土芋叶提取的氧化钴纳米颗粒:微观结构、形态、抗菌和光催化活性的综合研究

Md. Estabrak Ahammod Sakib , Md. Lael Hasan , Hridoy Roy , Md. Mahfujul Hasan , Md. Mintu Ali
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引用次数: 0

摘要

本研究以芋叶提取物为原料,探索生物合成氧化钴纳米颗粒(Co3O4 NPs)的生物医学和环境应用。通过x射线衍射(XRD)、扫描电子显微镜(SEM)、傅里叶变换红外光谱(FTIR)、能谱(EDS)和紫外可见光谱等分析技术对合成的纳米颗粒进行了表征。制备的氧化钴纳米颗粒的晶体性质通过XRD分析得到了很大程度的证实,其平均晶粒尺寸为18.233918 nm。随后,SEM显微照片显示球形纳米颗粒(22.26654 nm±0.17983 nm)分散在整个表面区域。EDS确保了成分中现有元素的存在。紫外可见光谱分析发现其吸光度峰为212.5 nm,能带隙为5.46 eV,对革兰氏阳性菌(金黄色葡萄球菌、枯草芽孢杆菌)和革兰氏阴性菌(铜绿假单胞菌、大肠杆菌)的抑菌活性进行了评价,通过增加抑菌面积破坏了细菌细胞。此外,Co3O4 NPs对有机染料(亚甲基蓝)的光催化降解活性在90 min内达到86.40%,可用于缓解相关的工业污染问题。这一探索也表明,合成的Co3O4可能是光催化降解染料的一种有前景的材料。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Colocasia esculenta leaf extracted cobalt oxide nanoparticles: A comprehensive investigation of the microstructural, morphological, antibacterial, and photocatalytic activity
This research was carried out to explore the biosynthesized cobalt oxide nanoparticles (Co3O4 NPs) for biomedical and environmental applications by using Colocasia esculenta (Taro) leaf extract. Herein, the synthesized nanoparticles were then characterized through several analytical techniques, such as x-ray diffraction (XRD), scanning electron microscopy (SEM), fourier transform infrared spectroscopy (FTIR), energy dispersive spectroscopy (EDS), and uv–visible spectroscopy. The crystallographic nature of prepared cobalt oxide NPs was largely confirmed by XRD analysis, with an average crystallite size of 18.233918 nm. Later, the SEM micrograph revealed spherical shape nanoparticles (22.26654 nm ± 0.17983 nm) dispersed throughout the surface area. EDS ensured the presence of existing elements in the composition. The absorbance peak at 212.5 nm and the energy band gap of 5.46 eV were noted by the uv–visible analysis, The antibacterial activity of the prepared NPs was evaluated against gram-positive (Staphylococcus aureus, Bacillus subtilis) and gram-negative (Pseudomonas aeruginosa, E. coli) bacteria, which demolished the bacterial cell by increasing the zone of inhibition area. Besides, the photocatalytic activity of Co3O4 NPs for an organic dye (Methylene Blue) degradation reached 86.40 % within 90 min, which may be recommended to mitigate related industrial contamination problems. This exploration also suggested that synthesized Co3O4 could be a promising material for photocatalytic dye degradation.
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