高熵复合陶瓷的微观结构与力学性能研究

IF 2.3 4区 材料科学 Q2 MATERIALS SCIENCE, CERAMICS
Hui-Ze Li, Yan Zhang, Bo-Yu Ni, Zhang-Yu Wu, Hao-Yu Cao, Fa-Cai Yan, Rui-Wen Tang, Ye Liu
{"title":"高熵复合陶瓷的微观结构与力学性能研究","authors":"Hui-Ze Li,&nbsp;Yan Zhang,&nbsp;Bo-Yu Ni,&nbsp;Zhang-Yu Wu,&nbsp;Hao-Yu Cao,&nbsp;Fa-Cai Yan,&nbsp;Rui-Wen Tang,&nbsp;Ye Liu","doi":"10.1111/ijac.15191","DOIUrl":null,"url":null,"abstract":"<p>To investigate the microstructure and mechanical properties of HEB-SiC composite ceramics, various SiC contents (10 vol%, 20 vol%, 30 vol%) were incorporated as the second phase. (Mo<sub>0.2</sub>Nb<sub>0.2</sub>Zr<sub>0.2</sub>Hf<sub>0.2</sub>Ti<sub>0.2</sub>)B<sub>2</sub>-(10 vol%, 20 vol%, 30 vol%)SiC composite ceramics were synthesized using borothermal/carbothermal reduction followed by SPS. As the sintering temperature increased, the hardness of the composite ceramics remained relatively stable, while the fracture toughness showed a notable improvement. Additionally, with an increase in SiC content, the hardness of the composite ceramics decreased, whereas the fracture toughness increased. The highest hardness values were observed for the 10 vol% SiC samples, measuring 31.4 ± 1.4 GPa at 1800°C and 31.4 ± 1.3 GPa at 1900°C. The 30 vol% SiC sample sintered at 1900°C exhibited the highest fracture toughness, reaching 5.24 ± 0.44 MPa·m<sup>1/2</sup>. These findings demonstrate that increasing the SiC content enhances the mechanical properties of high-entropy boride ceramics.</p>","PeriodicalId":13903,"journal":{"name":"International Journal of Applied Ceramic Technology","volume":"22 5","pages":""},"PeriodicalIF":2.3000,"publicationDate":"2025-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Research on the microstructure and mechanical properties of high-entropy composite ceramics\",\"authors\":\"Hui-Ze Li,&nbsp;Yan Zhang,&nbsp;Bo-Yu Ni,&nbsp;Zhang-Yu Wu,&nbsp;Hao-Yu Cao,&nbsp;Fa-Cai Yan,&nbsp;Rui-Wen Tang,&nbsp;Ye Liu\",\"doi\":\"10.1111/ijac.15191\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p>To investigate the microstructure and mechanical properties of HEB-SiC composite ceramics, various SiC contents (10 vol%, 20 vol%, 30 vol%) were incorporated as the second phase. (Mo<sub>0.2</sub>Nb<sub>0.2</sub>Zr<sub>0.2</sub>Hf<sub>0.2</sub>Ti<sub>0.2</sub>)B<sub>2</sub>-(10 vol%, 20 vol%, 30 vol%)SiC composite ceramics were synthesized using borothermal/carbothermal reduction followed by SPS. As the sintering temperature increased, the hardness of the composite ceramics remained relatively stable, while the fracture toughness showed a notable improvement. Additionally, with an increase in SiC content, the hardness of the composite ceramics decreased, whereas the fracture toughness increased. The highest hardness values were observed for the 10 vol% SiC samples, measuring 31.4 ± 1.4 GPa at 1800°C and 31.4 ± 1.3 GPa at 1900°C. The 30 vol% SiC sample sintered at 1900°C exhibited the highest fracture toughness, reaching 5.24 ± 0.44 MPa·m<sup>1/2</sup>. These findings demonstrate that increasing the SiC content enhances the mechanical properties of high-entropy boride ceramics.</p>\",\"PeriodicalId\":13903,\"journal\":{\"name\":\"International Journal of Applied Ceramic Technology\",\"volume\":\"22 5\",\"pages\":\"\"},\"PeriodicalIF\":2.3000,\"publicationDate\":\"2025-06-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"International Journal of Applied Ceramic Technology\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://ceramics.onlinelibrary.wiley.com/doi/10.1111/ijac.15191\",\"RegionNum\":4,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"MATERIALS SCIENCE, CERAMICS\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"International Journal of Applied Ceramic Technology","FirstCategoryId":"88","ListUrlMain":"https://ceramics.onlinelibrary.wiley.com/doi/10.1111/ijac.15191","RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"MATERIALS SCIENCE, CERAMICS","Score":null,"Total":0}
引用次数: 0

摘要

为了研究HEB-SiC复合陶瓷的微观组织和力学性能,将不同SiC含量(10 vol%, 20 vol%, 30 vol%)作为第二相。采用硼热/碳热还原- SPS法制备了(Mo0.2Nb0.2Zr0.2Hf0.2Ti0.2)B2-(10 vol%, 20 vol%, 30 vol%)SiC复合陶瓷。随着烧结温度的升高,复合陶瓷的硬度保持相对稳定,而断裂韧性有明显提高。随着SiC含量的增加,复合陶瓷的硬度降低,断裂韧性提高。SiC含量为10%的样品在1800℃和1900℃时的硬度分别为31.4±1.4 GPa和31.4±1.3 GPa。在1900℃下烧结的30 vol% SiC试样的断裂韧性最高,达到5.24±0.44 MPa·m1/2。结果表明,SiC含量的增加提高了高熵硼化物陶瓷的力学性能。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

Research on the microstructure and mechanical properties of high-entropy composite ceramics

Research on the microstructure and mechanical properties of high-entropy composite ceramics

Research on the microstructure and mechanical properties of high-entropy composite ceramics

To investigate the microstructure and mechanical properties of HEB-SiC composite ceramics, various SiC contents (10 vol%, 20 vol%, 30 vol%) were incorporated as the second phase. (Mo0.2Nb0.2Zr0.2Hf0.2Ti0.2)B2-(10 vol%, 20 vol%, 30 vol%)SiC composite ceramics were synthesized using borothermal/carbothermal reduction followed by SPS. As the sintering temperature increased, the hardness of the composite ceramics remained relatively stable, while the fracture toughness showed a notable improvement. Additionally, with an increase in SiC content, the hardness of the composite ceramics decreased, whereas the fracture toughness increased. The highest hardness values were observed for the 10 vol% SiC samples, measuring 31.4 ± 1.4 GPa at 1800°C and 31.4 ± 1.3 GPa at 1900°C. The 30 vol% SiC sample sintered at 1900°C exhibited the highest fracture toughness, reaching 5.24 ± 0.44 MPa·m1/2. These findings demonstrate that increasing the SiC content enhances the mechanical properties of high-entropy boride ceramics.

求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
International Journal of Applied Ceramic Technology
International Journal of Applied Ceramic Technology 工程技术-材料科学:硅酸盐
CiteScore
3.90
自引率
9.50%
发文量
280
审稿时长
4.5 months
期刊介绍: The International Journal of Applied Ceramic Technology publishes cutting edge applied research and development work focused on commercialization of engineered ceramics, products and processes. The publication also explores the barriers to commercialization, design and testing, environmental health issues, international standardization activities, databases, and cost models. Designed to get high quality information to end-users quickly, the peer process is led by an editorial board of experts from industry, government, and universities. Each issue focuses on a high-interest, high-impact topic plus includes a range of papers detailing applications of ceramics. Papers on all aspects of applied ceramics are welcome including those in the following areas: Nanotechnology applications; Ceramic Armor; Ceramic and Technology for Energy Applications (e.g., Fuel Cells, Batteries, Solar, Thermoelectric, and HT Superconductors); Ceramic Matrix Composites; Functional Materials; Thermal and Environmental Barrier Coatings; Bioceramic Applications; Green Manufacturing; Ceramic Processing; Glass Technology; Fiber optics; Ceramics in Environmental Applications; Ceramics in Electronic, Photonic and Magnetic Applications;
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:604180095
Book学术官方微信