. Ain Shams Engineering Journal focuses upon aspects of mechanical engineering, electrical engineering, civil engineering, chemical engineering, petroleum engineering, environmental engineering, architectural and urban planning engineering. Papers in which knowledge from other disciplines is integrated with engineering are especially welcome like nanotechnology, material sciences, and computational methods as well as applied basic sciences: engineering mathematics, physics and chemistry.
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:604180095
Book学术官方微信