{"title":"采用气雾化法制备高饱和磁化强度、低磁芯损耗的新型铁基纳米晶粉末","authors":"Yanqiu Li, Ling Zhang, Xingjie Jia, Yaqiang Dong, Aina He, Jiawei Li, Baogen Shen","doi":"10.1016/j.jmst.2025.03.066","DOIUrl":null,"url":null,"abstract":"Fe-based nanocrystalline powders are ideal soft magnetic materials for matching the wide bandgap semiconductors. Previously developed Fe-based nanocrystalline alloys are difficult to produce high-quality precursor powder by gas atomization due to their poor amorphous forming ability, and their following nanocrystallizations also require high temperatures or heating rates. In present work, we invented novel high-performance Fe-based nanocrystalline powders that can be directly manufactured by gas atomization without annealing. The as-atomized Fe<sub>73.3</sub>Si<sub>12</sub>B<sub>13</sub>Cu<sub>1.7</sub> nanocrystalline powders exhibit fine α-Fe(Si) crystals with an average size of 15.1 nm and high saturation magnetization (<em>M</em><sub>s</sub>) of 156.2 emu/g. The Fe<sub>73.3</sub>Si<sub>12</sub>B<sub>13</sub>Cu<sub>1.7</sub> soft magnetic powder cores annealed at 480°C for 60 min process high effective permeability of 35.9 and low core losses (50 mT/100 kHz) of 310.1 mW/cm<sup>3</sup>. These outstanding magnetic properties and good processability make the developed Fe<sub>73.3</sub>Si<sub>12</sub>B<sub>13</sub>Cu<sub>1.7</sub> nanocrystalline powders highly promising for high-performance inductors and transformers.","PeriodicalId":16154,"journal":{"name":"Journal of Materials Science & Technology","volume":"120 1","pages":""},"PeriodicalIF":11.2000,"publicationDate":"2025-05-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Manufacturing novel Fe-based nanocrystalline powders with high saturation magnetization and low core loss by gas atomization\",\"authors\":\"Yanqiu Li, Ling Zhang, Xingjie Jia, Yaqiang Dong, Aina He, Jiawei Li, Baogen Shen\",\"doi\":\"10.1016/j.jmst.2025.03.066\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Fe-based nanocrystalline powders are ideal soft magnetic materials for matching the wide bandgap semiconductors. Previously developed Fe-based nanocrystalline alloys are difficult to produce high-quality precursor powder by gas atomization due to their poor amorphous forming ability, and their following nanocrystallizations also require high temperatures or heating rates. In present work, we invented novel high-performance Fe-based nanocrystalline powders that can be directly manufactured by gas atomization without annealing. The as-atomized Fe<sub>73.3</sub>Si<sub>12</sub>B<sub>13</sub>Cu<sub>1.7</sub> nanocrystalline powders exhibit fine α-Fe(Si) crystals with an average size of 15.1 nm and high saturation magnetization (<em>M</em><sub>s</sub>) of 156.2 emu/g. The Fe<sub>73.3</sub>Si<sub>12</sub>B<sub>13</sub>Cu<sub>1.7</sub> soft magnetic powder cores annealed at 480°C for 60 min process high effective permeability of 35.9 and low core losses (50 mT/100 kHz) of 310.1 mW/cm<sup>3</sup>. These outstanding magnetic properties and good processability make the developed Fe<sub>73.3</sub>Si<sub>12</sub>B<sub>13</sub>Cu<sub>1.7</sub> nanocrystalline powders highly promising for high-performance inductors and transformers.\",\"PeriodicalId\":16154,\"journal\":{\"name\":\"Journal of Materials Science & Technology\",\"volume\":\"120 1\",\"pages\":\"\"},\"PeriodicalIF\":11.2000,\"publicationDate\":\"2025-05-08\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Materials Science & Technology\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://doi.org/10.1016/j.jmst.2025.03.066\",\"RegionNum\":1,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"MATERIALS SCIENCE, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Materials Science & Technology","FirstCategoryId":"88","ListUrlMain":"https://doi.org/10.1016/j.jmst.2025.03.066","RegionNum":1,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
Manufacturing novel Fe-based nanocrystalline powders with high saturation magnetization and low core loss by gas atomization
Fe-based nanocrystalline powders are ideal soft magnetic materials for matching the wide bandgap semiconductors. Previously developed Fe-based nanocrystalline alloys are difficult to produce high-quality precursor powder by gas atomization due to their poor amorphous forming ability, and their following nanocrystallizations also require high temperatures or heating rates. In present work, we invented novel high-performance Fe-based nanocrystalline powders that can be directly manufactured by gas atomization without annealing. The as-atomized Fe73.3Si12B13Cu1.7 nanocrystalline powders exhibit fine α-Fe(Si) crystals with an average size of 15.1 nm and high saturation magnetization (Ms) of 156.2 emu/g. The Fe73.3Si12B13Cu1.7 soft magnetic powder cores annealed at 480°C for 60 min process high effective permeability of 35.9 and low core losses (50 mT/100 kHz) of 310.1 mW/cm3. These outstanding magnetic properties and good processability make the developed Fe73.3Si12B13Cu1.7 nanocrystalline powders highly promising for high-performance inductors and transformers.
期刊介绍:
Journal of Materials Science & Technology strives to promote global collaboration in the field of materials science and technology. It primarily publishes original research papers, invited review articles, letters, research notes, and summaries of scientific achievements. The journal covers a wide range of materials science and technology topics, including metallic materials, inorganic nonmetallic materials, and composite materials.