Hang Xu, Yang Mo, Fulin Jiang, Luoyi Wu, Jie Tang, Jie Teng, Hui Zhang
{"title":"Mg-2Y-1Zn合金双级热压缩变形后的软化硬化机制","authors":"Hang Xu, Yang Mo, Fulin Jiang, Luoyi Wu, Jie Tang, Jie Teng, Hui Zhang","doi":"10.1016/j.jma.2025.05.005","DOIUrl":null,"url":null,"abstract":"Multi-pass hot processing methods are commonly used in magnesium (Mg) alloys to overcome the poor workability due to limited slip systems, which generally involve complicated post-deformation softening and hardening behaviors. In this work, to reveal post-deformation softening and hardening mechanisms of a Mg-2Y-1 Zn alloy, double-stage hot compression tests and microstructural observations were conducted. The results showed that the softening fraction of Mg-2Y-1 Zn alloy showed a non-linear dependence on deformation conditions and could be general coupled by <em>Z</em> parameter. Due to the formation and cross-overlapping of twins and kinks, only static recovery (SRV) occurred during holding process at 300 °C/0.001 s<sup>-1</sup> which led to the least static softening: 5.52 % after 10 s of holding. For samples at 400 °C/0.001s<sup>-1</sup>, the enhanced post-deformation softening, which is 11.93 % after 10 s of holding, was attributed to static recrystallization (SRX) followed continuous dynamic recrystallization (CDRX) happened during first deformation stage as well as SRV influenced by the LPSO phases. Under deformation condition of 400 °C/0.1 s<sup>-1</sup>, the coupled meta-dynamic recrystallization (MDRX) and SRX resulted in serious stress relaxation, which is 42.83 % after 10 s of holding, and caused hardening phenomenon at reloading stage. The 18R-LPSO and 14H-LPSO phases synchronously worked on deformation behaviors and limited the growth of recrystallized grains. Further, a simplified static softening kinetics model was established based on Johnson-Mehl-Avrami-Kolmogorov equation and employed to rationalize experimental data.","PeriodicalId":16214,"journal":{"name":"Journal of Magnesium and Alloys","volume":"39 1","pages":""},"PeriodicalIF":13.8000,"publicationDate":"2025-06-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"The post-deformation softening and hardening mechanisms of a Mg-2Y-1Zn alloy during double-stage hot compression\",\"authors\":\"Hang Xu, Yang Mo, Fulin Jiang, Luoyi Wu, Jie Tang, Jie Teng, Hui Zhang\",\"doi\":\"10.1016/j.jma.2025.05.005\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Multi-pass hot processing methods are commonly used in magnesium (Mg) alloys to overcome the poor workability due to limited slip systems, which generally involve complicated post-deformation softening and hardening behaviors. In this work, to reveal post-deformation softening and hardening mechanisms of a Mg-2Y-1 Zn alloy, double-stage hot compression tests and microstructural observations were conducted. The results showed that the softening fraction of Mg-2Y-1 Zn alloy showed a non-linear dependence on deformation conditions and could be general coupled by <em>Z</em> parameter. Due to the formation and cross-overlapping of twins and kinks, only static recovery (SRV) occurred during holding process at 300 °C/0.001 s<sup>-1</sup> which led to the least static softening: 5.52 % after 10 s of holding. For samples at 400 °C/0.001s<sup>-1</sup>, the enhanced post-deformation softening, which is 11.93 % after 10 s of holding, was attributed to static recrystallization (SRX) followed continuous dynamic recrystallization (CDRX) happened during first deformation stage as well as SRV influenced by the LPSO phases. Under deformation condition of 400 °C/0.1 s<sup>-1</sup>, the coupled meta-dynamic recrystallization (MDRX) and SRX resulted in serious stress relaxation, which is 42.83 % after 10 s of holding, and caused hardening phenomenon at reloading stage. The 18R-LPSO and 14H-LPSO phases synchronously worked on deformation behaviors and limited the growth of recrystallized grains. Further, a simplified static softening kinetics model was established based on Johnson-Mehl-Avrami-Kolmogorov equation and employed to rationalize experimental data.\",\"PeriodicalId\":16214,\"journal\":{\"name\":\"Journal of Magnesium and Alloys\",\"volume\":\"39 1\",\"pages\":\"\"},\"PeriodicalIF\":13.8000,\"publicationDate\":\"2025-06-06\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Magnesium and Alloys\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://doi.org/10.1016/j.jma.2025.05.005\",\"RegionNum\":1,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"METALLURGY & METALLURGICAL ENGINEERING\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Magnesium and Alloys","FirstCategoryId":"88","ListUrlMain":"https://doi.org/10.1016/j.jma.2025.05.005","RegionNum":1,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"METALLURGY & METALLURGICAL ENGINEERING","Score":null,"Total":0}
The post-deformation softening and hardening mechanisms of a Mg-2Y-1Zn alloy during double-stage hot compression
Multi-pass hot processing methods are commonly used in magnesium (Mg) alloys to overcome the poor workability due to limited slip systems, which generally involve complicated post-deformation softening and hardening behaviors. In this work, to reveal post-deformation softening and hardening mechanisms of a Mg-2Y-1 Zn alloy, double-stage hot compression tests and microstructural observations were conducted. The results showed that the softening fraction of Mg-2Y-1 Zn alloy showed a non-linear dependence on deformation conditions and could be general coupled by Z parameter. Due to the formation and cross-overlapping of twins and kinks, only static recovery (SRV) occurred during holding process at 300 °C/0.001 s-1 which led to the least static softening: 5.52 % after 10 s of holding. For samples at 400 °C/0.001s-1, the enhanced post-deformation softening, which is 11.93 % after 10 s of holding, was attributed to static recrystallization (SRX) followed continuous dynamic recrystallization (CDRX) happened during first deformation stage as well as SRV influenced by the LPSO phases. Under deformation condition of 400 °C/0.1 s-1, the coupled meta-dynamic recrystallization (MDRX) and SRX resulted in serious stress relaxation, which is 42.83 % after 10 s of holding, and caused hardening phenomenon at reloading stage. The 18R-LPSO and 14H-LPSO phases synchronously worked on deformation behaviors and limited the growth of recrystallized grains. Further, a simplified static softening kinetics model was established based on Johnson-Mehl-Avrami-Kolmogorov equation and employed to rationalize experimental data.
期刊介绍:
The Journal of Magnesium and Alloys serves as a global platform for both theoretical and experimental studies in magnesium science and engineering. It welcomes submissions investigating various scientific and engineering factors impacting the metallurgy, processing, microstructure, properties, and applications of magnesium and alloys. The journal covers all aspects of magnesium and alloy research, including raw materials, alloy casting, extrusion and deformation, corrosion and surface treatment, joining and machining, simulation and modeling, microstructure evolution and mechanical properties, new alloy development, magnesium-based composites, bio-materials and energy materials, applications, and recycling.