评估扭转恢复试验与聚合物改性沥青变形恢复测量指标的相互联系

Nazmus Sakib , Sabrina Islam , Shahriar Bin Kabir , Shamima Yasmin , Md. Mamun Kaysar , Joy Prakash Chowdhury , Md. Mahbubur Rahman
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引用次数: 0

摘要

聚合物改性沥青(PMB)的弹性回复率被认为是评价其通过恢复部分载荷相关变形来抵抗永久变形能力的有效参数。从概念上讲,它表示为沥青样品上使用各种设备和加载类型的恢复应变(在固定时间后零加载下测量)与最大应变(加载下)的比率。回收试验也表明聚合物的存在以及聚合程度。因此,在采购机构进行实地盘存检查时,这种测试可作为快速质量控制和核查工具。传统的基于韧性计的弹性恢复(ER-DB)方法依赖于笨重的大型设备、精细的样品制备工艺和可变的真应变率。另一方面,基于多重应力蠕变恢复(MSCR)测试的百分比恢复(%R)利用剪切应力在小沥青样品上施加的蠕变恢复来获得类似的信息,但它需要一个复杂而昂贵的设备。扭转恢复(TR),使用易于携带,手动操作,快速和廉价的设置,也依赖于剪切变形和角度恢复。在本研究中,用5种SBS和一种基础沥青制备了15种PMBs,评估了TR与这些既定方法的相关性。结果显示出很强的线性关系,线性回归R2值在许多情况下超过0.85,特别是用相同聚合物制成的PMBs。值得注意的是,TR和ER-DB的R2大于0.90,特别是在sbs型特定病例中,而全球相关为0.76。此外,我们发现TR可以可靠地用于sbs用量的初步定量,R2为0.88。有趣的是,扭转恢复值与动态模量值和相关参数具有良好的全局相关性,R2≥0.8。事实上,SBS用量、扭转恢复和动模量参数也表现出良好的PMB特异性相关性和合理的全局相关性。其他因素和相关性也表明,TR结果与现有的测试方法吻合良好,因此可用于PMB质量的初步评估和聚合物的定量存在,特别适合现场部署。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Evaluating Torsional Recovery test for interlinkage with deformation-recovery measurement metrics of polymer modified bitumen
Elastic recovery of polymer modified bitumen (PMB) is considered an effective parameter to evaluate its capacity to resist permanent deformation through recovering some part of load-related deformation. Conceptually, it is represented as the ratio of recovered strain (measured under zero loading after a fixed duration) to maximum strain (under loading) on a bitumen sample, using various devices and loading types. Recovery tests also indicate the presence of polymer as well as degree of polymerization. Hence, such tests can be useful as rapid quality control and verification tool during field inventory inspections by procuring agencies. Traditional method, that is, ductilometer-based Elastic Recovery (ER-DB) relies on an unwieldy large device, delicate sample preparation process, and variable true strain rate. On the other hand, Multiple Stress Creep Recovery (MSCR) test-based Percent Recovery (%R) utilizes creep-recovery from application of shear-stress on a small bitumen sample for obtaining similar information, but it requires a sophisticated and expensive device. Torsional Recovery (TR), which uses an easily portable, manually operable, quick and inexpensive setup, also relies on shear deformation and angular recovery. In the present study, TR was evaluated for its correlation with these established methods using a total of 15 PMBs, prepared with 5 types of SBS and one base bitumen. The results showed strong linear relationships, with linear regression R2 values exceeding 0.85 in many cases, especially for PMBs made with the same polymer. Notably, TR and ER-DB exhibited R2 more than 0.90, especially within SBS-type specific cases, while global correlation was found to be 0.76. In addition, it was found that TR can be reliably used for preliminary quantification of SBS-dosage with R2 of 0.88. Interestingly, Torsional recovery values show good global correlation with Dynamic Modulus values and associated parameters with R2 0.8. In fact, SBS dosage, Torsional Recovery and Dynamic Modulus parameters also displayed excellent PMB specific correlation and reasonable global correlation. Other factors and correlations also indicate that TR results align well with existing test methods and hence, can be used for preliminary assessment of PMB quality and quantitative presence of polymer, with particular suitability for site deployment.
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