食用脂肪的分离:卧螺离心机油脂分离模型

IF 1.8 3区 农林科学 Q3 FOOD SCIENCE & TECHNOLOGY
Myrofora Kyrimlidou, Carolin Prewitz, Luisa Lorimer, Miriam Gazmawe, Eckhard Flöter
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引用次数: 0

摘要

在这项工作中,研究了使用实验室规模的卧螺离心机从油中分离脂肪结晶团块。为此,使用了完全氢化菜籽油和菜籽油的模型系统。目的是对油脂浆进行连续的机械脱油。结合工艺参数、池深、流量、差速和向心加速度,对浆料的粒度和多分散性的影响进行了评估。这些参数导致驱动油/脂肪分离的力和颗粒速度。从理论上计算了特征参数,并评价了各参数对液体馏分和饼中固体含量的影响。每个分离过程的成功是通过气相色谱法和光显微镜数据来测量的。研究发现,碗壁上的高静水压力——它已经从水池开始——导致了饼的压实。下一步,在干燥的海滩上进行,低的饼轴向输送速度为油从饼孔中去除提供了足够的时间。这两种现象,特别是结合在一起,会导致饼干度高。对于一个完全连续的干燥分馏过程,未来的研究应集中在脂肪结晶步骤。实际应用:卧螺离心机用于研究传统干法分馏的替代方法,干法分馏采用过滤从液体油中分离脂肪结晶团块。目标是提供更高的分离效率,更多的能量和时间效率,完全连续的干法分馏的潜力,更少的空间需求和工艺选择性。特别是后者,可以作为目前多步干燥或溶剂分馏的替代方法。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

Fractionation of Edible Fats: Model Fat-Oil Separation in Decanter Centrifuge

Fractionation of Edible Fats: Model Fat-Oil Separation in Decanter Centrifuge

In this work, the use of a lab-scale decanter centrifuge for the separation of fat crystal agglomerates from oil is studied. For this purpose, a model system of fully hydrogenated rapeseed oil and canola oil is used. The goal is the continuous mechanical de-oiling of the oil-fat slurry. The impact of the particle size and poly-dispersity of the slurry in combination with the process parameters, pool depth, flowrate, differential speed, and centripetal acceleration, is evaluated. These parameters lead to forces and particles’ velocities that actuate the oil/fat separation. The characteristic ones are theoretically calculated and the impact of each on the solids content in the liquid fraction and in the cake is assessed. The success of each separation process is measured through gas chromatography and light microscopy data. It is found that high hydrostatic pressure on the bowl wall—it already starts from the pool—leads to a compacted cake. At the next step, which happens on the dry beach, low cake axial transport velocity provides enough time for the olein to be removed from the cake pores. These two phenomena, especially in combination, lead to high cake dryness. For a fully continuous dry fractionation process, future research should be focused on the fat crystallization step.

Practical applications: A decanter centrifuge is used to study an alternative to the conventional dry fractionation, which employs filtration to separate fat crystal agglomerates from liquid oil. The goal is to offer higher separation efficiencies, more energy and time efficiency, the potential for a fully continuous dry fractionation, less space demands, and process selectivity. Especially the latter, could be utilized as a tripalmitin-selective alternative method to the current multistep dry or solvent fractionation.

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来源期刊
CiteScore
5.50
自引率
0.00%
发文量
101
审稿时长
6-16 weeks
期刊介绍: The European Journal of Lipid Science and Technology is a peer-reviewed journal publishing original research articles, reviews, and other contributions on lipid related topics in food science and technology, biomedical science including clinical and pre-clinical research, nutrition, animal science, plant and microbial lipids, (bio)chemistry, oleochemistry, biotechnology, processing, physical chemistry, and analytics including lipidomics. A major focus of the journal is the synthesis of health related topics with applied aspects. Following is a selection of subject areas which are of special interest to EJLST: Animal and plant products for healthier foods including strategic feeding and transgenic crops Authentication and analysis of foods for ensuring food quality and safety Bioavailability of PUFA and other nutrients Dietary lipids and minor compounds, their specific roles in food products and in nutrition Food technology and processing for safer and healthier products Functional foods and nutraceuticals Lipidomics Lipid structuring and formulations Oleochemistry, lipid-derived polymers and biomaterials Processes using lipid-modifying enzymes The scope is not restricted to these areas. Submissions on topics at the interface of basic research and applications are strongly encouraged. The journal is the official organ the European Federation for the Science and Technology of Lipids (Euro Fed Lipid).
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