从骆驼骨环保产品中提取的新型绿色催化剂和抗菌剂:合成及理化表征

IF 3.5 4区 工程技术 Q3 ENERGY & FUELS
Amr Mohammad Nassar, Wael A. A. Arafa, Khulaif Ashammari, Shaima M. N. Moustafa, Alaa Muqbil Alsirhani, M. F. Hasaneen
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引用次数: 0

摘要

旨在从废物中生产可持续材料的循环经济在环境研究中发挥着重要作用。这项工作的主要目标是重新利用食物垃圾来合成可用的材料。我们在这里描述了一种可持续、绿色、简单、快速和廉价的方法,将废骆驼骨作为一种可再生材料进行有效利用。利用热重分析(TGA)、傅里叶变换红外光谱(FT-IR)、紫外-可见吸收光谱(UV-Vis)、能带间隙、x射线衍射(XRD)、扫描电镜(SEM)和拉曼光谱对回收的骆驼骨(RCB)材料进行了表征。SEM图像显示粒径在100-120 nm之间。RCB作为一种坚固的非均相催化剂在水介质中促进Knoevenagel缩合反应。应用的可持续条件促进了所有衍生物在6个循环8 min后的高收率(≈98%),而活性没有显着变化。评估了骆驼骨、提取的有机物种和提取的羟基磷灰石对蜡样芽孢杆菌、屎肠球菌、大肠杆菌和白色念珠菌等病原微生物的抗菌活性。羟基磷灰石对所研究的微生物菌株的抑菌活性最好。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
A new green catalyst and antimicrobial agent derived from eco-friendly products of camel bones: synthesis and physicochemical characterization

The circular economy, which aims to produce sustainable materials from waste, plays an important role in environmental research. This work’s primary goal is to reuse food waste to synthesize usable materials. We describe here a sustainable, green, easy, fast, and cheap method for recycling waste camel bone as a renewable material for effective applications. The recycled camel bone (RCB) material has been characterized using thermal gravimetric analysis (TGA), Fourier transform infrared spectroscopy (FT-IR, ultraviolet–visible absorption spectra (UV–Vis), energy band gap, X-ray diffraction (XRD), scanning electron microscopy (SEM)), and Raman spectroscopy were used to analyze the produced material. Particle sizes in the range of 100–120 nm were seen in SEM images. RCB has been utilized as a robust heterogeneous catalyst to promote Knoevenagel condensation reactions in an aqueous medium. The applied sustainable conditions promoted the reactions to afford superior yields (≈98%) after 8 min for all derivatives with six cycles without remarkable alterations in activity. The antimicrobial activity of camel bones, extracted organic species, and extracted hydroxyapatite was assessed against pathogenic microbes: Bacillus cereus, Enterococcus faecium, Escherichia coli, and Candida albicans. Hydroxyapatite showed the best antimicrobial activity against the studied microbial strains.

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来源期刊
Biomass Conversion and Biorefinery
Biomass Conversion and Biorefinery Energy-Renewable Energy, Sustainability and the Environment
CiteScore
7.00
自引率
15.00%
发文量
1358
期刊介绍: Biomass Conversion and Biorefinery presents articles and information on research, development and applications in thermo-chemical conversion; physico-chemical conversion and bio-chemical conversion, including all necessary steps for the provision and preparation of the biomass as well as all possible downstream processing steps for the environmentally sound and economically viable provision of energy and chemical products.
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