Zhelin Dong , Chunguang Wang , Kaining Zhang , Chongpu Zhai , Hanlin Wang , Feifei Zhu , Xiaoying Wang
{"title":"复合推进剂的细观损伤演化及速率相关孔隙率的原位x射线层析预测模型","authors":"Zhelin Dong , Chunguang Wang , Kaining Zhang , Chongpu Zhai , Hanlin Wang , Feifei Zhu , Xiaoying Wang","doi":"10.1016/j.compscitech.2025.111267","DOIUrl":null,"url":null,"abstract":"<div><div>Nitrate ester plasticized polyether (NEPE) composite propellant is widely used in solid rocket motors, serving as the power source of the launch vehicles. The propellant is always subjected to complex mechanical loads during the service, which could induce mesoscopic damage represented by cracks and pores, then eventually reduces carrying capacity of the composite. To illustrate the internal damage evolution mechanisms of NEPE propellant under uniaxial tension, this study developed an <em>in situ</em> X-ray tomography to extract the changing of mesosturctures at different strain rates, then reconstruction of components and pores was conducted to track the damage morphologies’ evolution. As the interfacial debonding preferred to initiate at the large particles, the debonded interfaces would grow into pores with extension of strain, then formed different damage morphologies depending on mesostructures. In addition, the porosity evolution was analyzed at different strain rates, which presented distinct rate-dependent characteristics. By introducing critical debonding stress criteria with a pore evolution model, a rate-dependent porosity prediction model was proposed, and this model provided an excellent agreement with experiment results, which is valuable to damage assessment and integrity analysis of the composite propellant.</div></div>","PeriodicalId":283,"journal":{"name":"Composites Science and Technology","volume":"270 ","pages":"Article 111267"},"PeriodicalIF":8.3000,"publicationDate":"2025-06-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Mesoscopic damage evolution and rate-dependent porosity prediction model of a composite propellant by in situ X-ray tomography\",\"authors\":\"Zhelin Dong , Chunguang Wang , Kaining Zhang , Chongpu Zhai , Hanlin Wang , Feifei Zhu , Xiaoying Wang\",\"doi\":\"10.1016/j.compscitech.2025.111267\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>Nitrate ester plasticized polyether (NEPE) composite propellant is widely used in solid rocket motors, serving as the power source of the launch vehicles. The propellant is always subjected to complex mechanical loads during the service, which could induce mesoscopic damage represented by cracks and pores, then eventually reduces carrying capacity of the composite. To illustrate the internal damage evolution mechanisms of NEPE propellant under uniaxial tension, this study developed an <em>in situ</em> X-ray tomography to extract the changing of mesosturctures at different strain rates, then reconstruction of components and pores was conducted to track the damage morphologies’ evolution. As the interfacial debonding preferred to initiate at the large particles, the debonded interfaces would grow into pores with extension of strain, then formed different damage morphologies depending on mesostructures. In addition, the porosity evolution was analyzed at different strain rates, which presented distinct rate-dependent characteristics. By introducing critical debonding stress criteria with a pore evolution model, a rate-dependent porosity prediction model was proposed, and this model provided an excellent agreement with experiment results, which is valuable to damage assessment and integrity analysis of the composite propellant.</div></div>\",\"PeriodicalId\":283,\"journal\":{\"name\":\"Composites Science and Technology\",\"volume\":\"270 \",\"pages\":\"Article 111267\"},\"PeriodicalIF\":8.3000,\"publicationDate\":\"2025-06-09\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Composites Science and Technology\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S0266353825002350\",\"RegionNum\":1,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"MATERIALS SCIENCE, COMPOSITES\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Composites Science and Technology","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0266353825002350","RegionNum":1,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"MATERIALS SCIENCE, COMPOSITES","Score":null,"Total":0}
Mesoscopic damage evolution and rate-dependent porosity prediction model of a composite propellant by in situ X-ray tomography
Nitrate ester plasticized polyether (NEPE) composite propellant is widely used in solid rocket motors, serving as the power source of the launch vehicles. The propellant is always subjected to complex mechanical loads during the service, which could induce mesoscopic damage represented by cracks and pores, then eventually reduces carrying capacity of the composite. To illustrate the internal damage evolution mechanisms of NEPE propellant under uniaxial tension, this study developed an in situ X-ray tomography to extract the changing of mesosturctures at different strain rates, then reconstruction of components and pores was conducted to track the damage morphologies’ evolution. As the interfacial debonding preferred to initiate at the large particles, the debonded interfaces would grow into pores with extension of strain, then formed different damage morphologies depending on mesostructures. In addition, the porosity evolution was analyzed at different strain rates, which presented distinct rate-dependent characteristics. By introducing critical debonding stress criteria with a pore evolution model, a rate-dependent porosity prediction model was proposed, and this model provided an excellent agreement with experiment results, which is valuable to damage assessment and integrity analysis of the composite propellant.
期刊介绍:
Composites Science and Technology publishes refereed original articles on the fundamental and applied science of engineering composites. The focus of this journal is on polymeric matrix composites with reinforcements/fillers ranging from nano- to macro-scale. CSTE encourages manuscripts reporting unique, innovative contributions to the physics, chemistry, materials science and applied mechanics aspects of advanced composites.
Besides traditional fiber reinforced composites, novel composites with significant potential for engineering applications are encouraged.