高压高温立方压机顶砧与叶蜡石块压力传递机理的数值模拟与验证

IF 4.3 3区 材料科学 Q2 MATERIALS SCIENCE, COATINGS & FILMS
Mrinal Dwivedi , Kannan Murugesan , N. Arunachalam , M.S. Ramachandra Rao
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引用次数: 0

摘要

在高压高温(HPHT)立方压机中,压力需要通过称为超级单体的材料界面的不同组合传递到碳金属催化剂体系。超级单体结构由碳金属催化剂系统组成,该系统被石墨加热器包围,并被热和电绝缘体包围。压力传递到形成超级单体外壳的叶蜡岩块是确保系统内部压力积聚的关键。然而,由于极端的操作条件,无法使用传统的监测方法,因此对这种压力传递的理解受到影响。这就需要使用有限元法来深入了解压力传递机理。本文采用一种新颖的有限元框架分析了铁砧叶蜡石界面系统的压力产生和叶蜡石的压力传递。叶蜡石的建模需要使用拉格朗日元,由于其弹塑性行为,拉格朗日元在高压条件下会变形。为了克服过度的单元畸变,需要进行局部重网格划分,这不仅增加了计算量,而且导致计算结果不准确。本工作提出使用耦合欧拉-拉格朗日(CEL)技术来模拟铁砧系统,其中叶蜡石使用欧拉单元建模,铁砧使用拉格朗日单元建模。这解决了由于欧拉单元在空间中固定的网格畸变问题。Mohr-Columb准则用于描述叶蜡石的弹塑性行为。将叶蜡石块体中心压力与实验结果进行了比较,结果吻合良好,误差小于1.6%。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

Numerical simulation and validation of pressure transfer mechanism between anvil and pyrophyllite block in high pressure high temperature cubic press

Numerical simulation and validation of pressure transfer mechanism between anvil and pyrophyllite block in high pressure high temperature cubic press
In High Pressure High Temperature (HPHT) cubic press, the pressure needs to be transmitted to the carbon metal catalyst system through different combination of material interfaces called the supercell. The supercell structure consists of the carbon metal catalyst system enclosed within a graphite heater surrounded by a thermal and electrical insulators. The pressure transmission to the pyrophyllite block which forms the outer envelope of the supercell is essential to ensure the pressure buildup inside the system. The understanding of this pressure transfer, however, is affected by the inability of using traditional monitoring methods due to extreme operating conditions. This requires use of Finite Element Method in order to gain in-depth understanding of the pressure transfer mechanism. In this work a novel finite element framework is used to analyze the pressure generation at the anvil pyrophyllite interface system and pressure transfer through the pyrophyllite. Modelling of Pyrophyllite requires use of Lagrangian elements which distort at high pressure conditions due to its elasto-plastic behavior. To overcome excessive element distortion, local re-meshing needs to be done which not only increases the computational effort but also leads to inaccurate results. This work proposes to use the Coupled Eulerian Lagrangian (CEL) technique to model anvil system where pyrophyllite is modelled using Eulerian elements and anvil is modelled using Lagrangian elements. This solves the issue of mesh distortion as Eulerian elements are fixed in space. Mohr-Columb criteria is used to capture the elasto-plastic behavior of the pyrophyllite. Pressure at the center of the pyrophyllite block is compared with experiments and an excellent match with error less than 1.6 % between the results is observed.
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来源期刊
Diamond and Related Materials
Diamond and Related Materials 工程技术-材料科学:综合
CiteScore
6.00
自引率
14.60%
发文量
702
审稿时长
2.1 months
期刊介绍: DRM is a leading international journal that publishes new fundamental and applied research on all forms of diamond, the integration of diamond with other advanced materials and development of technologies exploiting diamond. The synthesis, characterization and processing of single crystal diamond, polycrystalline films, nanodiamond powders and heterostructures with other advanced materials are encouraged topics for technical and review articles. In addition to diamond, the journal publishes manuscripts on the synthesis, characterization and application of other related materials including diamond-like carbons, carbon nanotubes, graphene, and boron and carbon nitrides. Articles are sought on the chemical functionalization of diamond and related materials as well as their use in electrochemistry, energy storage and conversion, chemical and biological sensing, imaging, thermal management, photonic and quantum applications, electron emission and electronic devices. The International Conference on Diamond and Carbon Materials has evolved into the largest and most well attended forum in the field of diamond, providing a forum to showcase the latest results in the science and technology of diamond and other carbon materials such as carbon nanotubes, graphene, and diamond-like carbon. Run annually in association with Diamond and Related Materials the conference provides junior and established researchers the opportunity to exchange the latest results ranging from fundamental physical and chemical concepts to applied research focusing on the next generation carbon-based devices.
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