{"title":"选择性激光熔化制备fesal软磁合金的显微组织和软磁行为","authors":"Feng-Hui Wang, Cai-Yin You, Bing-Xu Liu, He-Guang Liu, Jing Zhang, Xiao-Pei Zhu, Na Tian","doi":"10.1016/j.jallcom.2025.181940","DOIUrl":null,"url":null,"abstract":"FeSiAl magnetic cores are extensively utilized in power electronic devices. Additive manufacturing techniques, particularly selective laser melting (SLM), are increasingly employed to fabricate magnetic cores, meeting the demands for miniaturization and integration of electronic systems. This study fabricated FeSiAl magnetic cores <ce:italic>via</ce:italic> SLM, with varying line laser energy densities (LED). The correlation between LED and microstructure was examined from the perspective of rapid solidification. Grain morphology was dominated by equiaxed crystals in the cross-sectional plane (x-y) and columnar crystals in the longitudinal planes (x-z and y-z). Notably, the printed samples exhibit alternating coarse and fine grain zones, with Si element enrichment observed at melt pool boundaries. Increasing LED reduces defects and promotes larger grain growth, with the strongest texture (7.64) along the building direction (BD) observed at an LED of 167<ce:hsp sp=\"0.25\"></ce:hsp>J/m. For the sample processed at LED = 167<ce:hsp sp=\"0.25\"></ce:hsp>J/m, a saturation magnetization of <ce:italic>M</ce:italic><ce:inf loc=\"post\"><ce:italic>s</ce:italic></ce:inf> = 124.3<ce:hsp sp=\"0.25\"></ce:hsp>emu/g, coercivity of <ce:italic>H</ce:italic><ce:inf loc=\"post\"><ce:italic>c</ce:italic></ce:inf> = 2.9<ce:hsp sp=\"0.25\"></ce:hsp>Oe (magnetic field // BD), relative permeability <ce:italic>μ</ce:italic> = 51.6 (<ce:italic>f</ce:italic> = 100<ce:hsp sp=\"0.25\"></ce:hsp>kHz), and power loss <ce:italic>P</ce:italic><ce:inf loc=\"post\"><ce:italic>cv</ce:italic></ce:inf> = 728.39<ce:hsp sp=\"0.25\"></ce:hsp>mW/cm<ce:sup loc=\"post\">3</ce:sup> (<ce:italic>B</ce:italic><ce:inf loc=\"post\"><ce:italic>m</ce:italic></ce:inf> = 20 mT, <ce:italic>f</ce:italic> = 100<ce:hsp sp=\"0.25\"></ce:hsp>kHz) were achieved.","PeriodicalId":344,"journal":{"name":"Journal of Alloys and Compounds","volume":"46 1","pages":""},"PeriodicalIF":6.3000,"publicationDate":"2025-06-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Microstructure and soft magnetic behavior of FeSiAl soft magnetic alloys fabricated via selective laser melting\",\"authors\":\"Feng-Hui Wang, Cai-Yin You, Bing-Xu Liu, He-Guang Liu, Jing Zhang, Xiao-Pei Zhu, Na Tian\",\"doi\":\"10.1016/j.jallcom.2025.181940\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"FeSiAl magnetic cores are extensively utilized in power electronic devices. Additive manufacturing techniques, particularly selective laser melting (SLM), are increasingly employed to fabricate magnetic cores, meeting the demands for miniaturization and integration of electronic systems. This study fabricated FeSiAl magnetic cores <ce:italic>via</ce:italic> SLM, with varying line laser energy densities (LED). The correlation between LED and microstructure was examined from the perspective of rapid solidification. Grain morphology was dominated by equiaxed crystals in the cross-sectional plane (x-y) and columnar crystals in the longitudinal planes (x-z and y-z). Notably, the printed samples exhibit alternating coarse and fine grain zones, with Si element enrichment observed at melt pool boundaries. Increasing LED reduces defects and promotes larger grain growth, with the strongest texture (7.64) along the building direction (BD) observed at an LED of 167<ce:hsp sp=\\\"0.25\\\"></ce:hsp>J/m. For the sample processed at LED = 167<ce:hsp sp=\\\"0.25\\\"></ce:hsp>J/m, a saturation magnetization of <ce:italic>M</ce:italic><ce:inf loc=\\\"post\\\"><ce:italic>s</ce:italic></ce:inf> = 124.3<ce:hsp sp=\\\"0.25\\\"></ce:hsp>emu/g, coercivity of <ce:italic>H</ce:italic><ce:inf loc=\\\"post\\\"><ce:italic>c</ce:italic></ce:inf> = 2.9<ce:hsp sp=\\\"0.25\\\"></ce:hsp>Oe (magnetic field // BD), relative permeability <ce:italic>μ</ce:italic> = 51.6 (<ce:italic>f</ce:italic> = 100<ce:hsp sp=\\\"0.25\\\"></ce:hsp>kHz), and power loss <ce:italic>P</ce:italic><ce:inf loc=\\\"post\\\"><ce:italic>cv</ce:italic></ce:inf> = 728.39<ce:hsp sp=\\\"0.25\\\"></ce:hsp>mW/cm<ce:sup loc=\\\"post\\\">3</ce:sup> (<ce:italic>B</ce:italic><ce:inf loc=\\\"post\\\"><ce:italic>m</ce:italic></ce:inf> = 20 mT, <ce:italic>f</ce:italic> = 100<ce:hsp sp=\\\"0.25\\\"></ce:hsp>kHz) were achieved.\",\"PeriodicalId\":344,\"journal\":{\"name\":\"Journal of Alloys and Compounds\",\"volume\":\"46 1\",\"pages\":\"\"},\"PeriodicalIF\":6.3000,\"publicationDate\":\"2025-06-29\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Alloys and Compounds\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://doi.org/10.1016/j.jallcom.2025.181940\",\"RegionNum\":2,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"CHEMISTRY, PHYSICAL\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Alloys and Compounds","FirstCategoryId":"88","ListUrlMain":"https://doi.org/10.1016/j.jallcom.2025.181940","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"CHEMISTRY, PHYSICAL","Score":null,"Total":0}
Microstructure and soft magnetic behavior of FeSiAl soft magnetic alloys fabricated via selective laser melting
FeSiAl magnetic cores are extensively utilized in power electronic devices. Additive manufacturing techniques, particularly selective laser melting (SLM), are increasingly employed to fabricate magnetic cores, meeting the demands for miniaturization and integration of electronic systems. This study fabricated FeSiAl magnetic cores via SLM, with varying line laser energy densities (LED). The correlation between LED and microstructure was examined from the perspective of rapid solidification. Grain morphology was dominated by equiaxed crystals in the cross-sectional plane (x-y) and columnar crystals in the longitudinal planes (x-z and y-z). Notably, the printed samples exhibit alternating coarse and fine grain zones, with Si element enrichment observed at melt pool boundaries. Increasing LED reduces defects and promotes larger grain growth, with the strongest texture (7.64) along the building direction (BD) observed at an LED of 167J/m. For the sample processed at LED = 167J/m, a saturation magnetization of Ms = 124.3emu/g, coercivity of Hc = 2.9Oe (magnetic field // BD), relative permeability μ = 51.6 (f = 100kHz), and power loss Pcv = 728.39mW/cm3 (Bm = 20 mT, f = 100kHz) were achieved.
期刊介绍:
The Journal of Alloys and Compounds is intended to serve as an international medium for the publication of work on solid materials comprising compounds as well as alloys. Its great strength lies in the diversity of discipline which it encompasses, drawing together results from materials science, solid-state chemistry and physics.