绿色合成掺杂镍纳米羟基磷灰石用于光催化和抗菌剂的应用

IF 2.7 4区材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY

Materials Letters Pub Date : 2025-04-23 DOI:10.1016/j.matlet.2025.138621

Is Fatimah , Nunung Nurlaela , Anas Zahra Fauziyyah , Habibi Hidayat , Muhammad Fauzi Daud , Suresh Sagadevan

{"title":"绿色合成掺杂镍纳米羟基磷灰石用于光催化和抗菌剂的应用","authors":"Is Fatimah , Nunung Nurlaela , Anas Zahra Fauziyyah , Habibi Hidayat , Muhammad Fauzi Daud , Suresh Sagadevan","doi":"10.1016/j.matlet.2025.138621","DOIUrl":null,"url":null,"abstract":"<div><div>Green chemistry approach was applied to synthesize nickel-doped nanohydroxyapatite (Ni/nHA). Miana (<em>Coleus scutellarioides)</em> extract was utilized as a reducing agent in nickel nanoparticles (NiNPs) preparation for being a dopant to nHA by hydrothermal method. The successful synthesis was confirmed from XRD, TEM, SEM, UV-DRS, XPS and FTIR, analysis demonstrating the formation and crystallinity of the nanocomposite with particle size distributed at range of 10–50 nm. Ni/nHA has the band gap energy of 3.31 eV which facilitate its photocatalytic performance. Rhodamine B degradation efficiency of 99.84 % during 15 of photocatalytic oxidation suggests the high photoactivity. In addition, the Ni/nHA exhibits a good antibacterial activity against <em>Eschericia coli</em> and <em>Staphylococcus aureus</em>.</div></div>","PeriodicalId":384,"journal":{"name":"Materials Letters","volume":"394 ","pages":"Article 138621"},"PeriodicalIF":2.7000,"publicationDate":"2025-04-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Green synthesis of Ni-doped nanohydroxyapatite for photocatalysis and antibacterial agent applications\",\"authors\":\"Is Fatimah , Nunung Nurlaela , Anas Zahra Fauziyyah , Habibi Hidayat , Muhammad Fauzi Daud , Suresh Sagadevan\",\"doi\":\"10.1016/j.matlet.2025.138621\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>Green chemistry approach was applied to synthesize nickel-doped nanohydroxyapatite (Ni/nHA). Miana (<em>Coleus scutellarioides)</em> extract was utilized as a reducing agent in nickel nanoparticles (NiNPs) preparation for being a dopant to nHA by hydrothermal method. The successful synthesis was confirmed from XRD, TEM, SEM, UV-DRS, XPS and FTIR, analysis demonstrating the formation and crystallinity of the nanocomposite with particle size distributed at range of 10–50 nm. Ni/nHA has the band gap energy of 3.31 eV which facilitate its photocatalytic performance. Rhodamine B degradation efficiency of 99.84 % during 15 of photocatalytic oxidation suggests the high photoactivity. In addition, the Ni/nHA exhibits a good antibacterial activity against <em>Eschericia coli</em> and <em>Staphylococcus aureus</em>.</div></div>\",\"PeriodicalId\":384,\"journal\":{\"name\":\"Materials Letters\",\"volume\":\"394 \",\"pages\":\"Article 138621\"},\"PeriodicalIF\":2.7000,\"publicationDate\":\"2025-04-23\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Materials Letters\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S0167577X25006500\",\"RegionNum\":4,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q3\",\"JCRName\":\"MATERIALS SCIENCE, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Materials Letters","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0167577X25006500","RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}

引用次数: 0

摘要

采用绿色化学方法合成了掺镍纳米羟基磷灰石（Ni/nHA）。采用水热法制备了镍纳米粒子（NiNPs），并将其作为nHA的掺杂剂。通过XRD、TEM、SEM、UV-DRS、XPS和FTIR等测试手段证实了合成的成功，并分析了纳米复合材料的形成和结晶度，粒径分布在10 ~ 50 nm范围内。Ni/nHA的带隙能为3.31 eV，具有良好的光催化性能。在15个光催化氧化过程中，罗丹明B的降解效率为99.84%，显示出较高的光活性。此外，Ni/nHA对大肠杆菌和金黄色葡萄球菌具有良好的抑菌活性。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

查看原文本刊更多论文

Green synthesis of Ni-doped nanohydroxyapatite for photocatalysis and antibacterial agent applications

Green chemistry approach was applied to synthesize nickel-doped nanohydroxyapatite (Ni/nHA). Miana (Coleus scutellarioides) extract was utilized as a reducing agent in nickel nanoparticles (NiNPs) preparation for being a dopant to nHA by hydrothermal method. The successful synthesis was confirmed from XRD, TEM, SEM, UV-DRS, XPS and FTIR, analysis demonstrating the formation and crystallinity of the nanocomposite with particle size distributed at range of 10–50 nm. Ni/nHA has the band gap energy of 3.31 eV which facilitate its photocatalytic performance. Rhodamine B degradation efficiency of 99.84 % during 15 of photocatalytic oxidation suggests the high photoactivity. In addition, the Ni/nHA exhibits a good antibacterial activity against Eschericia coli and Staphylococcus aureus.

求助全文

通过发布文献求助，成功后即可免费获取论文全文。去求助

来源期刊

Materials Letters 工程技术-材料科学：综合

CiteScore

5.60

自引率

3.30%

发文量

1948

审稿时长

50 days

期刊介绍： Materials Letters has an open access mirror journal Materials Letters: X, sharing the same aims and scope, editorial team, submission system and rigorous peer review. Materials Letters is dedicated to publishing novel, cutting edge reports of broad interest to the materials community. The journal provides a forum for materials scientists and engineers, physicists, and chemists to rapidly communicate on the most important topics in the field of materials. Contributions include, but are not limited to, a variety of topics such as: • Materials - Metals and alloys, amorphous solids, ceramics, composites, polymers, semiconductors • Applications - Structural, opto-electronic, magnetic, medical, MEMS, sensors, smart • Characterization - Analytical, microscopy, scanning probes, nanoscopic, optical, electrical, magnetic, acoustic, spectroscopic, diffraction • Novel Materials - Micro and nanostructures (nanowires, nanotubes, nanoparticles), nanocomposites, thin films, superlattices, quantum dots. • Processing - Crystal growth, thin film processing, sol-gel processing, mechanical processing, assembly, nanocrystalline processing. • Properties - Mechanical, magnetic, optical, electrical, ferroelectric, thermal, interfacial, transport, thermodynamic • Synthesis - Quenching, solid state, solidification, solution synthesis, vapor deposition, high pressure, explosive