{"title":"新型生物活性炭填充环氧复合材料的合成。","authors":"Hatice Karaer Yağmur, Kübra Baykara, Seyithan Sönmez","doi":"10.1080/10826068.2025.2509307","DOIUrl":null,"url":null,"abstract":"<p><p>In this study, active carbons were obtained by carbonizing waste laurel fruit seeds at 500 °C for 1 hour. The surface area of the activated carbon obtained using the ZnCl<sub>2</sub> activator was determined as 873.93 m<sup>2</sup>/g while the surface area of the activated carbon obtained without using the activator was determined as 1.52 m<sup>2</sup>/g. Furthermore, in order to obtain epoxy composites with improved mechanical and thermal properties, activated carbons were added to epoxy as filler at rates of 0%, 5% and 10% and bio-based epoxy composites were obtained. Epoxy composites were produced using a mold prepared according to ASTM D638 TYPE I standard. Thermal and tensile properties of filled and unfilled epoxy composites were investigated. LOI values of NE, N5, N10, A5 and A10 composites were determined as 23.48, 24.28, 25.32, 26.55 and 27.06, respectively. Surface hardness and tensile strength of composites containing activated carbon were found to be higher than pure epoxy composite. The tensile test results obtained for NE, N5, N10, A5 and A10 were as follows: elongation percentages at break were 5.37%, 1.80%, 11.59%, 2.21% and 1.61% and tensile stress were 19.12, 11.52, 13.63, 16.45 and 20.33 N/mm<sup>2</sup>.</p>","PeriodicalId":20401,"journal":{"name":"Preparative Biochemistry & Biotechnology","volume":" ","pages":"1-10"},"PeriodicalIF":2.0000,"publicationDate":"2025-05-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Synthesis of new bio-activated carbon filled epoxy composites.\",\"authors\":\"Hatice Karaer Yağmur, Kübra Baykara, Seyithan Sönmez\",\"doi\":\"10.1080/10826068.2025.2509307\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p><p>In this study, active carbons were obtained by carbonizing waste laurel fruit seeds at 500 °C for 1 hour. The surface area of the activated carbon obtained using the ZnCl<sub>2</sub> activator was determined as 873.93 m<sup>2</sup>/g while the surface area of the activated carbon obtained without using the activator was determined as 1.52 m<sup>2</sup>/g. Furthermore, in order to obtain epoxy composites with improved mechanical and thermal properties, activated carbons were added to epoxy as filler at rates of 0%, 5% and 10% and bio-based epoxy composites were obtained. Epoxy composites were produced using a mold prepared according to ASTM D638 TYPE I standard. Thermal and tensile properties of filled and unfilled epoxy composites were investigated. LOI values of NE, N5, N10, A5 and A10 composites were determined as 23.48, 24.28, 25.32, 26.55 and 27.06, respectively. Surface hardness and tensile strength of composites containing activated carbon were found to be higher than pure epoxy composite. The tensile test results obtained for NE, N5, N10, A5 and A10 were as follows: elongation percentages at break were 5.37%, 1.80%, 11.59%, 2.21% and 1.61% and tensile stress were 19.12, 11.52, 13.63, 16.45 and 20.33 N/mm<sup>2</sup>.</p>\",\"PeriodicalId\":20401,\"journal\":{\"name\":\"Preparative Biochemistry & Biotechnology\",\"volume\":\" \",\"pages\":\"1-10\"},\"PeriodicalIF\":2.0000,\"publicationDate\":\"2025-05-23\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Preparative Biochemistry & Biotechnology\",\"FirstCategoryId\":\"5\",\"ListUrlMain\":\"https://doi.org/10.1080/10826068.2025.2509307\",\"RegionNum\":4,\"RegionCategory\":\"生物学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q3\",\"JCRName\":\"BIOCHEMICAL RESEARCH METHODS\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Preparative Biochemistry & Biotechnology","FirstCategoryId":"5","ListUrlMain":"https://doi.org/10.1080/10826068.2025.2509307","RegionNum":4,"RegionCategory":"生物学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"BIOCHEMICAL RESEARCH METHODS","Score":null,"Total":0}
引用次数: 0
摘要
在本研究中,将废月桂果种子在500℃下碳化1小时,得到活性炭。使用ZnCl2活化剂得到的活性炭的表面积为873.93 m2/g,而未使用活化剂得到的活性炭的表面积为1.52 m2/g。在环氧树脂中分别添加0%、5%和10%的活性炭作为填料,制备生物基环氧复合材料,从而得到力学性能和热性能均有所改善的环氧复合材料。采用ASTM D638 TYPE I标准制备的模具生产环氧复合材料。研究了填充和未填充环氧复合材料的热拉伸性能。NE、N5、N10、A5和A10复合材料的LOI值分别为23.48、24.28、25.32、26.55和27.06。结果表明,含活性炭复合材料的表面硬度和抗拉强度均高于纯环氧复合材料。拉伸试验结果表明,NE、N5、N10、A5和A10的断裂伸长率分别为5.37%、1.80%、11.59%、2.21%和1.61%,拉伸应力分别为19.12、11.52、13.63、16.45和20.33 N/mm2。
Synthesis of new bio-activated carbon filled epoxy composites.
In this study, active carbons were obtained by carbonizing waste laurel fruit seeds at 500 °C for 1 hour. The surface area of the activated carbon obtained using the ZnCl2 activator was determined as 873.93 m2/g while the surface area of the activated carbon obtained without using the activator was determined as 1.52 m2/g. Furthermore, in order to obtain epoxy composites with improved mechanical and thermal properties, activated carbons were added to epoxy as filler at rates of 0%, 5% and 10% and bio-based epoxy composites were obtained. Epoxy composites were produced using a mold prepared according to ASTM D638 TYPE I standard. Thermal and tensile properties of filled and unfilled epoxy composites were investigated. LOI values of NE, N5, N10, A5 and A10 composites were determined as 23.48, 24.28, 25.32, 26.55 and 27.06, respectively. Surface hardness and tensile strength of composites containing activated carbon were found to be higher than pure epoxy composite. The tensile test results obtained for NE, N5, N10, A5 and A10 were as follows: elongation percentages at break were 5.37%, 1.80%, 11.59%, 2.21% and 1.61% and tensile stress were 19.12, 11.52, 13.63, 16.45 and 20.33 N/mm2.
期刊介绍:
Preparative Biochemistry & Biotechnology is an international forum for rapid dissemination of high quality research results dealing with all aspects of preparative techniques in biochemistry, biotechnology and other life science disciplines.