Chenglin Zhang , Xian Luo , Zeyang Wu , Hang Zou , Rui Hu , Nizhi Zhai
{"title":"两步强化:有助于提高TiBw/TC4复合材料的强度和保持塑性","authors":"Chenglin Zhang , Xian Luo , Zeyang Wu , Hang Zou , Rui Hu , Nizhi Zhai","doi":"10.1016/j.compositesa.2025.109115","DOIUrl":null,"url":null,"abstract":"<div><div>The long-term demand for high strength and high toughness drives the development of titanium matrix composites (TMCs). In this work, the room temperature mechanical properties of TiB<sub>w</sub>/TC4 composites prepared by two-step low-energy ball milling and vacuum hot-pressing sintering (HPS) were successfully improved by two-step strengthening strategy. The synergistic optimization of strength and plasticity was achieved by using the grain bimodal heterogeneous design combined with the quenching and aging heat treatment process. The tensile strength and elongation of the as-HPSed composite with 10 wt% coarse-grained TC4 (CG) are 1129 MPa and 4.3 %, respectively, which are 17.2 % and 38.7 % higher than those of the TC4 matrix. After 910 ℃/1h quenching and 500 ℃/6h aging treatment, the composite exhibits more excellent comprehensive properties. The tensile strength is increased to 1202.5 MPa and the elongation still keeps to be 4.1 %. At the same time, the fracture toughness is 31.2 MPa <span><math><mrow><msqrt><mrow><mtext>m</mtext></mrow></msqrt></mrow></math></span>, which is 37.4 % higher than that of the untreated homogeneous composite. The strengthening mechanism analysis reveals that the synergistic effect of grain boundary strengthening, load transfer strengthening and dislocation strengthening is the key to strength improvement.</div></div>","PeriodicalId":282,"journal":{"name":"Composites Part A: Applied Science and Manufacturing","volume":"198 ","pages":"Article 109115"},"PeriodicalIF":8.1000,"publicationDate":"2025-06-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Two-step strengthening: Assist in enhancing the strength and maintaining plasticity of TiBw/TC4 composites\",\"authors\":\"Chenglin Zhang , Xian Luo , Zeyang Wu , Hang Zou , Rui Hu , Nizhi Zhai\",\"doi\":\"10.1016/j.compositesa.2025.109115\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>The long-term demand for high strength and high toughness drives the development of titanium matrix composites (TMCs). In this work, the room temperature mechanical properties of TiB<sub>w</sub>/TC4 composites prepared by two-step low-energy ball milling and vacuum hot-pressing sintering (HPS) were successfully improved by two-step strengthening strategy. The synergistic optimization of strength and plasticity was achieved by using the grain bimodal heterogeneous design combined with the quenching and aging heat treatment process. The tensile strength and elongation of the as-HPSed composite with 10 wt% coarse-grained TC4 (CG) are 1129 MPa and 4.3 %, respectively, which are 17.2 % and 38.7 % higher than those of the TC4 matrix. After 910 ℃/1h quenching and 500 ℃/6h aging treatment, the composite exhibits more excellent comprehensive properties. The tensile strength is increased to 1202.5 MPa and the elongation still keeps to be 4.1 %. At the same time, the fracture toughness is 31.2 MPa <span><math><mrow><msqrt><mrow><mtext>m</mtext></mrow></msqrt></mrow></math></span>, which is 37.4 % higher than that of the untreated homogeneous composite. The strengthening mechanism analysis reveals that the synergistic effect of grain boundary strengthening, load transfer strengthening and dislocation strengthening is the key to strength improvement.</div></div>\",\"PeriodicalId\":282,\"journal\":{\"name\":\"Composites Part A: Applied Science and Manufacturing\",\"volume\":\"198 \",\"pages\":\"Article 109115\"},\"PeriodicalIF\":8.1000,\"publicationDate\":\"2025-06-14\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Composites Part A: Applied Science and Manufacturing\",\"FirstCategoryId\":\"1\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S1359835X25004099\",\"RegionNum\":2,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"ENGINEERING, MANUFACTURING\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Composites Part A: Applied Science and Manufacturing","FirstCategoryId":"1","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S1359835X25004099","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"ENGINEERING, MANUFACTURING","Score":null,"Total":0}
Two-step strengthening: Assist in enhancing the strength and maintaining plasticity of TiBw/TC4 composites
The long-term demand for high strength and high toughness drives the development of titanium matrix composites (TMCs). In this work, the room temperature mechanical properties of TiBw/TC4 composites prepared by two-step low-energy ball milling and vacuum hot-pressing sintering (HPS) were successfully improved by two-step strengthening strategy. The synergistic optimization of strength and plasticity was achieved by using the grain bimodal heterogeneous design combined with the quenching and aging heat treatment process. The tensile strength and elongation of the as-HPSed composite with 10 wt% coarse-grained TC4 (CG) are 1129 MPa and 4.3 %, respectively, which are 17.2 % and 38.7 % higher than those of the TC4 matrix. After 910 ℃/1h quenching and 500 ℃/6h aging treatment, the composite exhibits more excellent comprehensive properties. The tensile strength is increased to 1202.5 MPa and the elongation still keeps to be 4.1 %. At the same time, the fracture toughness is 31.2 MPa , which is 37.4 % higher than that of the untreated homogeneous composite. The strengthening mechanism analysis reveals that the synergistic effect of grain boundary strengthening, load transfer strengthening and dislocation strengthening is the key to strength improvement.
期刊介绍:
Composites Part A: Applied Science and Manufacturing is a comprehensive journal that publishes original research papers, review articles, case studies, short communications, and letters covering various aspects of composite materials science and technology. This includes fibrous and particulate reinforcements in polymeric, metallic, and ceramic matrices, as well as 'natural' composites like wood and biological materials. The journal addresses topics such as properties, design, and manufacture of reinforcing fibers and particles, novel architectures and concepts, multifunctional composites, advancements in fabrication and processing, manufacturing science, process modeling, experimental mechanics, microstructural characterization, interfaces, prediction and measurement of mechanical, physical, and chemical behavior, and performance in service. Additionally, articles on economic and commercial aspects, design, and case studies are welcomed. All submissions undergo rigorous peer review to ensure they contribute significantly and innovatively, maintaining high standards for content and presentation. The editorial team aims to expedite the review process for prompt publication.