Qiangkun Wang , Wei Zhang , Pengfei Gao , Lu Wang , Gaige Chang , Baihao Cai , Chenyu Liu , Mengwei Duan , Yong Peng , Kehong Wang
{"title":"热等静压和热处理对CM247LC合金裂纹愈合和强塑性增强的影响","authors":"Qiangkun Wang , Wei Zhang , Pengfei Gao , Lu Wang , Gaige Chang , Baihao Cai , Chenyu Liu , Mengwei Duan , Yong Peng , Kehong Wang","doi":"10.1016/j.matchar.2025.115195","DOIUrl":null,"url":null,"abstract":"<div><div>High crack susceptibility remains a critical challenge in laser powder bed fusion of nickel-based superalloys with high γ'-volume fractions. This study systematically analyzes the crack formation mechanisms, melt pool morphology, and microstructural evolution of CM247LC alloy by optimizing selective laser re-melting (SLRM) parameters (laser power: 176 W, scan speed: 1143 mm/s, hatch spacing: 0.11 mm) combined with hot isostatic pressing (HIP: 1240 °C/150 MPa/4 h) and heat treatment (HT: 1260 °C solution treatment +870 °C aging). Results indicate that cracks primarily propagate along high-angle grain boundaries, with initiation closely linked to elemental segregation (O, Al, C, Ti) and residual stress concentration. Increasing the re-melting volumetric energy density (<em>E</em><sub><em>v</em></sub>) to 56.8 J/mm<sup>3</sup> significantly enhances the melt pool depth-to-width ratio (<em>D</em>/<em>W</em> = 0.62), exacerbating temperature gradients and stress concentrations, thereby elevating crack susceptibility. After SLRM + HIP + HT treatment, the grain aspect ratio decreases from 7.32 to 3.66, while serrated grain boundaries and uniformly distributed γ'-phases effectively inhibit crack propagation and reduce residual stress. The final specimens exhibit exceptional strength-ductility synergy: ultimate tensile strength of 1352 ± 16 MPa, yield strength of 988 ± 25 MPa, and elongation of 11.5 ± 0.8 %, representing improvements of 23.0 %, 18.9 %, and 79.7 %, respectively, compared to the as-built selective laser melting samples.</div></div>","PeriodicalId":18727,"journal":{"name":"Materials Characterization","volume":"225 ","pages":"Article 115195"},"PeriodicalIF":4.8000,"publicationDate":"2025-05-19","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Crack healing and strength-ductility enhancement of CM247LC alloy via laser powder bed re-melting followed by hot isostatic pressing and heat treatment\",\"authors\":\"Qiangkun Wang , Wei Zhang , Pengfei Gao , Lu Wang , Gaige Chang , Baihao Cai , Chenyu Liu , Mengwei Duan , Yong Peng , Kehong Wang\",\"doi\":\"10.1016/j.matchar.2025.115195\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>High crack susceptibility remains a critical challenge in laser powder bed fusion of nickel-based superalloys with high γ'-volume fractions. This study systematically analyzes the crack formation mechanisms, melt pool morphology, and microstructural evolution of CM247LC alloy by optimizing selective laser re-melting (SLRM) parameters (laser power: 176 W, scan speed: 1143 mm/s, hatch spacing: 0.11 mm) combined with hot isostatic pressing (HIP: 1240 °C/150 MPa/4 h) and heat treatment (HT: 1260 °C solution treatment +870 °C aging). Results indicate that cracks primarily propagate along high-angle grain boundaries, with initiation closely linked to elemental segregation (O, Al, C, Ti) and residual stress concentration. Increasing the re-melting volumetric energy density (<em>E</em><sub><em>v</em></sub>) to 56.8 J/mm<sup>3</sup> significantly enhances the melt pool depth-to-width ratio (<em>D</em>/<em>W</em> = 0.62), exacerbating temperature gradients and stress concentrations, thereby elevating crack susceptibility. After SLRM + HIP + HT treatment, the grain aspect ratio decreases from 7.32 to 3.66, while serrated grain boundaries and uniformly distributed γ'-phases effectively inhibit crack propagation and reduce residual stress. The final specimens exhibit exceptional strength-ductility synergy: ultimate tensile strength of 1352 ± 16 MPa, yield strength of 988 ± 25 MPa, and elongation of 11.5 ± 0.8 %, representing improvements of 23.0 %, 18.9 %, and 79.7 %, respectively, compared to the as-built selective laser melting samples.</div></div>\",\"PeriodicalId\":18727,\"journal\":{\"name\":\"Materials Characterization\",\"volume\":\"225 \",\"pages\":\"Article 115195\"},\"PeriodicalIF\":4.8000,\"publicationDate\":\"2025-05-19\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Materials Characterization\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S104458032500484X\",\"RegionNum\":2,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"MATERIALS SCIENCE, CHARACTERIZATION & TESTING\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Materials Characterization","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S104458032500484X","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"MATERIALS SCIENCE, CHARACTERIZATION & TESTING","Score":null,"Total":0}
Crack healing and strength-ductility enhancement of CM247LC alloy via laser powder bed re-melting followed by hot isostatic pressing and heat treatment
High crack susceptibility remains a critical challenge in laser powder bed fusion of nickel-based superalloys with high γ'-volume fractions. This study systematically analyzes the crack formation mechanisms, melt pool morphology, and microstructural evolution of CM247LC alloy by optimizing selective laser re-melting (SLRM) parameters (laser power: 176 W, scan speed: 1143 mm/s, hatch spacing: 0.11 mm) combined with hot isostatic pressing (HIP: 1240 °C/150 MPa/4 h) and heat treatment (HT: 1260 °C solution treatment +870 °C aging). Results indicate that cracks primarily propagate along high-angle grain boundaries, with initiation closely linked to elemental segregation (O, Al, C, Ti) and residual stress concentration. Increasing the re-melting volumetric energy density (Ev) to 56.8 J/mm3 significantly enhances the melt pool depth-to-width ratio (D/W = 0.62), exacerbating temperature gradients and stress concentrations, thereby elevating crack susceptibility. After SLRM + HIP + HT treatment, the grain aspect ratio decreases from 7.32 to 3.66, while serrated grain boundaries and uniformly distributed γ'-phases effectively inhibit crack propagation and reduce residual stress. The final specimens exhibit exceptional strength-ductility synergy: ultimate tensile strength of 1352 ± 16 MPa, yield strength of 988 ± 25 MPa, and elongation of 11.5 ± 0.8 %, representing improvements of 23.0 %, 18.9 %, and 79.7 %, respectively, compared to the as-built selective laser melting samples.
期刊介绍:
Materials Characterization features original articles and state-of-the-art reviews on theoretical and practical aspects of the structure and behaviour of materials.
The Journal focuses on all characterization techniques, including all forms of microscopy (light, electron, acoustic, etc.,) and analysis (especially microanalysis and surface analytical techniques). Developments in both this wide range of techniques and their application to the quantification of the microstructure of materials are essential facets of the Journal.
The Journal provides the Materials Scientist/Engineer with up-to-date information on many types of materials with an underlying theme of explaining the behavior of materials using novel approaches. Materials covered by the journal include:
Metals & Alloys
Ceramics
Nanomaterials
Biomedical materials
Optical materials
Composites
Natural Materials.