{"title":"食用脂肪的分离:卧螺离心机油脂分离模型","authors":"Myrofora Kyrimlidou, Carolin Prewitz, Luisa Lorimer, Miriam Gazmawe, Eckhard Flöter","doi":"10.1002/ejlt.70034","DOIUrl":null,"url":null,"abstract":"<p>In this work, the use of a lab-scale decanter centrifuge for the separation of fat crystal agglomerates from oil is studied. For this purpose, a model system of fully hydrogenated rapeseed oil and canola oil is used. The goal is the continuous mechanical de-oiling of the oil-fat slurry. The impact of the particle size and poly-dispersity of the slurry in combination with the process parameters, pool depth, flowrate, differential speed, and centripetal acceleration, is evaluated. These parameters lead to forces and particles’ velocities that actuate the oil/fat separation. The characteristic ones are theoretically calculated and the impact of each on the solids content in the liquid fraction and in the cake is assessed. The success of each separation process is measured through gas chromatography and light microscopy data. It is found that high hydrostatic pressure on the bowl wall—it already starts from the pool—leads to a compacted cake. At the next step, which happens on the dry beach, low cake axial transport velocity provides enough time for the olein to be removed from the cake pores. These two phenomena, especially in combination, lead to high cake dryness. For a fully continuous dry fractionation process, future research should be focused on the fat crystallization step.</p><p><i>Practical applications</i>: A decanter centrifuge is used to study an alternative to the conventional dry fractionation, which employs filtration to separate fat crystal agglomerates from liquid oil. The goal is to offer higher separation efficiencies, more energy and time efficiency, the potential for a fully continuous dry fractionation, less space demands, and process selectivity. Especially the latter, could be utilized as a tripalmitin-selective alternative method to the current multistep dry or solvent fractionation.</p>","PeriodicalId":11988,"journal":{"name":"European Journal of Lipid Science and Technology","volume":"127 8","pages":""},"PeriodicalIF":1.8000,"publicationDate":"2025-05-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://onlinelibrary.wiley.com/doi/epdf/10.1002/ejlt.70034","citationCount":"0","resultStr":"{\"title\":\"Fractionation of Edible Fats: Model Fat-Oil Separation in Decanter Centrifuge\",\"authors\":\"Myrofora Kyrimlidou, Carolin Prewitz, Luisa Lorimer, Miriam Gazmawe, Eckhard Flöter\",\"doi\":\"10.1002/ejlt.70034\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p>In this work, the use of a lab-scale decanter centrifuge for the separation of fat crystal agglomerates from oil is studied. For this purpose, a model system of fully hydrogenated rapeseed oil and canola oil is used. The goal is the continuous mechanical de-oiling of the oil-fat slurry. The impact of the particle size and poly-dispersity of the slurry in combination with the process parameters, pool depth, flowrate, differential speed, and centripetal acceleration, is evaluated. These parameters lead to forces and particles’ velocities that actuate the oil/fat separation. The characteristic ones are theoretically calculated and the impact of each on the solids content in the liquid fraction and in the cake is assessed. The success of each separation process is measured through gas chromatography and light microscopy data. It is found that high hydrostatic pressure on the bowl wall—it already starts from the pool—leads to a compacted cake. At the next step, which happens on the dry beach, low cake axial transport velocity provides enough time for the olein to be removed from the cake pores. These two phenomena, especially in combination, lead to high cake dryness. For a fully continuous dry fractionation process, future research should be focused on the fat crystallization step.</p><p><i>Practical applications</i>: A decanter centrifuge is used to study an alternative to the conventional dry fractionation, which employs filtration to separate fat crystal agglomerates from liquid oil. The goal is to offer higher separation efficiencies, more energy and time efficiency, the potential for a fully continuous dry fractionation, less space demands, and process selectivity. Especially the latter, could be utilized as a tripalmitin-selective alternative method to the current multistep dry or solvent fractionation.</p>\",\"PeriodicalId\":11988,\"journal\":{\"name\":\"European Journal of Lipid Science and Technology\",\"volume\":\"127 8\",\"pages\":\"\"},\"PeriodicalIF\":1.8000,\"publicationDate\":\"2025-05-20\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://onlinelibrary.wiley.com/doi/epdf/10.1002/ejlt.70034\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"European Journal of Lipid Science and Technology\",\"FirstCategoryId\":\"97\",\"ListUrlMain\":\"https://onlinelibrary.wiley.com/doi/10.1002/ejlt.70034\",\"RegionNum\":3,\"RegionCategory\":\"农林科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q3\",\"JCRName\":\"FOOD SCIENCE & TECHNOLOGY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"European Journal of Lipid Science and Technology","FirstCategoryId":"97","ListUrlMain":"https://onlinelibrary.wiley.com/doi/10.1002/ejlt.70034","RegionNum":3,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"FOOD SCIENCE & TECHNOLOGY","Score":null,"Total":0}
Fractionation of Edible Fats: Model Fat-Oil Separation in Decanter Centrifuge
In this work, the use of a lab-scale decanter centrifuge for the separation of fat crystal agglomerates from oil is studied. For this purpose, a model system of fully hydrogenated rapeseed oil and canola oil is used. The goal is the continuous mechanical de-oiling of the oil-fat slurry. The impact of the particle size and poly-dispersity of the slurry in combination with the process parameters, pool depth, flowrate, differential speed, and centripetal acceleration, is evaluated. These parameters lead to forces and particles’ velocities that actuate the oil/fat separation. The characteristic ones are theoretically calculated and the impact of each on the solids content in the liquid fraction and in the cake is assessed. The success of each separation process is measured through gas chromatography and light microscopy data. It is found that high hydrostatic pressure on the bowl wall—it already starts from the pool—leads to a compacted cake. At the next step, which happens on the dry beach, low cake axial transport velocity provides enough time for the olein to be removed from the cake pores. These two phenomena, especially in combination, lead to high cake dryness. For a fully continuous dry fractionation process, future research should be focused on the fat crystallization step.
Practical applications: A decanter centrifuge is used to study an alternative to the conventional dry fractionation, which employs filtration to separate fat crystal agglomerates from liquid oil. The goal is to offer higher separation efficiencies, more energy and time efficiency, the potential for a fully continuous dry fractionation, less space demands, and process selectivity. Especially the latter, could be utilized as a tripalmitin-selective alternative method to the current multistep dry or solvent fractionation.
期刊介绍:
The European Journal of Lipid Science and Technology is a peer-reviewed journal publishing original research articles, reviews, and other contributions on lipid related topics in food science and technology, biomedical science including clinical and pre-clinical research, nutrition, animal science, plant and microbial lipids, (bio)chemistry, oleochemistry, biotechnology, processing, physical chemistry, and analytics including lipidomics. A major focus of the journal is the synthesis of health related topics with applied aspects.
Following is a selection of subject areas which are of special interest to EJLST:
Animal and plant products for healthier foods including strategic feeding and transgenic crops
Authentication and analysis of foods for ensuring food quality and safety
Bioavailability of PUFA and other nutrients
Dietary lipids and minor compounds, their specific roles in food products and in nutrition
Food technology and processing for safer and healthier products
Functional foods and nutraceuticals
Lipidomics
Lipid structuring and formulations
Oleochemistry, lipid-derived polymers and biomaterials
Processes using lipid-modifying enzymes
The scope is not restricted to these areas. Submissions on topics at the interface of basic research and applications are strongly encouraged. The journal is the official organ the European Federation for the Science and Technology of Lipids (Euro Fed Lipid).