不锈钢应力腐蚀开裂的原位腐蚀小冲孔试验。

IF 2.4 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING
Experimental Mechanics Pub Date : 2025-01-01 Epub Date: 2025-03-27 DOI:10.1007/s11340-025-01177-y
K Yuan, M Mokhtarishirazabad, S Mckendrey, R Clark, M Peel, M Mostafavi
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引用次数: 0

摘要

背景:先进气冷堆乏燃料包壳在冷却池的过渡贮存期间可能发生应力腐蚀开裂(SCC),影响燃料贮存的结构完整性。目的:为了更好地了解SCC的影响,本研究开发了一种新的小冲孔试验(SPT)装置,该装置可以使用小体积的样品来限制对辐照材料的安全担忧。方法:SPT通过引入加热的腐蚀性溶液循环,在304不锈钢替代材料中加速SCC。进行了初步试验,以找出在替代材料中可能发生SCC的负载和环境条件。采用有限元模型对材料在试验过程中的力学行为进行了估计。结果:几个样品在不同的条件下进行了测试,并在样品上观察到SCC和其他形式的腐蚀行为。通过进一步的表征,包括扫描电子显微镜(SEM)和光学轮廓术,获得了不同腐蚀环境的影响。结论:实验表明,新装置可以在短时间内从小体积的样品中培养出SCC。提出了若干改进措施,包括增加了对辐照燃料材料进行实验的程序。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
An In-Situ Corrosion Small Punch Test for Developing Stress Corrosion Cracking in Stainless Steel.

Background: Spent AGR (advanced gas-cooled reactor) fuel cladding may suffer from stress corrosion cracking (SCC) during the interim storage period in cooling ponds and compromise the structural integrity of fuel storage.

Objective: To better understand the effect of SCC, a new small punch test (SPT) setup was developed in this study that can use a small volume of sample to limit the safety concerns about irradiated materials.

Methods: The SPT setup accelerated SCC in a surrogate material 304 stainless steel by introducing a circulation of a heated corrosive solution. Preliminary tests were performed to find the loading and environmental conditions that can develop SCC in the surrogate material. A finite element model was used to estimate the mechanical behaviour of the material during the test.

Results: Several samples were tested under different conditions, and SCC and other forms of corrosion behaviours were observed on the samples. The effects of different corrosive environments were obtained by further characterisation including scanning electron microscopy (SEM) and optical profilometry.

Conclusions: The experiment demonstrated the new setup can develop SCC from a small volume of sample in a short period of time. Several improvements are listed including extra procedures to enable the experiments on the irradiated fuel materials.

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来源期刊
Experimental Mechanics
Experimental Mechanics 物理-材料科学:表征与测试
CiteScore
4.40
自引率
16.70%
发文量
111
审稿时长
3 months
期刊介绍: Experimental Mechanics is the official journal of the Society for Experimental Mechanics that publishes papers in all areas of experimentation including its theoretical and computational analysis. The journal covers research in design and implementation of novel or improved experiments to characterize materials, structures and systems. Articles extending the frontiers of experimental mechanics at large and small scales are particularly welcome. Coverage extends from research in solid and fluids mechanics to fields at the intersection of disciplines including physics, chemistry and biology. Development of new devices and technologies for metrology applications in a wide range of industrial sectors (e.g., manufacturing, high-performance materials, aerospace, information technology, medicine, energy and environmental technologies) is also covered.
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