Ruyue Wang , Chengcheng Shi , Hao Qiu , Yaqin Zhou , Xuchang Cui , Hao Dong
{"title":"超细晶TZM合金热变形行为及显微组织演变","authors":"Ruyue Wang , Chengcheng Shi , Hao Qiu , Yaqin Zhou , Xuchang Cui , Hao Dong","doi":"10.1016/j.ijrmhm.2025.107387","DOIUrl":null,"url":null,"abstract":"<div><div>This research investigated the hot deformation behavior and microstructure evolution of ultrafine-grained TZM alloy over a temperature range of 1200–1350 °C and strain rates from 0.001 to 1 s<sup>−1</sup>. A strain-compensated Arrhenius constitutive model was developed and hot working maps were generated. Microstructural analysis revealed that at low temperatures and high strain rates, dynamic recrystallization (DRX) was insufficient, leading to a higher dislocation density and strong texture. As the temperature increased and the strain rate decreased, grain deformation was predominantly controlled by continuous dynamic recrystallization (CDRX). The proportion of recrystallized grains increased, as indicated by a rise in high-angle grain boundaries (HAGBs) and a reduction in dislocation density. Furthermore, the results showed that 〈100〉//CD and 〈111〉//CD were the primary slip directions. Elevated temperatures and reduced strain rates promoted the preferential growth of recrystallized grains along <100>//CD, enhancing texture strength. Based on the experimental findings, a schematic model of the microstructural evolution of ultrafine-grained TZM alloy during high-temperature deformation was proposed.</div></div>","PeriodicalId":14216,"journal":{"name":"International Journal of Refractory Metals & Hard Materials","volume":"133 ","pages":"Article 107387"},"PeriodicalIF":4.6000,"publicationDate":"2025-08-18","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Hot deformation behavior and microstructural evolution of ultrafine-grained TZM alloy\",\"authors\":\"Ruyue Wang , Chengcheng Shi , Hao Qiu , Yaqin Zhou , Xuchang Cui , Hao Dong\",\"doi\":\"10.1016/j.ijrmhm.2025.107387\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>This research investigated the hot deformation behavior and microstructure evolution of ultrafine-grained TZM alloy over a temperature range of 1200–1350 °C and strain rates from 0.001 to 1 s<sup>−1</sup>. A strain-compensated Arrhenius constitutive model was developed and hot working maps were generated. Microstructural analysis revealed that at low temperatures and high strain rates, dynamic recrystallization (DRX) was insufficient, leading to a higher dislocation density and strong texture. As the temperature increased and the strain rate decreased, grain deformation was predominantly controlled by continuous dynamic recrystallization (CDRX). The proportion of recrystallized grains increased, as indicated by a rise in high-angle grain boundaries (HAGBs) and a reduction in dislocation density. Furthermore, the results showed that 〈100〉//CD and 〈111〉//CD were the primary slip directions. Elevated temperatures and reduced strain rates promoted the preferential growth of recrystallized grains along <100>//CD, enhancing texture strength. Based on the experimental findings, a schematic model of the microstructural evolution of ultrafine-grained TZM alloy during high-temperature deformation was proposed.</div></div>\",\"PeriodicalId\":14216,\"journal\":{\"name\":\"International Journal of Refractory Metals & Hard Materials\",\"volume\":\"133 \",\"pages\":\"Article 107387\"},\"PeriodicalIF\":4.6000,\"publicationDate\":\"2025-08-18\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"International Journal of Refractory Metals & Hard Materials\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S026343682500352X\",\"RegionNum\":2,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"MATERIALS SCIENCE, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"International Journal of Refractory Metals & Hard Materials","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S026343682500352X","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
Hot deformation behavior and microstructural evolution of ultrafine-grained TZM alloy
This research investigated the hot deformation behavior and microstructure evolution of ultrafine-grained TZM alloy over a temperature range of 1200–1350 °C and strain rates from 0.001 to 1 s−1. A strain-compensated Arrhenius constitutive model was developed and hot working maps were generated. Microstructural analysis revealed that at low temperatures and high strain rates, dynamic recrystallization (DRX) was insufficient, leading to a higher dislocation density and strong texture. As the temperature increased and the strain rate decreased, grain deformation was predominantly controlled by continuous dynamic recrystallization (CDRX). The proportion of recrystallized grains increased, as indicated by a rise in high-angle grain boundaries (HAGBs) and a reduction in dislocation density. Furthermore, the results showed that 〈100〉//CD and 〈111〉//CD were the primary slip directions. Elevated temperatures and reduced strain rates promoted the preferential growth of recrystallized grains along <100>//CD, enhancing texture strength. Based on the experimental findings, a schematic model of the microstructural evolution of ultrafine-grained TZM alloy during high-temperature deformation was proposed.
期刊介绍:
The International Journal of Refractory Metals and Hard Materials (IJRMHM) publishes original research articles concerned with all aspects of refractory metals and hard materials. Refractory metals are defined as metals with melting points higher than 1800 °C. These are tungsten, molybdenum, chromium, tantalum, niobium, hafnium, and rhenium, as well as many compounds and alloys based thereupon. Hard materials that are included in the scope of this journal are defined as materials with hardness values higher than 1000 kg/mm2, primarily intended for applications as manufacturing tools or wear resistant components in mechanical systems. Thus they encompass carbides, nitrides and borides of metals, and related compounds. A special focus of this journal is put on the family of hardmetals, which is also known as cemented tungsten carbide, and cermets which are based on titanium carbide and carbonitrides with or without a metal binder. Ceramics and superhard materials including diamond and cubic boron nitride may also be accepted provided the subject material is presented as hard materials as defined above.