氧化锆复合修复:不同喷砂预处理及各种通用胶粘剂对剪切强度的影响。

Malin Janson, Vanessa Bassier, Anja Liebermann, Christoph Matthias Schoppmeier, Maria Di Gregorio-Schininà
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引用次数: 0

摘要

目的:在体外研究了通用胶粘剂和50 μm和110 μm氧化铝颗粒(Al2O3)喷砂对复合材料与氧化锆在不同时效时间修复中的剪切结合强度(SBS)的影响。材料与方法:将1296个氧化锆(Katana zirconia HT)试样随机分为三组:(A) 50 μm Al2O3喷砂组,(B) 110 μm Al2O3喷砂组,(C)对照组。每组进一步分为六个亚组:OPB (Optibond Universal)、PBA (Prime&Bond Active)、IBU (iBond Universal)、CUBQ (Clearfil Universal Bond Quick)、MBP (Monobond Plus)和SBUP (Scotchbond Universal Plus)。应用复合材料(Clearfil Majesty ES-2 Universal),在30天和90天以及7天+ 5000热循环(5-55°C)后的基线(24小时储存)测量SBS (MPa)。在40倍放大下评估失效模式。分析采用Bonferroni平差(α 0.05)的广义线性模型(GLM)。结果:与对照组相比,喷砂显著增加了SBS, B组在热循环后表现出最高的耐久性,随着老化时间的推移,该值逐渐降低。A、B组IBU(21.43±2.7 MPa);25.60±5.78 MPa), SBUP(19.26±3.2 MPa;23.62±4.4 MPa), CUBQ(19.92±2.8 MPa);22.75±4.34 MPa)的SBS最高,以粘接失败为主,内聚失败主要发生在高SBS亚组。结论:Al2O3预处理能显著提高复合材料与氧化锆的结合强度,且粒度越大效果越明显。建议使用含有mdp的粘合剂进行可靠的氧化锆修复。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Composite Repair on Zirconia: Influence of Different Sandblasting Pretreatments and Various Universal Adhesives on Shear Bond Strength.

Purpose: This in-vitro study evaluated the effect of universal adhesives and sandblasting with 50 μm and 110 μm aluminum oxide particles (Al2O3) on the shear bond strength (SBS) between composite and zirconia in repair applications across different aging intervals.

Materials and methods: 1296 zirconia specimens (Katana Zirconia HT) were randomized into three main groups: (A) sandblasting with 50 μm Al2O3, (B) sandblasting with 110 μm Al2O3, and (C) control. Each group was further divided into six subgroups: OPB (Optibond Universal), PBA (Prime&Bond Active), IBU (iBond Universal), CUBQ (Clearfil Universal Bond Quick), MBP (Monobond Plus), and SBUP (Scotchbond Universal Plus). Composite (Clearfil Majesty ES-2 Universal) was applied, and SBS (MPa) measured at baseline (24-h storage) at 30 and 90 days, and after 7 days + 5000 thermocycles (5-55°C). Failure modes were assessed at 40 × magnification. Analysis used a generalized linear model (GLM) with Bonferroni adjustment (α 0.05).

Results: Sandblasting significantly increased SBS compared to controls, with Group B showing the highest durability after thermocycling, with values decreasing over aging periods. In Groups A and B IBU (21.43 ± 2.7 MPa; 25.60 ± 5.78 MPa), SBUP (19.26 ± 3.2 MPa; 23.62 ± 4.4 MPa), and CUBQ (19.92 ± 2.8 MPa; 22.75 ± 4.34 MPa) achieved the highest SBS, with adhesive failures being predominant and cohesive failures mainly in high-SBS subgroups.

Conclusion: Pretreatment with Al2O3 significantly enhances composite-zirconia bond strength, with larger grit sizes more effective. MDP-containing adhesives are recommended for reliable zirconia repairs.

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