{"title":"TiN为界面层的仿生层状Si3N4陶瓷力学性能的改善","authors":"Xinghua Shen, Tongyang Li, Lizhi Zhang, Lujie Wang, Yuan Yu, Huaguo Tang, Zhuhui Qiao","doi":"10.1002/ces2.10248","DOIUrl":null,"url":null,"abstract":"<p>In order to synergistically improve the strength and toughness of Si<sub>3</sub>N<sub>4</sub> ceramic. We imitate the structure of shell nacre and use Si<sub>3</sub>N<sub>4</sub> as the matrix layer, TiN is used as the interface layer. During the experiment, the samples were prepared by dry lamination and discharge plasma sintering techniques. In the process of the study, ceramic samples with different microstructures were obtained by adjusting the amount of TiN addition and sintering temperature. The fracture toughness and flexural strength were improved by the layered ceramics modeled after the micro-nano structure was regulated by the nacre, the toughness can reach to 17.04 ± 1.32 MPa·m<sup>1/2</sup>. At the same time, the bending strength can reach 322 ± 3.2 MPa. Bio-inspired layered ceramics with high toughness can be better choice for industrial equipment in the aerospace field and daily life.</p>","PeriodicalId":13948,"journal":{"name":"International Journal of Ceramic Engineering & Science","volume":"7 3","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2025-04-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://onlinelibrary.wiley.com/doi/epdf/10.1002/ces2.10248","citationCount":"0","resultStr":"{\"title\":\"Improvement of mechanical properties of biomimetic-layered Si3N4 ceramics with TiN as the interface layer\",\"authors\":\"Xinghua Shen, Tongyang Li, Lizhi Zhang, Lujie Wang, Yuan Yu, Huaguo Tang, Zhuhui Qiao\",\"doi\":\"10.1002/ces2.10248\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p>In order to synergistically improve the strength and toughness of Si<sub>3</sub>N<sub>4</sub> ceramic. We imitate the structure of shell nacre and use Si<sub>3</sub>N<sub>4</sub> as the matrix layer, TiN is used as the interface layer. During the experiment, the samples were prepared by dry lamination and discharge plasma sintering techniques. In the process of the study, ceramic samples with different microstructures were obtained by adjusting the amount of TiN addition and sintering temperature. The fracture toughness and flexural strength were improved by the layered ceramics modeled after the micro-nano structure was regulated by the nacre, the toughness can reach to 17.04 ± 1.32 MPa·m<sup>1/2</sup>. At the same time, the bending strength can reach 322 ± 3.2 MPa. Bio-inspired layered ceramics with high toughness can be better choice for industrial equipment in the aerospace field and daily life.</p>\",\"PeriodicalId\":13948,\"journal\":{\"name\":\"International Journal of Ceramic Engineering & Science\",\"volume\":\"7 3\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2025-04-28\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://onlinelibrary.wiley.com/doi/epdf/10.1002/ces2.10248\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"International Journal of Ceramic Engineering & Science\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://onlinelibrary.wiley.com/doi/10.1002/ces2.10248\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"International Journal of Ceramic Engineering & Science","FirstCategoryId":"1085","ListUrlMain":"https://onlinelibrary.wiley.com/doi/10.1002/ces2.10248","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Improvement of mechanical properties of biomimetic-layered Si3N4 ceramics with TiN as the interface layer
In order to synergistically improve the strength and toughness of Si3N4 ceramic. We imitate the structure of shell nacre and use Si3N4 as the matrix layer, TiN is used as the interface layer. During the experiment, the samples were prepared by dry lamination and discharge plasma sintering techniques. In the process of the study, ceramic samples with different microstructures were obtained by adjusting the amount of TiN addition and sintering temperature. The fracture toughness and flexural strength were improved by the layered ceramics modeled after the micro-nano structure was regulated by the nacre, the toughness can reach to 17.04 ± 1.32 MPa·m1/2. At the same time, the bending strength can reach 322 ± 3.2 MPa. Bio-inspired layered ceramics with high toughness can be better choice for industrial equipment in the aerospace field and daily life.