以碱性离子液体[(HOCH2)2C(CH3)NH3+][HCOO−]为绿色催化剂合成（羟甲基）（甲基磺酰基）吡喃[3,2-b]吡喃衍生物

IF 2.1 3区化学 Q2 CHEMISTRY, ORGANIC

Tetrahedron Pub Date : 2025-05-27 DOI:10.1016/j.tet.2025.134755

Farhad Shirzaei, Hamid Reza Shaterian

引用次数: 0

摘要

合成了稳定的离子液体催化剂[(HOCH2)2C(CH3)NH3+][HCOO−]。用该催化剂在回流条件下成功制备了新的（羟甲基）（甲基磺酰基）吡喃[3,2-b]吡喃化合物。方法简便、反应时间短、溶剂环保、产品收率高是本研究的优点。该催化剂在连续5次循环使用的情况下，没有失去催化活性。

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Synthesis of (hydroxymethyl)(methylsulfonyl)pyrano[3,2-b]pyran derivatives using a basic ionic liquid, [(HOCH2)2C(CH3)NH3+][HCOO−], as a green catalyst

A stable ionic liquid catalyst, [(HOCH₂)₂C(CH₃)NH₃⁺][HCOO⁻], was synthesized. New (hydroxymethyl)(methylsulfonyl)pyrano[3,2-b]pyran compounds were successfully prepared by the mentioned catalyst under refluxing conditions. Easy working method, short reaction times, green solvent, and high yield of products are the advantages of this research. The catalyst was recycled and reused for five consecutive times without loss of its catalytic activity.

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来源期刊

Tetrahedron 化学-有机化学

CiteScore

3.90

自引率

4.80%

发文量

439

审稿时长

34 days

期刊介绍： Tetrahedron publishes full accounts of research having outstanding significance in the broad field of organic chemistry and its related disciplines, such as organic materials and bio-organic chemistry. Regular papers in Tetrahedron are expected to represent detailed accounts of an original study having substantially greater scope and details than that found in a communication, as published in Tetrahedron Letters. Tetrahedron also publishes thematic collections of papers as special issues and ''Reports'', commissioned in-depth reviews providing a comprehensive overview of a research area.