固体材料表面有机化合物被动吸附的氧热成像法评价14C对背景的贡献

IF 1 4区 化学 Q4 CHEMISTRY, ANALYTICAL
M. Yu. Vorobyeva, B. K. Zuev, V. G. Filonenko, I. V. Rogovaya, D. V. Filosofov
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引用次数: 0

摘要

提出了一种研究室内空气中有机化合物在固体表面被动吸附的方法。该方法是将材料在室内空气中保持一定时间后,利用氧热成像法检测材料表面的有机物。该方法通过评估材料表面的碳总量,并在低本底实验中评估材料表面吸附的有机物对辐射本底的14C贡献。该方法已在两个不同机构的实验室进行了测试。将样品在室内空气中放置10分钟至34天,评估其吸附在铂、钯和熔融二氧化硅表面的有机物总量。已经观察到吸附的差异,它们取决于表面的材料组成和进行实验的洁净室的级别。该方法允许检测样品而无需将其转移到其他地方。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Oxythermography Method for Assessing Passive Adsorption of Organic Compounds on Surfaces of Solid Materials to Evaluate the 14C Contribution to the Background

The method for investigating passive adsorption of organic compounds from the indoor air on surfaces of solids is proposed. The method is based on detecting organic matter on the surface of the material using oxythermography after keeping the material in the indoor air for a certain time. The method evaluates the total amount of carbon on the surface of the material and assesses the 14C contribution of organic substances adsorbed on the surface to the radiation background in low-background experiments. The method has been tested in laboratory rooms of two different institutions. The total amount of organic substances adsorbed on the surface of platinum, palladium, and fused silica has been evaluated after keeping the samples in the indoor air for 10 minutes to 34 days. The differences in adsorption have been observed, and they depend on the material composition of the surface and the class of the cleanrooms where the experiments were performed. The method allows examining the samples without transferring them elsewhere.

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来源期刊
Journal of Analytical Chemistry
Journal of Analytical Chemistry 化学-分析化学
CiteScore
2.10
自引率
9.10%
发文量
146
审稿时长
13 months
期刊介绍: The Journal of Analytical Chemistry is an international peer reviewed journal that covers theoretical and applied aspects of analytical chemistry; it informs the reader about new achievements in analytical methods, instruments and reagents. Ample space is devoted to problems arising in the analysis of vital media such as water and air. Consideration is given to the detection and determination of metal ions, anions, and various organic substances. The journal welcomes manuscripts from all countries in the English or Russian language.
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