Qiang Wang , Zhao-Hui Zhang , Xing-Wang Cheng , Xiao-Tong Jia , Yang-Yu He , Jin-Zhao Zhou , Yuan-Hao Sun , Xian-Yu Li
{"title":"通过火花等离子烧结和热处理,获得了优异的(TiC + (TiZr)5Si3)/TA15复合材料的高温强度","authors":"Qiang Wang , Zhao-Hui Zhang , Xing-Wang Cheng , Xiao-Tong Jia , Yang-Yu He , Jin-Zhao Zhou , Yuan-Hao Sun , Xian-Yu Li","doi":"10.1016/j.coco.2025.102520","DOIUrl":null,"url":null,"abstract":"<div><div>To further enhance the mechanical performance of as-sintered (TiC + (TiZr)<sub>5</sub>Si<sub>3</sub>)/TA15 composites, this study explores the influence of heat treatment on their microstructure and mechanical behavior. Following solution treatment at 1100 °C for 30 min and subsequent water quenching, the matrix transforms entirely into α′ martensite. The TiC particles retain a stable quasi-continuous network distribution, while the (TiZr)<sub>5</sub>Si<sub>3</sub> particles dissolve back into the matrix. After quenching, the composite achieves outstanding compressive properties at room temperature, including a yield strength of 1442 MPa, an ultimate compressive strength of 2178 MPa, and a fracture strain of 25.8 %. At 650 °C, it demonstrates a tensile strength of 835 MPa and an elongation of 18.5 %. Subsequent aging at 600 °C for 300 min results in the α′ martensitic structure without significant decomposition, and (TiZr)<sub>5</sub>Si<sub>3</sub> particles re-precipitate within the quasi-continuous network. After solution + aging treatment, the room-temperature compressive yield strength increases to 1617 MPa, representing a 35.0 % improvement over the as-sintered condition. At 650 °C, the tensile strength rises to 887 MPa, marking a 51.6 % increase compared to the as-sintered composite. The remarkable enhancement in mechanical performance following heat treatment is primarily attributed to the combined effects of α′ martensite strengthening, dislocation strengthening, and solid solution strengthening.</div></div>","PeriodicalId":10533,"journal":{"name":"Composites Communications","volume":"58 ","pages":"Article 102520"},"PeriodicalIF":7.7000,"publicationDate":"2025-06-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Attaining superior high-temperature strength in (TiC + (TiZr)5Si3)/TA15 composites through spark plasma sintering and heat treatment\",\"authors\":\"Qiang Wang , Zhao-Hui Zhang , Xing-Wang Cheng , Xiao-Tong Jia , Yang-Yu He , Jin-Zhao Zhou , Yuan-Hao Sun , Xian-Yu Li\",\"doi\":\"10.1016/j.coco.2025.102520\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>To further enhance the mechanical performance of as-sintered (TiC + (TiZr)<sub>5</sub>Si<sub>3</sub>)/TA15 composites, this study explores the influence of heat treatment on their microstructure and mechanical behavior. Following solution treatment at 1100 °C for 30 min and subsequent water quenching, the matrix transforms entirely into α′ martensite. The TiC particles retain a stable quasi-continuous network distribution, while the (TiZr)<sub>5</sub>Si<sub>3</sub> particles dissolve back into the matrix. After quenching, the composite achieves outstanding compressive properties at room temperature, including a yield strength of 1442 MPa, an ultimate compressive strength of 2178 MPa, and a fracture strain of 25.8 %. At 650 °C, it demonstrates a tensile strength of 835 MPa and an elongation of 18.5 %. Subsequent aging at 600 °C for 300 min results in the α′ martensitic structure without significant decomposition, and (TiZr)<sub>5</sub>Si<sub>3</sub> particles re-precipitate within the quasi-continuous network. After solution + aging treatment, the room-temperature compressive yield strength increases to 1617 MPa, representing a 35.0 % improvement over the as-sintered condition. At 650 °C, the tensile strength rises to 887 MPa, marking a 51.6 % increase compared to the as-sintered composite. The remarkable enhancement in mechanical performance following heat treatment is primarily attributed to the combined effects of α′ martensite strengthening, dislocation strengthening, and solid solution strengthening.</div></div>\",\"PeriodicalId\":10533,\"journal\":{\"name\":\"Composites Communications\",\"volume\":\"58 \",\"pages\":\"Article 102520\"},\"PeriodicalIF\":7.7000,\"publicationDate\":\"2025-06-26\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Composites Communications\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S2452213925002736\",\"RegionNum\":2,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"MATERIALS SCIENCE, COMPOSITES\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Composites Communications","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S2452213925002736","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"MATERIALS SCIENCE, COMPOSITES","Score":null,"Total":0}
Attaining superior high-temperature strength in (TiC + (TiZr)5Si3)/TA15 composites through spark plasma sintering and heat treatment
To further enhance the mechanical performance of as-sintered (TiC + (TiZr)5Si3)/TA15 composites, this study explores the influence of heat treatment on their microstructure and mechanical behavior. Following solution treatment at 1100 °C for 30 min and subsequent water quenching, the matrix transforms entirely into α′ martensite. The TiC particles retain a stable quasi-continuous network distribution, while the (TiZr)5Si3 particles dissolve back into the matrix. After quenching, the composite achieves outstanding compressive properties at room temperature, including a yield strength of 1442 MPa, an ultimate compressive strength of 2178 MPa, and a fracture strain of 25.8 %. At 650 °C, it demonstrates a tensile strength of 835 MPa and an elongation of 18.5 %. Subsequent aging at 600 °C for 300 min results in the α′ martensitic structure without significant decomposition, and (TiZr)5Si3 particles re-precipitate within the quasi-continuous network. After solution + aging treatment, the room-temperature compressive yield strength increases to 1617 MPa, representing a 35.0 % improvement over the as-sintered condition. At 650 °C, the tensile strength rises to 887 MPa, marking a 51.6 % increase compared to the as-sintered composite. The remarkable enhancement in mechanical performance following heat treatment is primarily attributed to the combined effects of α′ martensite strengthening, dislocation strengthening, and solid solution strengthening.
期刊介绍:
Composites Communications (Compos. Commun.) is a peer-reviewed journal publishing short communications and letters on the latest advances in composites science and technology. With a rapid review and publication process, its goal is to disseminate new knowledge promptly within the composites community. The journal welcomes manuscripts presenting creative concepts and new findings in design, state-of-the-art approaches in processing, synthesis, characterization, and mechanics modeling. In addition to traditional fiber-/particulate-reinforced engineering composites, it encourages submissions on composites with exceptional physical, mechanical, and fracture properties, as well as those with unique functions and significant application potential. This includes biomimetic and bio-inspired composites for biomedical applications, functional nano-composites for thermal management and energy applications, and composites designed for extreme service environments.