反应结合碳化硅(RBSiC)钎焊Si-Ti共晶合金的显微组织和力学性能

IF 5.1 2区 材料科学 Q1 MATERIALS SCIENCE, CERAMICS
Xiaoqian Xue , Fugang Lu , Jia Yang , Yibo Fu , Tong Wu , Qiuguang Zhang , Ce Wang , Yongkang Dong , Panpan Lin , Tiesong Lin , Peng He
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引用次数: 0

摘要

采用Si-Ti共晶合金真空钎焊实现了反应键合碳化硅(RBSiC)的自连接,为高性能碳化硅元件集成提供了一种新途径。本研究对RBSiC上Si-Ti共晶的润湿行为进行了全面的研究,并详细分析了钎焊温度对接头显微组织、力学性能和断口形貌的影响。Si-Ti共晶合金在RBSiC表面表现出极低的15°接触角,表明优越的润湿性和铺展特性对坚固的结合至关重要。接头主要是通过原子尺度的相互作用形成的,没有产生新的金属间化合物,确保了界面的长期稳定性。在1375°C下钎焊15分钟,抗剪强度为154 MPa,在基体处发生断裂,突出了接头的优异力学性能。阐明了接头微观结构的演变和潜在的强化机制,为结合过程的内在行为提供了见解。这种无压连接技术为高性能SiC组件的广泛应用铺平了道路,特别是在要求先进材料完整性和可靠性的行业。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Microstructural and mechanical properties of reaction-bonded silicon carbide (RBSiC) brazed with Si-Ti eutectic alloy
The self-joining of Reaction-Bonded Silicon Carbide (RBSiC) was achieved using a Si-Ti eutectic alloy via vacuum brazing, offering a novel approach for high-performance SiC component integration. This study provides a comprehensive investigation into the wetting behavior of the Si-Ti eutectic on RBSiC, coupled with a detailed analysis of how brazing temperature influences joint microstructure, mechanical properties, and fracture morphology. The Si-Ti eutectic alloy exhibits an exceptionally low contact angle of 15° on the RBSiC surface, indicating superior wettability and spreading characteristics critical for robust bonding. The joints were primarily formed through atomic-scale interactions, with no new intermetallic compounds generated, ensuring the long-term stability of the interface. Brazing at 1375 °C for 15 min resulted in a shear strength of 154 MPa, with fracture occurring at the substrate, highlighting the excellent mechanical properties of the joints. The evolution of the joint microstructure and the underlying strengthening mechanisms were elucidated, providing insights into the intrinsic behavior of the bonding process. This pressureless joining technique paves the way for broader applications of high-performance SiC components, particularly in industries demanding advanced material integrity and reliability.
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来源期刊
Ceramics International
Ceramics International 工程技术-材料科学:硅酸盐
CiteScore
9.40
自引率
15.40%
发文量
4558
审稿时长
25 days
期刊介绍: Ceramics International covers the science of advanced ceramic materials. The journal encourages contributions that demonstrate how an understanding of the basic chemical and physical phenomena may direct materials design and stimulate ideas for new or improved processing techniques, in order to obtain materials with desired structural features and properties. Ceramics International covers oxide and non-oxide ceramics, functional glasses, glass ceramics, amorphous inorganic non-metallic materials (and their combinations with metal and organic materials), in the form of particulates, dense or porous bodies, thin/thick films and laminated, graded and composite structures. Process related topics such as ceramic-ceramic joints or joining ceramics with dissimilar materials, as well as surface finishing and conditioning are also covered. Besides traditional processing techniques, manufacturing routes of interest include innovative procedures benefiting from externally applied stresses, electromagnetic fields and energetic beams, as well as top-down and self-assembly nanotechnology approaches. In addition, the journal welcomes submissions on bio-inspired and bio-enabled materials designs, experimentally validated multi scale modelling and simulation for materials design, and the use of the most advanced chemical and physical characterization techniques of structure, properties and behaviour. Technologically relevant low-dimensional systems are a particular focus of Ceramics International. These include 0, 1 and 2-D nanomaterials (also covering CNTs, graphene and related materials, and diamond-like carbons), their nanocomposites, as well as nano-hybrids and hierarchical multifunctional nanostructures that might integrate molecular, biological and electronic components.
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